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Contaminated Soil 1999 EnvironmentalSafetyHealthGeotechnical t O'Reilly, Talbot & Okun —r [ A S S O C I A T E S ] November 3, 1999 File No.J84-05-17 Mr.Peter McErlain Office of Planning and Development City Hall 210 Main Street Northampton,MA 01060 Re: Limited Removal Action Atwood Drive Northampton, MA Dear Mr.McErlain: 293 Bridge Street Suite 500 Springfield MA 01103 Tel 413 788 6222 Fax 413 7B8 8830 Email orete @oto-env com This letter documents completion of a Limited Removal Action (LRA) as defined in the Massachusetts Contingency Plan (310 CMR 40.0318) to remove lead contaminated soil from the above referenced property in Northampton, Massachusetts. Our report is subject to the limitations attached in Appendix A. Background A site locus and site plan are provided as Figures 1 and 2 respectively. An environmental site assessment performed by O'Reilly, Talbot & Okun Associates, Inc. (OTO) for a perspective leasee indicated that fill material was likely present on the Atwood Drive property. A series of test pits was performed on the property, which included analytical testing of the fill material. The fill material was tested for Extractable Petroleum Hydrocarbons (EPH), polychlorinated byphenols (PCBs) and RCRA 8 metals. Location Test Pit 1 (TP-1) contained approximately 2.5 feet of granular fill with concentrations of lead at 347 mg/kg, above the applicable Reportable Concentration (RCS-1) for total lead of 300 mg/kg. No EPH or PCB compounds were detected above Reportable Concentrations. A copy of the test pit log for TP-I is provided in Appendix B Analytical data are summarized in Table I and analytical data sheets are provided in Appendix C. We understand that the City of Northampton was notified of concentrations of lead in site soil above reportable concentrations by facsimile letter dated February 3, 1999 Additional Fill Characterization The extent of lead impacted soil around TP-1 was further characterized through a boring program performed December 18, 1998 and January 29, 1999. Ten additional soil samples were collected on these dates and analyzed for total lead. The results are summarized in Table 1. The locations of samples (NOHO-2,3,5,7,8,9,101,103,105, and 108) and results of total lead analyses are shown on Figure 2. Each of these samples was collected from the fill material within 2.0 to 2.5 feet of the ground surface, with the exception of NOHO-9, which was collected from the natural soil material underlying the fill. Soil sample NOHO-5 had the highest total lead concentration at 783 mg/kg. The T O'Reilly, Talbot & Okun 4-COW-4 [ A S S O C I A T E S ] NOHO-5 sample was tested for leachable lead by the Toxicity Characteristic Leaching Procedure (TCLP) and found to contain a leachable lead concentration of 6.07 mg/I,which exceeded the 5.0 mg/I standard defining a characteristically hazardous waste. Based on the analytical data, an area of lead contaminated soil of approximately 20 cubic yards was identified as shown on Figure 2. Groundwater Characterization In addition to fill characterization, a groundwater monitoring well (NOHO-1) was installed adjacent to test pit TP-1 (approximately 15 feet south in the inferred downgradient groundwater flow direction) to evaluate potential groundwater impacts. The well was installed on December 18, 1999 in a boring drilled to a depth of 24 feet. The monitoring well installation and subsurface conditions encountered are shown on the boring log attached in Appendix B. Soil samples were collected by split spoon using standard penetration tests continuously to depths of 15 feet and screened for VOCs with the PID. No VOCs were detected. Soil conditions consisted of granular fill to a depth of 2 feet, followed by fine to medium sand, with trace amounts of silt Thin (1 to 2 inch thick) layers of clay were observed below 10 feet. Groundwater was encountered at a depth of approximately 18 feet. On December 28, 1998 a groundwater sample was collected from the monitoring well. The groundwa- ter sample was collected using an individually dedicated disposable plastic bailer. Prior to sample collection three to five times the volume of standing water in the well was removed to provide a sample of formation water in the well for collection. Groundwater samples were than collected into pre-preserved bottles for analysis for Extractable and Volatile Petroleum Hydrocarbons (EPH/VPH) Volatile Organic Compounds (VOCs) and dissolved lead. The dissolved lead sample was filtered prior to preservation to remove sediment. The analytical data sheets for the groundwater analyses are also attached in Appendix C. As shown, no contaminants were detected in the groundwater samples. A groundwater sample was also screened in the field for pH and specific conductance. The pH reading was 6.5 and the specific conductance reading was 290. These values are within the range typical for this geographic region. Limited Removal Action Excavation The lead contaminated soils were excavated by CT Environmental, Inc. of Longmeadow, Massachusetts on May 27, 1999. The excavation was observed by Bruce H. Nickelsen of O'Reilly, Talbot & Okun Associates, Inc. The soils were excavated to a depth of 2.5 feet (the depth of fill) and to the lateral limits shown on Figure 2. Excavated soils were placed on top of and covered with plastic sheeting. Approximately 5 cubic yards was excavated from the vicinity of the NOHO-5 sample location, which had been found to be characteristically hazardous based on TCLP testing. The remaining approximately 15 cubic yards of soil were excavated and stockpiled separately. A soil sample was collected from the 15 cubic yard pile (STOCK-1) and analyzed for TCLP lead. A concentration of 3.23 mg/I of leachable lead was detected from this sample, indicating the 15 cubic yards pile of soil was not a characteristically hazardous waste. Page 2 O'Reilly, Talbot & Okun ~C=1.4-4 ( A S S U C I A r E S I Sail Disposal On September 9, 1999, the 15 cubic yard stockpile was transported to the Northampton Landfill for use as daily cover under a Massachusetts Bill of Lading. The Bill of Lading is attached in Appendix D. The 5 cubic yard pile was transported to Chem-Met Services, Inc. of Brownstown, Michigan for disposal in their hazardous waste landfill. A copy of the hazardous waste manifest showing this disposal is attached in Appendix D.Both Bill of Lading and hazardous waste manifest were signed by a representative of the City of Northampton as generator of the waste material. Conclusions Based on the investigations and analytical test results described in this letter lead impacted soil has been removed from the vicinity of the TP-1 location to levels below applicable Reportable Concentrations. Given that soils which exceed applicable reportable concentrations have been removed, no further actions are warranted under the MCP, other then maintenance of this documentation report for a period of five years as required under 310 CMR 40.0318. You should sign section M of the last page of the original Bill Of Lading,and keep it with your records. It has been our pleasure to work with you on this project. Please feel free to call us if you have any questions or comments. Very truly yours, O'Reilly,Talbot&Okun Associates,Inc. �l._,/t(,L&t 11/1,1a/tit Bruce H. Nickelsen Associate cc Wayne Fe den Attachments: Figures Tables Appendix A Appendix B- Appendix C Appendix D -Limitation Test Pit/Boring Logs -Analytical Data -Bill of Lading, Manifest Page 3 Kevin J. O'Reilly Principal Table I Soil Quality Data Atwood Drive r "„ TP:l/S."1 s®H0.2 IOHs QRO5 NOHO-1 NO °4 e e OHO- =14(*D e o e O...'77 k:` t a i 02 fy. 104�" rations i wx Depth;- E ' . .` a7 .v o-- a". axa '. Aa'2„O it .::" ® Coll . 0 xxft ..' ,n), . t e t �w; t o " a° ni) °mss ND3a.: °tiND£ ° @y:NOD l rip?,s ?m EPfi mB,.�) .ti"� 'tn. W Si.._ . , t$ . ,. .. Aliphatics/Aromatics ND NA NA NA NA NA NA NA NA NA NA Various Targeted PAH's Analytes(mg/Kg) Fluoranthene ND NA NA NA NA NA NA NA NA NA NA 1,000 Phenanthrene ND NA NA NA NA NA NA NA NA NA NA 100 Pyrene ND NA NA NA NA NA NA NA NA NA NA 700 PCB-1254 0.75 NA NA NA NA NA NA NA NA NA NA 2 KCRA�SJ TALS.(tng/ 3'r-'! . . 34' .. .S.3" ei4x .8z. .=i333 . e _3 357'3337 y133 '. ,.: .r_. ?. ""*s'.'.`::,:..: Total Barium 51.3 NA NA NA NA NA NA NA NA NA NA 1,000 Total Chromium 13.8 NA NA NA NA NA NA NA NA NA NA 1,000 Total Lead 3473 163 69 783 73 159 47.2 69.9 10.2 9.26 10.9 300 TCLP Lead NA NA NA 6.07 NA NA NA NA NA NA NA N/A i Samples were screened for Volatile Organic Compounds(VOCs)with a Photoionization Detector(PID). l "ND" indicates Not Detected. Only detected analytes are shown. "NA" indicates Not Analyzed.N/A indicates Not Applicable. J Following receipt of analytical results,this sample was composited by the laboratory,and three separate aliquots of soil analyzed for total lead.The results of this analysis indicated total lead readings of 380,302,and 474 mg/kg total lead. \\Main\data\Bruce Nickelsen\atwooddrive table 1.lwp O'Reilly, Talbot & Okun Associates, Inc. Atwood Drive Northampton, Massachusetts Site Locus October 1999 Figure 1 N O'Reilly, Talbot & Okun [ A S S O C I A T E S ] 1 LIMITATIONS 1. The observations presented in this report were made under the conditions described herein. The conclusions presented in this report were based solely upon the services described in the report and not on scientific tasks or procedures beyond the scope of the project or the time and budgetary constraints imposed by the client. 2. In preparing the report O'Reilly, Talbot, Okun & Associates Inc relied on certain information provided by state and local officials and other parties referenced herein and on information contained in the files of state or local regulatory agencies. Although there may have been some degree of overlap in the information provided by these sources, O'Reilly,Talbot, Okun&Associates, Inc. did not attempt to independently verify the accuracy or completeness of all information reviewed or received during the course of this assessment. 3. Observations were made of the site and of the structures on the site as indicated within the report. Where access to portions of the site or to structures on the site was unavailable or limited, we render no opinion as to the presence or hazardous materials or oil, or to the presence of indirect information relating to hazardous materials or oil in that portion of the site. In addition, we render no opinion as to the presence of hazardous materials or oil, where direct observations of portions of the site where obstructed by objects or coverings on or over these surfaces. 4. Unless otherwise specified in the Report, we did not perform testing or analyses to determine the presence or concentration or concentration of asbestos or polychlorinated biphenyls (PCBs) at the site or in the environment at the site. 5. The purpose of this Report was to assess the physical characteristics of the subject site with respect to the presence of oil or hazardous material (OHM) in soil or groundwater at the site, and to assess risks associated with detected OHM, within the meaning of the Massachusetts Contingency Plan, 310 CMR 40.0000. No specific attempt was made to check on the compliance of present or past owners or operators of the site with federal, state, or local laws and regulations, environmental or otherwise. 6. Risk assessment was performed in accordance with generally accepted practices of government agencies and other consultants conducting similar characterizations. The findings of the risk characterization are dependent on numerous assumptions and uncertainties inherent in the risk assessment process. Therefore, the findings of the risk assessment should not be interpreted as an absolute characterization of actual risks, but as general indicators highlighting potential sources of risk at the site. Although the range of uncertainty in the risk characterization has not (and cannot) be quantified, the use of conservative assumptions throughout the process would be expected to err on the side of protection of human health and the environment. 7. Where analytical data or information regarding site environmental conditions was unavailable or limited, we render no opinion as to risks due to oil or hazardous materials in those portions of the site, or to oil or hazardous materials not tested for. 8. Our report was prepared for the exclusive benefit of our client. Reliance upon the report and its conclusions is not extended to third parties or future property owners. We acknowledge copies of our report may be submitted to DEP for MCP compliance purposes. O'Reilly, Talbot & Okun Associates, Inc. 293 Bridge Street, Suite 500 Springfield,Massachusetts. 01103 (413)-788-6222 PROJECT Description: Atwood Drive Location: Northhampton, MA Test Pit No. TP-1 Job No. 084-5-17 Date: 06/23/98 Engineer/Geologist: Weather: Bruce Nickelsen Contractor: Gary Guertin Ex. Overcast, 70's Backhoe: Case 580 Capacity: 1/2 yard cubic yard Ground Elev: Start: Finish: 9:10 9:30 DEPTH SOIL DESCRIPTION EXCAV. EFFORT BOULDER COUNT PID REMARKS 5 Brown Fine to Medium sand with some brick fragments(Fill) E None 1 S-1 =ND 2.5' Sample S-1 collected from 0-2.5 feet Natural Brown Fine Sand,trace silt. Sample S-2, collected from 8' E None S-2 =ND 10 8.0 End of Exploration REMARKS: 1. Samples screened with TEl 580B Photoionization detecto r, referenced to part per million(PPM) 2. Soil at 8'was moist. benzene in air. PLAN Vol. = LEGEND EFFORT E=Easy M=Moderate D=Difficult O'REILLY, TALBOT& O%UN ASSOCIATES, INC ENVIRONMENTAL AND GEOTECHNICAL ENGINEERING CONSULTANTS LOG OF BORING NOHO—I SHEET I OF I IOJECT Atwood Drive °CATION 31LUNG COMPACTOR Seaboard IFORS(&N Jeff N. i DATE STARTED 12/1898 DATE FINISHED 13/18/98 KILLING EQUIPMENT BS) ''COMPLETION DEPTH 1 240 GROUND SURFACE ELEV. DAIUM YPE BR RSA. SIZE@MEOE COPE BAMEL ''.,NO.SA.W 7 DIST. UNDIST. ASINO I' TIME FIRST COMPL. 1 110. ASING HAtbt WEIGHT I DROP I WATER LEVEL(FT) \MPLER 21/a Split Spoon i HORMO NoM 12 feet South of TP-1 9MPLER AMMER WEIGHT IGO pound DROP 30inde I LOCATION 'ENGINEEWGEOLWLET Meluu Sdwmmber SAMPLES DEPTH Ff. SAlNV.4 DESCRIPTION �I FIELD IEASUREMENTS SOIL REMARKS PENSTR. RF96i. MA IN. RRC D4 I MPl NO. DESCRIPTION ' 4W&S 2/&bH NIINII 1 1 ID/1V16/18 INIMIVII 9/19/11 20' 6' ID IT If IS' 20' sl S3 S3 5-4 5-5 S-a S-7 Helium dace.bmwm!m medium SAND.Pace silt brck Fnvpnmo. Med ium,dense, brown d ne,dowi fine mmedium SAND,trace medium,dub It and trace fine snivel Medium dense,down firm to medium SAND,trace medium,dense brown,silt and mu fine gravel. Medium,da,s brown.fine to medium SAND.Idle,medium due. brown,cons SAND,twee silt(moist). Medium,dense.brown,fine to medium SAND.liMe medium.dose own,poem SAND, ne silt(moist). d sane NO ND ND ND NO ND N[1 PII _ _ S Mdium Sand the _ � _ ♦� 5 ♦ _ ._ — _ ♦ Dame blown,r e to medium SAND.tram dmu blow SILT trot at 18.5. Beacon 2'wet dense,brown.silt fine SAND. Rep 0.5 feet Medium dense,hale SILTY,Eve SAND.(moist). (Hater table 125fl) Bottom 5'Mdimq dame,dark brown,silty,fire SAND.(sWm¢d) Little,very stf dark brown,clay. E a __ 1 _ 15 L 1— _ 20 zs emmin. Sampler maned in field wing TEL Model 580B RfRmed to PPM of Benzene in air. Readings in meta unia'ND.'indicates none detected Well set m2v',IV oft'PVC gaming(24 IT of filter sand(24.0..12 -10 01-Ground Surface)7 of bmMite(12 0-10.0),PVC ruing pipe W-N2 fm above ground emfea.metal rising (N 2 ft below ground surface to N2 ft above ground surface). SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID:TP-1/S-1 Lab ID No: AB10787 Matrix: Soil Collected: 0623/98 by OTO Received on 07/02/98 by DDR QC and Data Review by Location: Atwood Drive-Northampton,MA Client Job No: J84-0520 Preservative: Refrigeration Container: 1 Glass Soil Jar Condition of Sample as Received: Satisfactory Delivered by: Courier Parameter PCB-1016 PCB-1221 PCB-1232 PCB-1242 PCB-1248 PCB-1254 PCB-1260 Decachlorobiphenyl (%) % Solids Polychlorinated Biphenyls (PCB's) Modified SW846 8081/8082 Result (ug/Kg) Not detected Not detected Not detected Not detected Not detected 750 Not detected 73 91.3 MDL Extracted Analyzed Analyst 250 07/02/98 07/06/98 TG 250 07/02/98 07/06/98 TG 250 07/02/98 07/06/98 TO 250 07/02/98 07/06/98 TG 250 07/02/98 07/06/98 TG 250 07/02/98 07/06/98 TG 250 07/02/98 07/06/98 TG 07/02/98 07/06/98 TG 0.1 07/02/98 07/02/98 SEC SAk SPECTitUMANALYTICAL.MC. Massachusetts Certification MA 138 Connecticut Approval No.PH 0777 New Hampshire ID No.2538 New York ID No. 11393 Florida HRS87448 O'Reilly, Talbot&Okun Assoc. 293 Bridge Street Springfield, MA 01103 Attn. Bruce Nickelsen July 9, 1998 Client Project No J84-0520 Location: Atwood Drive - Northampton, MA Lab TD Nn Client ID Analysis Regnestrrl. AB10787 TP-1/S-1 Extractable Oil Hydrocarbons Modified SW846 8081/8082 Total Arsenic Total Barium Total Cadmium Total Chromium Total Lead Total Mercury Total Selenium Total Silver AE10788 TP-4/S-1 Extractable Oil Hydrocarbons Modified SW846 8081/8082 Total Arsenic Total Barium Total Cadmium Total Chromium Total Lead Total Mercury Total Selenium Total Silver AB10789 TP-5/S-1 Extractable Oil Hydrocarbons Modified SW846 8081/8082 Total Arsenic Total Barium Total Cadmium Total Chromium Total Lead Total Mercury Continued next page. . . ENVIRONMENTAL ANALYSES 11 Alme en Drive •Agawam,Massachusetts 01001 •413-789-9018 • FAX 413-789-4076 SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID:TP-1/S-1 Lab ID No.:AB10787 Matrix Soil Collected: 06/23/98 by OTO Received on 07/02/98 by DDR QC and Data Review by Location: Atwood Drive-Northampton,MA Client Job No.: J84-0520 Preservative: Refrigeration Container: 1 Glass Soil Jar Condition of Sample as Received: Satisfactory Delivered by: Courier Extractable Petroleum Hydrocarbons MA DEP Modified EPA 8270/8100 Parameter for AB10787 Aliphatics/Aromatics(mg/Kg) C9- C18 Aliphatics C19- 06 Aliphatics C11- C22 Aromatics Targeted PAH's Analytes (ug/Kg) Acenaphthene Acenaphthylene Anthracene Benzo (a) anthracene Benzo (b) fluoranthene Benzo (k) fluoranthene Benzo (a)pyrene Benzo (g,h.i)perylene Chrysene Dibenz(a,h) anthracene Fluoranthene Fluorene Indeno (1,2,3-cd)pyrene 2-Methylnaphthalene Naphthalene Phenanthrene Pyrene Surrogate Recovery(%) 1-Chloro-octadecane(%SR) Ortho-Terphenyl(%SR) Results Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected 43 42 MDL Extracted Analyzed Analyst 33 07/02/98 07/08/98 MB 33 07/02/98 07/08/98 MB 33 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 07/02/98 07/08/98 MB 07/02/98 07/08/98 MB % Solids 91.3 0.1 07/02198 07/02/98 SEC CHAIN OF CUSTODY RECORD age I of 1 9� SPECTRUM ANALYTICAL OJECT NO.: -,',' -- t(- _ 3-- 2.. 'E NAME: .'.•.-_,2.2_J,o'Ip! b.' %.-i CATION: !1 /'0,r-1) ;,\G 'u:td 1-l.V\ STATE(L-14- FERENCE QUOTE NUMBER (RQN): RCHASE ORDER Na: OJECT Mgr: /ti it /li—e. >:-./ L,L MPLER(s): tMPLE TYPE & MATRIX CODES: 1-PCBS 2-PEST(608/B080) 4°C 2=HCI 3=F12SO4 4=HNO, 5=OTHER > j w N ce ce a :COMPOSITE G=GRAB >i r i E Q rf' :AQUEOUS 3=SLUDGE :SOIL 4=SEDIMENT S=OTHER X E2 F- E t B USE DNLY SAMPLE I.D. DATE TIME ryi;z'? 773- ( s- r 6/z3 (s1jt 1-4 s( s- f ' :t 2 Q ;a,.W.• T-0-5 S- ( L< 2 --r4 cc". s- ( 1 '7 (1 ,;,,»v. Lrci/ 4 BY: RECEIV,FD V., DATE TIME ;RELINQUISHED % C' f f�91, , �:A ,J 7 Y 4�/ - 7-af91( ?Lc° IPECIAL INST9UCTIONS: r •{ �i-Yt;l I,(,�Pr74L.;, DAd �A ❑Return Sample ❑ Dispose TAT • Standard ❑SP�ISI TAT •TAT for begins when •TAT for samples •All TATS are subject DATE RESULTS SPECIAL HANDLING: Please check business consent. day. after Analysis -7 to 10 r 4a -24 hr-48 sample Is read after to laboratory NEEDED' usness Business days hr-T2 hr-5 b.days received at test to the. 3 pm will begin on the approval and customer cirry /7,11p 1U�� $ I „A / / d I � M "1» � ' .�i. ��' / ( f U �I�S/Jt l_ / %�/�f: 7 Fax results when available to ( ) 11 Almgrea Drive•Agawam,M chum 01001 •413-789-9018•Fax 413-789-4076 SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID:TP-1/S-1 Lab ID No: AB1O787 Matrix Soil Collected: 06/23/98 by OTO Received on 07/02/98 by DDR QC and Data Review by Location: Atwood Drive-Northampton,MA Client Job No: J84-0520 Preservative: Refrigeration Container: 1 Glass oil Jar Condition of Sample as Received: Satisfactory Delivered by: Courier Parameter Total Arsenic Total Barium Total Cadmium Total Chromium Total Lead Total Mercury Total Selenium Total Silver Result (mg/Kg) nd 51.3 nd 13.8 347 nd nd nd MDL 0.904 0.904 0.904 0.904 0.452 0.225 0.452 1.81 Metals Method EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 245.1 EPA 200.7 EPA 200.7 Digested Analyzed Analyst 07/08/98 07/08/98 CR 07/08/98 07/08/98 CR 07/08/98 07/08/98 CR 07/08/98 07/08/98 CR 07/08/98 07/08/98 CR 07/08/98 07/07/98 JM 07/08/98 07/07/98 CR 07/08/98 07/07/98 CR PECTIN ANALYTICAL,INC. Massachusetts Certification MA 138 Connecticut Approval No. PH 0777 New Hampshire ID No. 2538 New York ID No. 11393 Florida HRS87448 O'Reilly, Talbot& Okun Assoc 293 Bridge Street Springfield, MA 01103 Attu- Bruce Nickelson December 30, 1998 Client Project No.: 30840517 Location: Atman - Northampton I all in No Client Til Analysis Requested .4829056 NOHO-2 Total Lead AB29057 NOHO-5 Total Lead AB29058 NOHO-3 Total Lead AB29059 NOHO-7 Total Lead AB29060 NOHO-9 Total Lead AB29061 NOHO-l0 Total Lead Extractable Oil Hydrocarbons Modified SW846 8082 AB29062 NOHO-11 Total Lead Extractable Oil Hydrocarbons Modified SW846 8082 AB29063 NOHO-12 Total Lead Extractable Oil Hydrocarbons Modified SW846 8082 .4829064 NOHO-13A Total Lead Extractable Oil Hydrocarbons Modified SW846 8082 AB29065 NOHO-12B Total Lead Extractable Oil Hydrocarbons Modified SW846 8082 AB29066 NOHO-14 Total Lead Extractable Oil Hydrocarbons Modified SW846 8082 AB29067 NOHO-15 Total Lead Extractable Oil Hydrocarbons Modified SW846 8082 AB29068 NOHO-16 Total Lead Extractable Oil Hydrocarbons Continued next page. . . ENVIRONMENTAL ANALYSES 11 Almgen Drive •Agawam,Massachusetts 01001 • 413-789-9018 • FAX 413-789-4076 O'Reilly,Talbot& Okun Assoc. December 30, 1998 Client Project: J0840517 Location. Atman-Northampton I ah TT) Nn Client IT) Aagjvsis Requested AS29068 NOHO-16 Modified SW846 8082 4829069 NOHO-17 Total Lead Extractable Oil Hydrocarbons Modified SW846 8082 21829070 NOHO-18 Total Lead Extractable Oil Hydrocarbons Modified SW846 8082 ayeh ENVIRONMENTAL ANALYSES Preside '7�T.�: :tb y Director 11 Alma en Drive •Agawam,Massachusetts 01001 • 413-789-9018 • FAX 413-789-4076 SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: NOHO.2 Lab ID No: AB29056 Matrix Soil Collected: 12/18/98 OTO Received on 12/21/98 MBR QC and Data Review by Location: Atman -Northampton Client Job No: J0840517 Preservative: Refrigeration Container: 1 Clear Glass Jar Condition of Sample as Received: Satisfactory Delivered by: Client Parameter Total Lead Total Lead EPA Method 6010200.7 Result (mg/Kg) MDL Digested Analyzed Analyst 163 0.449 1229/98 12/30/98 DMM SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: NOHO-3 Lab ID No: AB29058 Matrix: Soil Collected: 12/18/98 by OTO Received on 12/21/98 by MBR QC and Data Review by Location: Atman-Northampton Client Job No: J0840517 Preservative: Refrigeration Container. 1 Clear Glass Jar Condition of Sample as Received: Satisfactory Delivered by: Client Parameter Total Lead Total Lead EPA Method 6010/200.7 Result (mg/Kg) MDL Digested Analyzed Analyst 69.0 0.464 12/29/98 12/30/98 DMM SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: NOBO-5 Lab ID No: AB29057 Matrix: Soil Collected: 12/18/98 by OTO Received on 12/21/98 by MBR OC and Data Review by Location: Atman -Northampton Client Job No: J0840517 Preservative: Refrigeration Container: 1 Clear Glass Jar Condition of Sample as Received: Satisfactory Delivered by: Client Parameter Total Lead Total Lead EPA Method 6010/200.7 Result (mg/Kg) MDL Digested Analyzed Analyst 783 0.455 12/29/98 12/30/98 DMM SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: NO11O-7 Lab ID No: AB29059 Matrix Soil Collected: 12/18/98 by OTO Received on 12/21/98 by MBR QC and Data Review by Location: Atman-Northampton Client Job No: J0840517 Preservative: Refrigeration Container: 1 Clear Glass Jar Condition of Sample as Received: Satisfactory Delivered by Client Parameter Total Lead Total Lead EPA Method 6010/200.7 Result (mg/Kg) MDL Digested Analyzed Analyst 73.4 0558 12/29/98 12/30/98 DMM SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: NO13O-9 Lab ID No: AB29060 Matrix: Soil Collected: 12/18/98 by OTO Received on 12/21/98 by MBA QC and Data Review by Location: Atman-Northampton Client Job No: J0840517 Preservative: Refrigeration Container: 1 Clear Glass Jar Condition of Sample as Received: Satisfactory Delivered by Client Parameter Total Lead Total Lead EPA Method 6010200.7 Result (mg/Kg) MDL Digested Analyzed Analyst 47.2 0.458 12/29/98 12/30/98 DMM Sh _Special Handling;..__.__ CHAIN OF CUSTODY RECORD andardTAT- "° '°bttT %�I shtA T- 7t ,eify.ush TAT-Date Needed/r a 6/1.1> • All TATS subject to laboratory approval;mm. I /'� 24 hour notification needed for rushes. Page o • Samples disposed of after 60 days unless SPECTRUM ANALYTICAL ,,r� otherwised instructed. Report To: K<177) Invoice To: ACtrl j Project No.: 7—CALL — OS-1 7 •J Site Name:Ark-al C'fl Location: NJ�n/ h % tken fr b11 Slate: Project Mgr.: ISYVC P N P.O.No.: RQN: Sampler(s):dv\P ,lc Sa) 1=4° 5 2—HCl 3=41rSOt 4=HNOr 5—NaOH 6=MeOH 7= Containers: Analyses: Notes: fDW Qrinking Water GW=Ground Water WW=Waste Water C SO=S SL=Sludge 0=011 Xl= X2= ^ t b tc V Q l 'A G=Grab C=Composite to O u gz > C 0 w b v �� Lab Id: Sample Id: Date: rr Time: �' o, :, � Q i% Au?`1.6i“, !V/10n^ g, l��/o%ItT C S ' I I ✓ aeJg0)y7'/V hp S _ I - v Aa 9%0;8 Moho-3 I Allee `1 Mohb- 7 _ _ 1 . _ Y. - Al3r- UL.en, &oho- - _ 1 ✓ . Ahin`�%) Aloha-IV _ 1 ,i v_ v As,a41a‘ &to , b -I 1 I v- L...- V Anij40 A/oho -/Q 1 V - '' - - Au,A 1uk Vnho-I,i!]co a) v V AN I OCA/ahn-6b62-C) I v Additional Instructions: ��yy �Relinq�uished By: Received By: Date: Time: .7� r = idpo/%e ,ijj7/IR�4fstlRIntWSJLh /I `A( ;/,>--ced Nit request I . , PIW. a;-- -/ r ', I_45`-I /d •1/- y /0--.43—t 11 Almeren Drive•Aeawam.Massachusetts 01001 •413-789-9018•Fax 413-789-4076 Special Handling: 1 gie CHAIN OF CUSTODY RECORD Standard TAT-7 to 10 business days ❑ Rush TAT-Date Needed: • All TATS subject to laboratory approval;min. B 24 a hour notification id needed 60 for ru unless Page o£ • Samples disposed of after 60 days unless SPECTRUM ANALYTICAL ,(r —rte, �ottherwised instructed. Report To: (1� Invoice To: 11/41k(An/ Project No.: J S4—O�-17 Site Name: Minn 1'1 Location: (�if0%1-il et riPin 1 State: Project Mgr.: Br17(2- ^I P.O.No.: RQN: Sampler(s): MO Ji cc n ) 1=4° 2=HCI 3=H2SO4 4=11NO3 5=NaOH 6=MeOH 7= Containers: Analyses: Notes: N ill C7 3 • m O -9 m a� U I.a � � Lab Id. Sample Id: Date: Time: w` a u u ' "Ada A10h0-jr II II Alle16617 IVdIO4 1 i ABA90 AJ,Iha-1 '7 ! II k I.-- 1.--: 1 Apr7.c(t,7r otin —i An A9 ao AB AH Additional Instructions: By: Received By: Date: Time: X4.7" is/sO/9f- I I Lt A _ • -Al t. ■ PL Jac (11C 1A a- 11/01)..., ) If 1 Y 1_, /3 “l1 • I ,'Iii, II Almgren Drive•Agawam,Massachusetts 01001.413-789-9018•Fax 413-789-4076 IR SPECTRUM ANALYTICAL,INC. Massachusetts Certification M-MA 138 Connecticut Approval#PH 0777 Rhode Island#988c Maine#nla New Hampshire ID#2538 New York ID#11393 Florida HRS87448 O'Reilly, Talbot& Olrun Assoc. 293 Bridge Street Springfield, MA 01103 Attn: Bruce Nic&elsen Client Project No.: 1840517 Location: Atwood Drive January II, 1999 Lab TT) No Client ID Analysis Requested AH29697 NOHO-1 EPA Method 8260 Extractable Oil Hydrocarbons Soluble Lead Volatile Petroleum Hydrocarbons A129698 NOHO-10 Volatile Petroleum Hydrocarbons EPA Method 8260 Extractable Oil Hydrocarbons Soluble Lead ENVIRONMENTAL ANALYSES Presider aborato - Director 11 Almgren Drive •Agawam,Massachusetts 01001 • 413-789-9018 • FAX 413-789-4076 SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: NOH0-1 Lab ID No: AB29697 Matric Ground Water Sampled on1228/98 by OTO Received on 12/28/98 by MBA QC and Data Review by AM Location: Atwood Drive Client Job No.: J840517 Preservative: Refrigeration,HC1 Container : 2 VOA Vials Condition of Sample as Received: Satisfactory Delivered by Client Parameter for AB29697 Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene Volatile Organics EPA Method 8260 Result (ug/L) MDL Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Not detected 1.0 Analyzed Analyst 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN Continued next page... Parameter for AB29697 Volatile Organics EPA Method 8260 Result (ug/L) NIDL trans-1,3-Dichloropropene Not detected 1.0 Ethylbenzene Not detected 2.0 Hexachlorobutadiene Not detected 1.0 Isopropylbenzene Not detected 1.0 4-Isopropyltoluene Not detected 1.0 Methylene chloride Not detected 1.0 Naphthalene Not detected 4.0 n-Propylbenzene Not detected 1.0 Styrene Not detected 1.0 1,1,1,2-Tetrachloroethane Not detected 1.0 1,1,2,2-Tetrachloroethane Not detected 1.0 Tetrachloroethee Not detected 8.0 Toluene Not detected 3.0 1,2,3-Trichlorobenzene Not detected 1.0 1,2,4-Trichlorobenzene Not detected 1.0 1,1,1-Trichloroethane Not detected 1.0 1,1,2-Trichloroethane Not detected 1.0 Trichloroethene Not detected 1.0 Trichlorofluoromethane Not detected 1.0 1,2,3-Trichloropropane Not detected 1.0 1,2,4-Trimethylbenzene Not detected 4.0 1,3,5-Trimethylbenzene Not detected 2.0 m,p-Xylenes Not detected 2.0 o-Xylene Not detected 1.0 Vinyl chloride Not detected 1.0 Methyl-t-butyl ether Not detected 2.0 BFB Surrogate Recovery(%) 99 p-DFB Surrogate Recovery(%) 103 CLB-d5 Surrogate Recovery (%) 97 Analyzed Analyst 01/09/99 SN 01/09/99 SN 01'09/99 SN 01/09/99 SN 01/19/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01109/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN OL/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN SPECTRUM ANALYTICAL, INC. Laboratory Report Location: Atwood Drive Client Job No.: J840517 Client ID:NO11O-1 Lab ID No.:AB29697 Matrix: Ground Water Collected: 12/28/98by QTQ Received: 12/28/98by MBR Preservative: Refrigeration,HO Container: 2 VOA Vials Condition of Sample as Received:See Attached Sheet Volatile Petroleum Hydrocarbons MADEP VPH 97-12 Parameter for AB29697 Aliphatics/Aromatics (mg/L) C5-C8 Aliphatic Hydrocarbons C9-C12 Aliphatic Hydrocarbons C9-C10 Aromatic Hydrocarbons Unadjusted C5-C8 Aliphatics Unadjusted C9-C12 Aliphatics Target VPH Analytes (ug/L) Benzene Ethylbenzene Methyl-tert-butylether Naphthalene Toluene m,p-Xylenes o-Xylene Results MDL Not detected 0.150 Not detected 0.050 Not detected 0.050 Not detected 0.150 Not detected 0.050 Not detected 5.0 Not detected 5.0 Not detected 5.0 Not detected 5.0 Not detected 5.0 Not detected 5.0 Not detected 5.0 Analyzed Analyst 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN Dilution Factors Carbon Chain Dilution Factor 1 01/09/99 SN Target Analytes Dilution Factor 1 01/09/99 SN Surrogate Recoveries (%) 2,5-Dibromotoluene PID (%SR) 2,5-Dibromotoluene FID (%SR) 2,5-Dibromotoluene GCMS (%SR) 4-Bromofluorobenzene GCMS (%SR) NA NA 118 106 01/09/99 SN 01/09/99 SN 01/09/99 SN 01/09/99 SN Were all QA/QC procedures required by the VPH method followed? Yes No Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ( / No Were any significant modifications made to the VPH method,as specified in Section 11.3? Yes' ✓No ayes is answered to above question,then this sample was run via GCMS using all VPH method specified QC criteria I attest that b the materi inquiry of those individuals immediately responsible for obtaining the information, repo 1 ,to the best of my knowledge and belief,accurate and complete. / tory Director 01/11/99 SPECTRUM ANALYTICAL, INC. Laboratory Report Location: Atwood Drive Client Job No.: J840517 Client ID: NOHO-1 Lab ID No.:AB29697 Matrix: Ground Water Collected: 1228/986y OTO Received: 1228/98by MBR Preservative: Refrigeration/INO3 Container: 1 Amber/1 Plastic Condition of Sample as Received:See Attached Sheet Extractable Petroleum Hydrocarbons MADEP EPH 98-1,SW846 3510C Separatory Funnel Liquid-Liquid Extraction ParameterforAB29697 Aliphatics/Aromatics (mg/L) C9-C18 Aliphatic Hydrocarbons C19-C36 Aliphatic Hydrocarbons C11-C22 Aromatic Hydrocarbons Unadjusted C11-C22 Aromatics Diesel PAH Analytes (ug/L) Naphthalene 2-Methylnaphthalene Phenanthrene Acenaphthene Other Target PAH Analytes (ug/L) Acenaphthylene Anthracene Benzo (a) anthracene Benzo (a)pyrene Benzo (b) fluoranthene Benzo (g,h,i)perylene Benzo (k) fluoranthene Chrysene Dibenzo (a,h) anthracene Fluoranthene Fluorene Indeno (1,2,3-cd) pyrene Pyrene Dilution Factors Carbon Chain Dilution Factor Target Analyte Dilution Factor Results Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected 1 1 MDL 0.2 0.2 0.2 0.2 Extracted Analyzed Analyst 12/30/98 12/30/98 12/30/98 12/30/98 01/03/99 01/03/99 01/03/99 01/03/99 KS KS KS KS 10.0 12/30/98 01/03/99 KS 10.0 12/30/98 01/03/99 KS 10.0 12/30/98 01/03/99 KS 10.0 12/30/98 01/03/99 KS 10.0 12/30/98 01/03/99 KS 10.0 12/30/98 01/03/99 KS 10.0 12/30/98 01/03/99 KS 10.0 12/30/98 01/03/99 KS 10.0 12/30/98 01/03/99 KS 10.0 12/30/98 01/03/99 KS 10.0 12/30/98 01/03/99 KS 10.0 12/30/98 01/03/99 KS 10.0 12/30/98 01/03/99 KS 10.0 12/30/98 01/03/99 KS 10.0 12/30/98 01/03/99 KS 10.0 12/30/98 01/03/99 KS 10.0 12/30/98 01/03/99 KS 12/30/98 01/03/99 KS 12/30/98 01/03/99 KS Parameter for/0329697 Results Surrogate Recoveries (%) 1-Chloro-octadecane Aliphatic (%SR) 82 Ortho-Terphenyl Aromatic (%SR) 62 2-Bromonaphthalene Fractionation(%SR)43 2-Fluorobiphenyl Fractionation(%SR) 51 IVIDL Extracted Analyzed Analyst 12/30/98 12/30/98 12/30/98 12/30/98 01/03/99 01/03/99 01/03/99 01/03/99 KS KS KS KS Were all QA/QC procedures required by the EPH method followed? Yes No Were all performance/acceptance standards for required QA/QC procedures achieved? Yes C, No Were any significant modifications made to the EPH method,as specified in Section 11.3? Yes•, __No •If yes answered to above question,the aromatic hydrocarbons from C11-C22 along with target PAH aoalytes were performed via GC/MS following all EPH method specified QC criteria. I attest that based up>n ml inquiry of those individuals immediately responsible for obtaining the information, the best of my knowledge and belief,accurate and complete. 01/11/99 SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: NOH0-1 Lab ID No: AB29697 Matrix: Ground Water Collected: 1228/98 by OTO Received on 12/28/98 by MBR OC and Data Review by Location: Atwood Drive Client Job No: J840517 Preservative: RefrigerationlHNO3 Container: 1 Amber/1 Plastic Condition of Sample as Received: Satisfactory Delivered by Client Parameter Soluble Lead EPA Method 200.7 Result (mg/L) MDL Extracted Analyzed Analyst Soluble Lead nd 0.005 01/04/99 01/06/99 DMM Standard TAT-7 to 10 business days CHAIN OF CUSTODY RECORD ❑ Rush TAT-Date Needed: • All TATS subject to laboratory approval;min. glit 24 hour notification needed for rushes. Page / of I • Samples disposed of after 60 days unless otherwised instructed. SPECTRUM ANALYTICAL —17 -t-7 �(t Project No.: �—C`' I C Invoice To: 11/In rY nn II �_�r, Report To: Site Name; !1'-f U)vt� State: Location: c {_ RQN: Sampler(s) ccv Cc-WAN',1Phf? r- Project Mgr.: ` U(.-Q- k Sr- £ P.O.No.: Q Anal Analyses. Notes: =4°0(2=HC� 3=HaSOa �13N0��S=NT'a.�.,.OH 6=MeOH 7= Containers: y DW=Drinking Water °Ground Wa1 WW=Waste Water t7 i � SO=Sail SL=Sludge O=Oil X1= > M — Z CI ¢ p G=Grab C=Composite j a o pt, .� w d x o 0 0 o l_43 -.Cl) Ak Lab Id: Sample Id: Date: Time: , a cs * u se u GW Iy' 2 I ✓ V AB 1G 11` IA vN0—I I a6/(16 GW a�, 2 1 I V ABg`1(rrlis Nn1(10-IO N Ali An AB • • AB AB AB AB' - • -ced By: Date: Time: Relinquished By: bd6 Additional Instructions: �/�/[[//�� • I� b ,4 0 • II Almgren Drive•Agawam,Massachusetts 01001.413-789-9018•Fax 413-789-4076 SPECI'1�1M ANiLYTICAL,INC, Massachusetts Certification M-MA 138 Cooacedcut Approval#PH Rhode Island M 92&Mainz#n/e New Hasnpsbisz ID#2538 NewYoskID#11393 Florida HR587448 O'Reilly, Talbot a Okun Assoc. 293 Bridge Street Springfield MA 01103 Atut Bruce MakeLen Client Project No.: 30840517 Location: Abnan-Northampton February 3, 1999 1 7,TD Nn Client-1D_ A829057 NOH0-5 TO'd Anal3BeltEluac=1 TCZP Lead ENVIRONMENTAL ANALYSES 11 Maim Driva Agawam,Massachusetts 01001. 4l37$9-9018• FAX 413-7894076 FT:LT 66, V 957j - SPECTRUM ANALYTICAL,INC. Laboratory Report(Subcontracted Analysis) Location: Atman-Northampton Client Job No: J0840517 Preservative: Refrigeration Container. 1 Clear Glass Jar Semple as Received: Satisfactory o Client ID:NOHO-S Lab ID No: AB29057 Co llected:iut&9s OTO Received Data Reew AM Parameter TCLP Lead TCLP Lead EPA Method 1311/5W846 6019 Result(mg/L) MILL 6.07 ZOd £T:L1 66, b Clad Extracted Analyzed Analyst 0.010 02/01/99 02/03199 CR Spectrum Analytical,Inc. Laboratory Report Supplement Re eience Methods for the Dete+mination of Organic Compounds in Drinking Water. EPA-600/418/039. EMSL 1988. Methods for Chemical Analysis of Water and Wastes. EPA 600/4-79.020. EMSL 1983- Methods for Organic Chemical Analysis of Municipal and Industrial Wastewater. EPA 600/4-82-057. EMSL 1982 Test Methods for Evaluating Solid Waste. Physical/Chemical Methods. EPA SW-846. 1986. Standard Met hods for the Examinatinon of Water and Wastes. APHA-AWWA-WPCF. 1611vEdition. 1985. Standard Methods for Comparison of Waterborne Petroleum Oils by Gas Chromatography. ASTM D 3328. 1982. Oil Spill Identification System- U.S.Coast Guard CG-D-52-77. 1977. Handbook for Analytical Quality Control in Water and Wastewater Laboratories. EPA 60014-79-019- EMSL 1979. Choosing Cost-Effective QA/QC(Quality Assurance Quality Control)Programs for Chemical Anslyses. EPA 600/4-85/056. EMSL 1985. Report No ations Not Detected, The compound was not detected at a concentration equal to or above Not Pet,ND or nd the established method detection limit. NC = Nor Calculated MCL EPA Maximum Contamination Level VOA = Volatile Organic Analysis (An EPA 624 Surrogate) BFB = 4-Bromojfvarobenzene p-DEB . • 1,4-Diffuorobenrene (An EPA 624 Surrogate) Chforobenzene-d5 (An EPA 624 Surrogate) CLB BC? = (An EPA 601 Surrogate) BCP = a a,a T,-1 nrotoluene TFf = ¢,cep-T>�varotofuene (An EPA 602 Surrogate) Decachlorobiphenyl = (an EPA 60818080 Surrogate) DEfinisiam Surrogate Recovery—The recovery(expressed as a percent)of a non-method analyte(see surrogates listed above)added to the sample for the purpose of monitoring system performance. Matrix Spike Recovery=The recovery(expressed on analyte of to thod a alytes added to the sample for the purpose of determining any effect of sample composition Laboratory Replicate=Two sample aliquots taken in the analytical laboratory and analyzed separately with identical procedures. Analyses of laboratory duplicates give era as�Stf the procedures.S$ociated with or laboratory procedures,but not with sample collection,pr Field Duplicate Two separate samples collected at the same time and place under F d ntifc l circumstances t nce sand treated exactly the same throughout field and laboratory p well as duplicates laboratory give a measure of the precision associated with sample collection,preservaton and storage,as Relative Percent Difference(%RPD)=The precision measurement obtained on duplicate/replicate analyses. 4/4RPD is calculated as: %RPD v =rah el -vaLue2 ' 100% ave.value £0'd £T:LT 66. P gad ' LHandliyg CHAIN OF CUSTODY RECORD °ndard TAT-7 ol06uaiaeaad ush T Dale Needed .., .; IR All TATS subject to laboratory approval;min. 24 hour notification needed for rushes. Sl'FCIAUMAMALY7JCA1. Page / o� • Samples disposed of Thar 60days unless '-4j n othenvised instructed. Report To: 617?)C) Invoice To: W\CLI 9 Project No.: SOtSd-1 -• US I7 •J Site Name:A-f in Ofl Location: NotA-ha m cribn State: - ProecMg : O P.O.No.: RQN: Sampler(s); WL' 1LGSC ) 61=4Y 2=HCI 1=11350, 4=HNO, 5-NaOH 6=MeOH 7= Containers: Arses: Notes: I • • D eking Water CW.43round Water WW-Waste Water ` 2 /SO-Soi SL-Sludge O=Oil %I= %2= p 4 • 0.-Drab C=Composite a OQ �� 4 --( .d f, 2 i E a Leh Id: Sample Id: Date: Time: ,i' 4` o• a .6 Q !�� apdw4zGmai,, — a affelk , c Sot I 1 ✓ As 1C∎Cl fpho-5 1 V. u iVetf58 Noho-3 1 ✓ - Al1216/ MAO- 7 I ✓ , - *4So 0 yoho- 9 1 ✓ .i .ApalAt ftiolio 1 v. v ,,� 19i./1062 No h b -I I _ 1 v v v All a'ab3'Nohp -IQ 1 v v 1— ^"AO A/nhoBale9 1 V v I. Aoc7`005-eiaho-13d^(d!-s� 1 _ v 1/ ✓ Additional Instructions.J�C 1 4 S 5(.r Relinquished By: Received By: • Dale: Time: Sig v�qt i�ct g�, mil/1;741v �Gh � Ai 41- II Aril 11 A Infirm,Drive•A ammo, Maaarhmm is Al AM I•411-1119-90111•Par 411-7R9.41176 SPECTRU ANAlYTICAI,INC. Massachusetts Certification M-MA 138 Connecticut Approval#PH 0717 Rhode Island it 98&Maine#Na New Hominid=ID#2538 New Yerk ID#11393 Florida HRS87448 O'Reilly, Talbot&Okun Assoc. 293 Bridge Sirta:t Springfield,MA 01103 Attn: Bruce Nickebsen Client Project No.:70840517 Location:Atwood January 5, 1999 L'6 In No G7ient In A329860 MONO-a Analysis RTue_stad Total Load ENVIRONMENTAL ANALYSES II Magnet Drive •Agawam,Massachusetts 01001 • 413-789-9018 • FAX 413-789-40/6 T0' d £00' ON TS:VI 66,SO OE( : 131 SPECTRUM ANALYTICAL,INC. Laboratory Report Client ID:NOHO-S Location: Atwood Lab ID No: AB29860 Client Job No: J0840517 Mate Soil Collected: 12118N8 by OTO Received on 12/31198 by MDR QC and Data Review by Preservative: Refrigeration Container: 1 Clear Glass Jar Condition of Sample as Received: Satisfactory Delivered by Client Total Lead EPA Method 6010200.7 Parameter Result(mg/Hg) MDL Total Lead 159 0.470 ZO' d £00' °N ZS:VI 66, 50 laf Digested Analysed Analyst 01104198 01105A9 DMM 131 Spectrum Analytical,Inc. Laboratory Report Supplement R&M= M= Methods for the Determination of Organic Compounds in Drinking Water. EPA-600/4.88/039. EMSL 1988. Methods for Chemical Analysis of Water and Wastes. EPA 600/4.79020. EMSL 1983. Methods for Organic Chemical Analysis of Municipal and Industrial Wastewater. EPA 600/442-057. EMSL 1982. Test Methods for Evaluating Solid Waste. Physical/Chemical Methods. EPA SW-846. 1986. Standard Methods for the Examiratinon of Water and Wastes. APHA-AW WA-WPCF. 16th Edition- 19S5. Standard Methods for Comparison of Waterborne Petroleum Oils by Gas Chromatography. ASTM 0 3328. 1982. Oil Spill Identification System. U.S Coast Guard CG-D-52.77. 1977. Handbook for Analytical Quality Control in Water and Wastewater Laboratories- EPA 600/4.79419. EMSL 1979 Choosing Cost-Effective QA/QC(Quality Assurance/Quality Control)Programs for Chemical Anslyses. EPA 600/4-85/056. EMSL 1985. Retort Noations Not Detected, = The compound was not detected at a concentration equal to or above Not Det,ND or nd the established method detection limit NC = Not Calculated MCL = EPA Maximum Contamination Level VOA = Volatile Organic Analysis BFB = 4-Bromoflaorobenrane (An EPA 624 Surrogate) p-DFB = 1,4-Difluorobeneene (An EPA 624 Surrogate) CLB-d5 = ChlorobensenedS (An EPA 624 Surrogate) BCP = 2-Bromo-l-chloropropane (An EPA 60)Surrogate) TFT = a tea-Trtfluorotoluene (An EPA 602 Surrogate) DecachlorobiphenYl = (an EPA 608/8080 Surrogate) Definlllons Surrogate Recovery=The recovery(expressed as a percent)of a non-method analyte(see surrogates listed above)added to the sample for the purpose of monitoring system performance. Matrix Spike Recovery=The recovery(expressed as a percent)of method analyzes added to the sample for the purpose of determining any effect of sample composition on analyte recovery. Laboratory Replicate=Two sample aliquots taken in the analytical laboratory and analyzed separately with identical procedures. Analyses of laboratory duplicates give a measure of the precession associated with laboratory procedures,but not with sample collection,preservation,or storage procedures. Field Duplicate=Two separate samples collected at the same time and And place of Field identifical duplicates cu circumstances es and under treated exactly the same throughout field and collection,ptoep and storage,as well as with laboratory procedures. of the precision associated with sample collection,pre Relative Percent Difference(34 RPD)=The precision measurement obtained on duplicate/replicate analyses. %RPD is calculated as: %RPD a(value'-value2l• 100% ave.value £0' d 200' 0N ZS: VT 66. 50 upf : 131 Special Handling: ilik CHAIN OF CUSTODY RECORD DStandard TAT-7m I0 business ya Rush TAT-Date Needed:� s 9Fl • All T.ATs subject to laboratory jppro al;min. 24 hour m tilcation needed for msbes. Page of / • Samples disposed of after 60 days unless SPECTACMANALYDCRL otherwieed instructed. Report To: GTO Invoice To: MO• 1 Project No.'SC40 4 —or'�L 17 Site Name: 4t Lt )COC , Localion: Stale: _ y Project Mgr.: RVJ C P 14 P.O.No.: RQN: Sampler(s): ill • 4 I in && P 40CC 2=HCI 3=H,S0< 4=HNO, 5—NaOH 6=MeOH 7= Containers: Analyses: Notes: DW— raking Water GW4irouad Water WW—Waste Water '3lkSo SL-Sludge Oil XI— X2= V j a 4 I p a O='emb C=Conposite a 0 B a 4 Ci d O O O O Lab Id: Sample W: Date: Time: E d', I. x x : x t0a?4 44 Al0ho—X ieQft/lt So 1 i. >I * ' • V N 0 V Lc F ABV.. - U AB 1 U d _ C Additional Instructions: Relinquished B : „ ived By: Of Date: Time: c /Ii' A J al-.1 4 / /31h-9J is 4_, , L 11 Mom°Drive•Agawam,Mamchusetts01001 •411-789-9018•Fax 413-789.4076 SPECTRUM AN U' Massachusetts Certification PA-MA 138 Connecticut Rhode Island#98&Maine#n/a New Hampshire ID#1538 New York ID#I1393 Florida HRS87448 O'Reilly, Talbot& Okun Assoc. 293 Bridge Street Springfield, MA 01103 Attn. Bruce Nickelsen Client Project No.: J084 1,41:0D-No- c t`I77 AB32346 NOHO-101 Total Lead AB32348 NOHO-103 Total Lead .9B 32350 NOHO-105 Total Lead AB32353 NOH0-108 Total Lead NOH0-11 Conductance AB32356 ERA Method 8260 TPH by GC EPA Method 8270 NOHOCOMP Conductance AB32390 EPA Method 8260 TPH by GC EPA Method 8270 February 3, 1999 Location: Atwood ArawAhsassa.mated ENVIRONMENTAL ANALYSES 11 Almgren Drive• Agawam,Massachusetts 01001 • 413-789-9018• FAX 413-789-4076 SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID:NOHO-101 Lab ID No: AB32346 Matrix: Soil Collected: 01/29/99 by OTO Received on 0129/99 by MBR QC and Data Review by Location: Atwood Client Job No: J084 Preservative: Refrigeration Container: 1 Clear Glass Jar Condition of Sample as Received: Satisfactory Delivered by Client 'arameter tal Lead Total Lead EPA Method 6010/200.7 Result (mg/Kg) MDL Digested Analyzed Analyst 69.9 0.454 02/02/99 02/03/99 CR SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: NOHO-103 Lab ID No: A1332348 Matrix: Soil Collected: 01/29/99 by OTO Received on 0129/99 by MBA QC and Data Review by Location: Atwood Client Job No: J084 Preservative: Refrigeration Container: 1 Clear Glass Jar Condition of Sample as Received: Satisfactory Delivered by: Client 'arameter tal Lead Total Lead EPA Method 6010/200.7 Result (mg/Kg) MDL Digested Analyzed Analyst 10.2 0.454 02/02/99 02/03/99 CR SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: NOHO-105 Lab ID No: AB32350 Matrix Soil Collected: 01/29/99 by OTO Received on 0129/99 by MBR QC and Data Review by Location: Atwood Client Job No: J084 Preservative: Refrigeration Container: 1 Clear Glass Jar Condition of Sample as Received: Satisfactory Delivered by: Client arameter tal Lead Total Lead EPA Method 6010/200.7 Result (mg/Kg) MDL Digested Analyzed Analyst 9.26 0.450 02/02/99 02/03/99 CR SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: NOHO-108 Lab ID No: A1232353 Matrix: Soil Collected: 01/29/99 by OTO Received on 01/29/99 by MBR QC and Data Review by Location: Atwood Client Job No: J084 Preservative: Refrigeration Container: 1 Clear Glass Jar Condition of Sample as Received: Satisfactory Delivered by Client Total Lead EPA Method 6010/200.7 'arameter Result (mg/Kg) MDL Digested Analyzed Analyst tal Lead 10.9 0.447 02/02/99 02/03/99 CR SPECTRUM ANALYTICAL,INC. Laboratory Report Client ID: NOHO-11 Lab ID No: AB32356 Matrix: Soil Collected: 01/29/99 by OTO Received on 01/29/99 by MBR QC and Data Review by Location: Atwood Client Job No.: J084 Preservative: Refrigeration Container : 3 Clear Glass Jars Condition of Sample as Received: Satisfactory Delivered by: Client arameter for AB32356 maphthene maphthylene thracene lzidine izoic acid no (a) anthracene tzo (b) fluoranthene no(k)fluoranthene no(g,h,i) perylene no (a)pyrene nyl alcohol (2-chloroethoxy) methane (2-chloroethyl) ether (2-chloroisopropyl) ether (2-ethylhexyl)phthalate Iromophenyl phenyl ether tyl benzyl phthalate iloroaniline iloronaphthalene lloro-3-methylphenol ;hlorophenol ;hlorophenyl phenyl ether rysene )enz(a,h) anthracene ,enzofuran n-butylphthalate -Dichlorobenzene -Dichlorobenzene -Dichlorobenzene '-Dichlorobenzidine Semivolatile Organics EPA Method 8270 Result (ug/Kg) MDL Extracted Analyzed Analyst Not detected 151.0 02/02/99 02/03/99 KS Not detected 151.0 02/02/99 02/03/99 KS Not detected 151.0 02/02/99 02/03/99 KS Not detected 151.0 02/02/99 02/03/99 KS Not detected 755.0 02/02/99 02/03/99 KS Not detected 151.0 02/02/99 02/03/99 KS Not detected 151.0 02/02/99 02/03/99 KS Not detected 151.0 02/02/99 02/03/99 KS Not detected 151.0 02/02/99 02/03/99 KS Not detected 151.0 02/02/99 02/03/99 KS Not detected 302.0 02/02/99 02/03/99 KS Not detected 151.0 02/02/99 02/03/99 KS Not detected 151.0 02/02/99 02/03/99 KS Not detected 151.0 02/02/99 02/03/99 KS Not detected 1510.0 02/02/99 02/03/99 KS Not detected 151.0 02/02/99 02/03/99 KS Not detected 151.0 02/02/99 02/03/99 KS Not detected 302.0 02/02/99 02/03/99 KS Not detected 151.0 02/02/99 02/03/99 KS Not detected 302.0 02/02/99 02/03/99 KS Not detected 151.0 02/02/99 02/03/99 K5 Not detected 151.0 02/02/99 02/03/99 KS Not detected 151.0 02/02/99 02/03/99 KS Not detected 151.0 02/02/99 02/03/99 KS Not detected 151.0 02/02/99 02/03/99 KS Not detected 151.0 02/02/99 02/03/99 KS Not detected 151.0 02/02/99 02/03/99 KS Not detected 151.0 02/02/99 02/03/99 KS Not detected 151.0 02/02/99 02/03/99 KS Not detected 302.0 02/02/99 02/03/99 ICS Continued next page.. ammeter for AB32356 Result (ug/Kg) MDL Extracted Analyzed Analyst Dichlorophenol Not detected 151.0 02/02/99 02/03/99 KS Dichlorophenol Not detected 151.0 02/02/99 02/03/99 KS :thy] phthalate Not detected 151.0 02/02/99 02/03/99 KS -Dimethlylphenol Not detected 151.0 02/02/99 02/03/99 KS .Dinitro-2-methylphenol Not detected 755.0 02/02/99 02/03/99 KS -Dinitrophenol Not detected 755.0 02/02/99 02/03/99 KS -Dinitrotoluene Not detected 151.0 02/02/99 02/03/99 KS -Dinitrotoluene Not detected 151.0 02/02/99 02/03/99 KS •Diphenylhydrazine Not detected 151.0 02/02/99 02/03/99 KS n-Propylnitrosoamine Not detected 151.0 02/02/99 02/03/99 KS oranthene Not detected 151.0 02/02/99 02/03/99 KS orene Not detected 151.0 02/02/99 02/03/99 KS xachlorobenzene Not detected 151.0 02/02/99 02/03/99 KS xachlorobutadiene Not detected 151.0 02/02/99 02/03/99 KS xachlorocyclopentadiene Not detected 151.0 02/02/99 02/03/99 KS xachloroethane Not detected 151.0 02/02/99 02/03/99 KS leno (1,2,3-cd)pyrene Not detected 151.0 02/02/99 02/03/99 KS phorone Not detected 151.0 02/02/99 02/03/99 KS 4ethylnaphthalene Not detected 151.0 02/02/99 02/03/99 KS ilethylphenol (0-cresol) Not detected 151.0 02/02/99 02/03/99 KS dethylphenol (p-cresol) Not detected 151.0 02/02/99 02/03/99 KS phthalene Not detected 151.0 02/02/99 02/03/99 KS litroaniline Not detected 755.0 02/02/99 02/03/99 KS litroaniline Not detected 755.0 02/02/99 02/03/99 KS 4itroaniline Not detected 755.0 02/02/99 02/03/99 KS trobenzene Not detected 151.0 02/02/99 02/03/99 KS 4itrophenol Not detected 151.0 02/02/99 02/03/99 KS 4itrophenol Not detected 755.0 02/02/99 02/03/99 KS Nitrosodimethylamine Not detected 151.0 02/02/99 02/03/99 KS Nitrosodiphenylamine Not detected 151.0 02/02/99 02/03/99 KS ntachlorophenol Not detected 755.0 02/02/99 02/03/99 KS enanthrene Not detected 151.0 02/02/99 02/03/99 KS enol Not detected 151.0 02/02/99 02/03/99 KS rene Not detected 302.0 02/02/99 02/03/99 KS !,4-Trichlorobenzene Not detected 151.0 02/02/99 02/03/99 KS 1,5-Trichlorophenol Not detected 151.0 02/02/99 02/03/99 KS 1,6-Trichlorophenol Not detected 151.0 02/02/99 02/03/99 KS ridine Not detected 151.0 02/02/99 02/03/99 KS methyl phthalate Not detected 151.0 02/02/99 02/03/99 K5 i-n-octyl phthalate Not detected 151.0 02/02/99 02/03/99 KS Solids 86.4 0A 02/03/99 02/03/99 CD SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: NO110-11 Lab ID No.:AB32356 Matrix: Soil Collected:01/29/99 by OTO Received on 0129/99 by MBR QC and Data Review by Location: Atwood Client Job No.: J084 Preservative: Refrigeration Container: 1 Clear Glass Jar Condition of Sample as Received: Satisfactory Delivered by: Client Parameter for AB32356 Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroform 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dbromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane Volatile Organics EPA Method 8260 Result (ug/Kg) Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected MDL 31.8 31.8 31.8 31.8 31.8 31.8 31.8 31.8 31.8 31.8 31.8 31.8 31.8 31.8 31.8 31.8 31.8 31.8 31.8 31.8 31.8 31.8 31.8 31.8 31.8 31.8 31.8 31.8 Extracted Analyzed Analyst 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 CD CD CD CD CD CD CD CD CD CD CD CD CD CD CD CD CD CD CD CD CD CD CD CD CD CD Continued next page.. Parameter for AB32356 1,1-Dichloropropene :is-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Elexachlorobutadiene lsopropylbenzene 4-Isopropyltoluene Methylene chloride Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene m,p-Xylenes o-Xylene Methyl-t-butyl ether BFB Surrogate Recovery(%) p-DFB Surrogate Recovery(%) CLB-d5 Surrogate Recovery (%) % Solids Result(ug/Kg) MDL Not detected 31.8 Not detected 31.8 Not detected 31.8 Not detected 31.8 Not detected 63.6 Not detected 31.8 Not detected 31.8 Not detected 31.8 Not detected 63.6 Not detected 31.8 Not detected 31.8 Not detected 31.8 Not detected 31.8 Not detected 31.8 Not detected 31.8 Not detected 63.6 Not detected 63.6 Not detected 31.8 Not detected 31.8 Not detected 31.8 Not detected 31.8 Not detected 31.8 Not detected 31.8 Not detected 31.8 Not detected 63.6 Not detected 31.8 Not detected 31.8 104 104 100 86.4 0.1 Extracted Analyzed Analyst 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 CD CD CD 02/03/99 02/03/99 CD SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: NOHO-11 Lab ID No.:AB32356 Matrix: Soil Collected: 0129/99 by OTO Received on 01/29/99 by MBR QC and Data Review by Location: Atwood Client Job No.: J084 Preservative: Refrigeration Container: 3 Clear Glass Jars Condition of Sample as Received: Satisfactory Delivered by: Client ammeter 'otal Hydrocarbons(GC) Not detected Total Hydrocarbons by GC Modified EPA Method 8100 Result (mg/Kg) fingerprint based quantificaton: iasoline 'uel Oil #2 'uel Oil #4 'uel Oil #6 4otor Oil Igroin ,viation Fuel )ther Oil Jnidentified ro Solids Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected 86.4 MDL Extracted Analyzed Analyst 02/02/99 02/02/99 LR 40 02/02/99 02/02/99 LR 40 02/02/99 02/02/99 LR 40 02/02/99 02/02/99 LR 80 02/02/99 02/02/99 LR 80 02/02/99 02/02/99 LR 40 02/02/99 02/02/99 LR 40 02/02/99 02/02/99 LR 80 02/02/99 02/02/99 LR 02/02/99 02/02/99 LR 0.1 02/03/99 02/03/99 CD Petroleum identification is determined by comparing the GC fingerprint obtained from the sample with a library of GC fingerprints obtained from petroleum products. Possible match categories are as follows; Gasoline-includes regular,unleaded,premium,etc. Fuel Oil#2-includes home heating oil,#2 fuel oil and diesel. Fuel Oil#4-Includes#4 Fuel Oil. Fuel Oil#6-includes#6 oil and bunker"C"oil. Motor Oil-includes virgin and waste automobile. Ligroin-includes mineral spirits,petroleum naphtha,vm&p naphtha. Aviation Fuels-includes Kerosene,Jet A and JP-4. Other Oil-includes lubricating and cutting oil and silicon oil. Factors such as microbial degradation,weathering and solubility generally prevent specific identification within a petroleum category. A finding of"unidentified"means that the sample fingerprint was characteristic of a petroleum product,but could not be matched to a fingerprint in the library. After fingerprint identification,the amount present in the sample is quantified using a calibration curve prepared from a petroleum product of the same category as the identified petroleum. Unidentified petroleum is quantified using a petroleum calibration that approximates the distribution of compounds in the sample. A*in the results column indicates the petroleum calibration used to quantify unidentified samples. SPECTRUM ANALYTICAL, INC. Laboratory Report(Subcontracted Analyses) Client ID: NO11O-11 Lab ID No: AB32356 Matrie Soil Collected: 01/29/99 by OTO Received on 01/29/99 by MBR QC and Data Review by Location: Atwood Client Job No: J084 Preservative: Refrigeration Container: 3 Clear Glass Jars Condition of Sample as Received: Satisfactory Delivered by Client ameter iductance Result 20 Wet Chemistry Analyses MDL 1.0 Units Method Start Date Analyst umhos/cm S205/E120.1 02/01/99 PX SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: NOHOCOMP Lab ID No: AB32390 Matrix: Soil Collected: 01/29/99 by OTO Received on 01/29/99 by MBR QC and Data Review by Location: Atwood Client Job No.: J084 Preservative: Refrigeration Container : 2 Amber Glass Jars Condition of Sampple as Received: Satisfactory Delivered by Client Irameter for AB32390 naphthene naphthylene hracene zidine zoic acid ¢o (a) anthracene izo (b)fluoranthene zo (k) fluoranthene izo (g,h,i) perylene izo (a)pyrene izyl alcohol (2-chloroethoxy) methane (2-chloroethyl) ether (2-chloroisopropyl) ether (2-ethylhexyl)phthalate romophenyl phenyl ether yl benzyl phthalate :hloroaniline lloronaphthalene :hloro-3-methylphenol :hlorophenol 2tlorophenyl phenyl ether rysene tenz (a,h) anthracene ,enzofuran n-butylphthalate -Dichlorobenzene -Dichlorobenzene -Dichlorobenzene '-Dichlorobenzidine Semivolatile Organics EPA Method 8270 Result (ug/Kg) MDL Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not de tected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected 144.0 144.0 144.0 144.0 720.0 144.0 144.0 144.0 144.0 144.0 288.0 144.0 144.0 144.0 144.0 144.0 144.0 288.0 144.0 288.0 144.0 144.0 144.0 144.0 144.0 144.0 144.0 144.0 144.0 288.0 Extracted Analyzed Analyst 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS Continued Mitt page.. rameter for AB32390 Result (ug/Kg) MOL Extracted Analyzed Analyst Dichlorophenol Not detected 144.0 02/02/99 02/03/99 KS Dichlorophenol Not detected 144.0 02/02/99 02/03/99 KS hyl phthalate Not detected 144.0 02/02/99 02/03/99 K5 Dimethlylphenol Not detected 144.0 02/02/99 02/03/99 KS Dinitro-2-methylphenol Not detected 720.0 02/02/99 02/03/99 KS Dinitrophenol Not detected 720.0 02/02/99 02/03/99 KS Dinitrotoluene Not detected 144.0 02/02/99 02/03/99 KS Dinitrotoluene Not detected 144.0 02/02/99 02/03/99 KS Diphenylhydrazine Not detected 144.0 02/02/99 02/03/99 KS t-Propylnitrosoamine Not detected 144.0 02/02/99 02/03/99 KS )ranthene Not detected 144.0 02/02/99 02/03/99 KS )rene Not detected 144.0 02/02/99 02/03/99 K5 achlorobenzene Not detected 144.0 02/02/99 02/03/99 KS achlorobutadiene Not detected 144.0 02/02/99 02/03/99 KS achlorocyclopentadiene Not detected 144.0 02/02/99 02/03/99 KS achloroethane Not detected 144.0 02/02/99 02/03/99 KS mo (1,2,3-cd)pyrene Not detected 144.0 02/02/99 02/03/99 K5 )horone Not detected 144.0 02/02/99 02/03/99 KS ethylnaphthalene Not detected 144.0 02/02/99 02/03/99 KS ethylphenol (0-cresol) Not detected 144.0 02/02/99 02/03/99 K5 ethylphenol (p-cresol) Not detected 144.0 02/02/99 02/03/99 KS hthalene Not detected 144.0 02/02/99 02/03/99 KS itroaniline Not detected 720.0 02/02/99 02/03/99 K5 itroaniline Not detected 720.0 02/02/99 02/03/99 KS itroaniline Not detected 720.0 02/02/99 02/0399 KS tbenzene Not detected 144.0 02/02/99 02/03/99 KS itrophenol Not detected 144.0 02/02/99 02/03/99 KS itrophenol Not detected 720.0 02/02/99 02/03/99 KS ditrosodimethylamine Not detected 144.0 02/02/99 02/03/99 KS litrosodiphenylamine Not detected 144.0 02/02/99 02/0399 KS ltachlorophenol Not detected 720.0 02/02/99 02/03/99 KS :nanthrene Not detected 144.0 02/02/99 02/03/99 KS :nol Not detected 144.0 02/02/99 02/03/99 KS ene Not detected 288.0 02/02/99 02/03/99 KS 4-Trichlorobenzene Not detected 144.0 02/02/99 02/0399 Ks 5-Trichlorophenol Not detected 144.0 02/02/99 02/03/99 KS 6-Trichlorophenol Not detected 144.0 02/02/99 02/03/99 KS idine Not detected 144.0 02/02/99 02/03/99 KS nethyl phthalate Not detected 144.0 02/02/99 02/03/99 KS n-octyl phthalate Not detected 144.0 02/02/99 02/03/99 K5 Solids 89.7 0.1 02/03/99 02/03/99 GMM SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: NOHOCOMP Lab ID No.:AB32390 Matrix Soil Collected:01/29/99 by OTO Received on 01/29/99 by MBR QC and Data Review by Location: Atwood Client Job No.: J084 Preservative: Container: Condition of Sample as Received: Satisfactory Delivered by: Client ?ammeter for A1332390 3enzene 3romobenzene 3romochloromethane 3romodichloromethane 3romoform 1-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroform 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane Volatile Organics EPA Method 8260 Result (ug/lCg) Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected MOL 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 Extracted Analyzed Analyst 02/02/99 02/02/99 0) 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD Continued next page.. 'arameter for AB32390 ,1-Dichloropropene is-1,3-Dichloropropene rans-1,3-Dichloropropene ?thylbenzene 3exachlorobutadiene sopropylbenzene 1-Isopropyltoluene Kethylene chloride naphthalene 1-Propylbenzene ityrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene m,p-Xylenes o-Xylene Methyl-t-butyl ether Result (ug/Kg) MDL Not detected 6.1 Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected BFB Surrogate Recovery (%) 101 p-DFB Surrogate Recovery(%) 105 CLB-d5 Surrogate Recovery (%) 98 % Solids 89.7 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 12.2 6.1 6.1 0.1 Extracted Analyzed Analyst 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 CD CD CD 02/03/99 02/03/99 GMM SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: NOHOCOMP Lab ID No.:AB32390 Matrix: Soil Collected: 01/29/99 by OTO Received on 01/29/99 by MBR QC and Data Review by Location: Atwood Client Job No.: J084 Preservative: Refrigeration Container: 2 Amber Glass Jars Condition of Sample as Received: Satisfactory Delivered by Client Total Hydrocarbons by GC Modified EPA Method 8100 arameter otal Hydrocarbons (GC) ingerprint based quantificaton: lasoline uel Oil #2 uel Oil #4 uel Oil #6 lotor Oil .groin wiation Fuel )ther Oil Jnidentified to Solids Result (mg/Kg) Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected 89.7 MDL Extracted 02/02/99 Analyzed Analyst 02/02/99 LR 40 02/02/99 02/02/99 LR 40 02/02/99 02/02/99 LR 40 02/02/99 02/02/99 LR 80 02/02/99 02/02/99 LR 80 02/02/99 02/02/99 LR 40 02/02/99 02/02/99 LR 40 02/02/99 02/02/99 LR 80 02/02/99 02/02/99 LR 02/02/99 02/02/99 LR 0.1 02/03/99 02/03/99 GMM Petroleum identification is determined by comparing the GC fingerprint obtained from the sample with a library of GC fingerprints obtained from petroleum products. Possible match categories are as follows; Gasoline-includes regular,unleaded,premium,etc. Fuel Oil#2-includes home heating oil,#2 fuel oil and diesel. Fuel Oil#4-Includes#4 Fuel Oil. Fuel Oil#6-includes#6 oil and bunker"C"oil. Motor Oil-includes virgin and waste automobile. Ligroin-includes mineral spirits,petroleum naphtha,vm&p naphtha. Aviation Fuels-includes Kerosene,Jet A and JP-4. Other Oil-includes lubricating and cutting oil and silicon oil. Factors such as microbial degradation,weathering and solubility generally prevent specific identification within a petroleum category. A finding of"unidentified"means that the sample fingerprint was characteristic of a petroleum product,but could not be matched to a fingerprint in the library. After fingerprint identification,the amount present in the sample is quantified using a calibration curve prepared from a petroleum product of the same category as the identified petroleum. Unidentified petroleum is quantified using a petroleum calibration that approximates the distribution of compounds in the sample. A`in the results column indicates the petroleum calibration used to quantify unidentified samples. SPECTRUM ANALYTICAL, INC. Laboratory Report (Subcontracted Analyses) Client ID:NOHOCOMP Lab ID No: AB32390 Matrix: Soil Collected: 01/29/99 by OTO Received on 01/29/99 by MDR QC and Data Review by Location: Atwood Client Job No: J084 Preservative: Refrigeration Container: 2 Amber Glass Jars Condition of Sample as Received: Satisfactory Delivered by Client 'meter ductance Result 56 Wet Chemistry Analyses MDL Units Method Start Date Analyst 1.0 umhos/cm S205/E120.1 02/01/99 PX Spectrum Analytical, Inc. Laboratory Report Supplement References thods for the Determination of Organic Compounds in Drinking Water. EPA-600/4-88/039. EMSL 1988. thods for Chemical Analysis of Water and Wastes. EPA 600/4-79-020. EMSL 1983. :thods for Organic Chemical Analysis of Municipal and Industrial Wastewater. EPA 600/4-82-057. EMSL 1982. st Methods for Evaluating Solid Waste. Physical/Chemical Methods. EPA SW-846. 1986. mdard Methods for the Examinatinon of Water and Wastes. APHA-AWWA-WPCF. 16th Edition. 1985. mdard Methods for Comparison of Waterborne Petroleum Oils by Gas Chromatography. ASTM D 3328. 1982. 1 Spill Identification System. U.S.Coast Guard CG-D-52-77. 1977. mdbook for Analytical Quality Control in Water and Wastewater Laboratories. EPA 600/4-79-019. EMSL 1979. loosing Cost-Effective QA/QC(Quality Assurance/Quality Control)Programs for Chemical Anslyses. EPA 600/4-85/056. YISL 1985. Reoort Notations Not Detected, = The compound was not detected at a concentration equal to or above Not Det,ND or nd the established method detection limit. NC = Not Calculated MCL = EPA Maximums Contamination Level VOA = Volatile Organic Analysis BFB = 4-Bromofluorobenzene (An EPA 624 Surrogate) p-DFB = . 1,4-Diiluorobenzene (An EPA 624 Surrogate) CLB-d5 = Chlorobenzene-d5 (An EPA 624 Surrogate) BCP = 2-Bromo-l-chloropropane (An EPA 601 Surrogate) TFT = a,a,a-Trj luorotohrene (An EPA 602 Surrogate) Decachlorobiphenyl = (an EPA 608/8080 Surrogate) Definitions Surrogate Recovery=The recovery(expressed as a percent)of a non-method analyte(see surrogates listed above)added to the sample for the purpose of monitoring system performance. Matrix Spike Recovery=The recovery(expressed as a percent)of method analytes added to the sample for the purpose of determining any effect of sample composition on analyte recovery. Laboratory Replicate=Two sample aliquots taken in the analytical laboratory and analyzed separately with identical procedures. Analyses of laboratory duplicates give a measure of the preceision associated with laboratory procedures,but not with sample collection,preservation,or storage procedures. Field Duplicate=Two separate samples collected at the same time and place under identifical circumstances and treated exactly the same throughout field and laboratory procedures. Analysis of Field duplicates give a measure of the precision associated with sample collection,preservaton and storage,as well as with laboratory procedures. Relative Percent Difference(%RPD)=The precision measurement obtained on duplicate/replicate analyses. %RPD is calculated as: %RPD=(valuel -value21* 100% ave.value CHAIN OF CUSTODY IZhCUKll a aranaa - - u o L4})`Rush TAT T-Date Needed: WE 6• II TATs subject to laboratory approva 24 hour notification needed for rushes. Page / of • Samples disposed of after 60 days unless SPECTRUMAHALYTICAL ,t �� �/� 7 other-wised instructed. OTT) Invoice To: l�(t2� 1 t'l Project No.: �`�V Report To: ^ Site Name: t'l-1 F(s9C2UC Location: ,rA ( State: Project Mgr.: f�ice P.O.No.: RQN: Sampler(s): J('1 e (t C.\el-) SI (1=4°Q 2=HC1 3=1-1,S0• 4=HNO, 5=NaOH 6=Me0H 7= Containers: Analyses Notes: DW-Drinking Water GW=Ground Water WW=Waste Water H O id, 18 SO=Soil' SL=Sludge 0=Oi1 Xl= X2= ? A A H • cv 0 a • > d) G ) \C(1' ➢ G=Gmb G-Composite d` ZIA u fi a) x O O O O W d d vi Lab Id Sample Id: Date: Time: 2 µ, a x xt a x `...j V 3 hi a 1 SO 1 1 V'T` ✓ ✓ - ^YJ (\},x.t9 0.1\(uLFS,) Ash?lt Ut�I(7��b 1 v [.>✓0_.,Seti r. Ciz c'l—\ AR , ) ; �7 NoAt1 '1�. 1 . AR 7a',n I 17 si.-V-�'a.�i `�`'1) M4L(.A ✓ iz nlr11 I r9 ' AR ' ./B(< ` v. 7('' CO 1\in1 e1 7 Ncllo ID4/ 9 7 t er "�7 Cen„ix,�'iC- ftchto,-lot._ AB )3R{\ k o'10 /�, r AB,3:act L cA et W 1 y x 0e -ta i, ni4o MC, AB- zz 1 V � 1a aka ti�6- ru&e 0., A8✓A3) MlO�7 'Aet 1 V y- V ✓.s (vf G,,m, ,A"4++ bht 1 . r ` AR2�3cI�/'vr IJ } 1 (/ 8n�rr 0loo YeA 6 N. • AB d ? ctr1c71) 1 L-- x bn 644,Pit I1,0U )r,t,e, Date: 'h fu' 2•Al M Relinquished By: Received By: fr' Y1 rm�: Additional Instructions: /� 3' 7-- a>(' A Q cl L 4i iC QTIO-`�(A e LL4 , ,-294`. /1.:43-htiu ❑Fax results when available to( ) 11 Almgren Drive•Agawam,Massachusetts 01001 •413-789-9018•Fax 413-789-4076 CHAIN OF CUSTODY RE UKU ❑u RushTAT-Date Needed LS 7� • All TATs subject to laboratory approval;mm. IR 24 hour notification needed for rushes. Page a of D-- • Samples disposed of after 60 days unless SPECTRUM ANALYTICAL ,^' / ,t k 1 Fotherwised instructed. 1 - Report To: 0 .) Invoice To: NI a i Vy Project No.: tf /// Site Name: -"E'149 0 cc( / A Location: A r State: Project Mgr.: �[rZ GS Ai P.O.No.: RQN: Sampler(s): e c I rS r s 64°B! 2=HCI 3=H2SOa 4=HN01 S=NaOH 6=Me0H 7= Containers: Analyses: Notes: DW=Prinking Water GW=Ground Water W W=Waste Water y H .-S SL=Sludge O=Oil X1= X2= b i° ro O Z P. o a C G=Grab C=Composite E > Q U a , B x o 0 0 0 o q4 cc Lab Id: Sample Id: Date: Time: ',$ a a x x u V i 1- C, 1i L-4,--1 ( 1 �-P tu rr 4ato • I ,NJIr i, AB,j,�, b �D� o Cow P / I�1t i y q G , ( 7 7 V 1 1Ja1.,,-3, ♦uWL„-F B Ctnelfv.i� Fur C.vlwi 141 AB l AB e Aiii i...]7o i 7' rico AB t. W ICA 134 fr7 f-r,.)111 D AB AB . AB AB' Additional Instructions: Relinquished By: Received By: Date: Time: ❑Fax results when available to( ) I I Almgren Drive•Agawam,Massachusetts 01001 •413-789-9018•Fax 413-789-4076 SPECTRUM.ANALYTICAL,LNC. Massachusetts Certification M-MA 138 Connccticut Approval#PH 0777 Rhode Island#98&Maine#n/a New Hampshire ID#2538 New York ID#11393 Florida HRS87448 O'Reilly, Talbot&Okun 293 Bridge Street, Suite 500 Springfield, MA 01103 June 2, 1999 Client Project Not 84-05-17 Location: Atwood Drive - Northampton, MA Lab ID No AB44666 Client to STOCK-1 Analysis Re[11rwctrcl TCLP Lead or-ed.b u / bal •ye Presiden orator irector ENVIRONMENTAL ANALYSES I 1 Almgren Drive • Agawam,Massachusetts 01001 • 413-789-9018 • FAX 413-789-4076 SPECTRUM ANALYTICAL, INC. Laboratory Report(Subcontracted Analysis) Client ID: STOCK-1 Lab ID No: AB44666 Matrix: Soil Collected: 05/27/99 by OTO Received on 05/27/99 by KC QC and Data Review by MD Location: Atwood Drive-Northampton,MA Client Job No: 84-05-17 Preservative: Refrigeration Container: 1 Amber Glass Condition of Sample as Received: Satisfactory Delivered by: Client rameter P Lead TCLP Lead EPA Method 1311/SW846 6010 Result (mg/L) MDL 3.23 Extracted Analyzed Analyst 0.010 06/01/99 06/02/99 CR CHAIN OF CUSTODY REUUKll u Rush TAT-Date Needed: (.7///214/4 • All TATs subject to laboratory apyrovai;min. III 24 hour notification needed for rushes. Page(of / • Samples disposed of after 60 days unless SPECTRUM ANALYTICAL otherwised instructed. 0 Project No.: Ci c( i^)5 ( 7 Report To: ( �T Invoice To: (� 1 �i r Site Name: �kTOVnO"/, (JT. f 54 Location: Alf d`4k(Mve. rS-oan State:44LL Project Mgr.: A. It .< • • P.O.No.; RQN: Sampler(s): /f Adhr-(, " (144°C 2=HC1 3=H2SOs 4=HN0, 5=NaOH 6=MeOH 7= Containers: Analyses: Notes: DW=Drinking Water GW=Ground Water WW=Waste Water IT 0 IT SO=Sail Sf=Sludge 0 0i1 X1= X2= - A > C7 d = 'P G=Grab C=Composite i O E R n 1 i > d 0 w s' x O O O O iv Lab Id: Sample Id: Date: Time: $_ a w 4t 4t u bii .ABIAT104 S •Cue k- i .51;4://q1 C S! 1 / _ AB . AB AB- AB AB AB AB AB Additional Instructions:_ Relinquished B Received By: Date: Time: 7� I/l. ,t 4\ "'WAA,-cdttedera—_ IA 7/91 /G•7=07 ❑Fax results when available to( ) 11 Almgren Drive•Agawam,Massachusetts 01001 •413-789-9018•Fax 413-789-4076 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BILL OF LADING(pursuant to 310 CYR 4toos0 8WSC-o, Imams Taman/ �I LRA E. RECEIVING FACILITyfTEMPORARy STORAGE LOCATION(continued): Temporary Storage Address: Street City/Town. F. DESCRIPTION OF REMEDIATION WASTE: (check all that apply) ® Contaminated Media(circle all that apply): ❑ Contaminated Debris(circle all that apply): Inorganic Absrbant Materials Sate: Zip Code: GmuMwaaor Swims Water - Otter: Demoilion/Coastrurath Waste Vegetation/Organic Materials ❑ Non-hazardous 00000th nedzed Waste(drrde al that apply): Non-aqueous Phase Uquid Otter: ❑ Non-hazardous Containerized Waste(ekde al that apply): Tankeottms,Sludges Container: Drums Engineered Impoundments Other: - Type of CanbminaEan(circle al that apply): Gasoline Diesel Fuel *2 ell *4 Oil e6 OR Waste 01 kerosene Jet Fuel otter; Soil with lead above reportable standards Estimated Volume of Materials: Cubic Yank: 1 S - Tons: Other: Contaminant Source(check anaspecify): ❑ Transportation Accident ❑ Underground Storage Tank ®Omer. VA A wit w.A Response Actin Associated with Bill of Lading(circle rue): immediate Response Actin Release Abatement Measure Utility-Related Abatement Measure (linked Removal Action(LAA)-3/4) Comprehensive Response khan Other(specify): Remediaticn Waste Characterization Support Documentation attached: ❑ Sine History Information ❑ Sampling act Analytical Methods and Pbcedmes ❑ Laboratory Data ❑ Field Data paabueN to DEP.. If supporting dooumenthicn k not appended,provide an attachment stating the date and h comedian will what document such information was submitted - G. LICENSED SITE PROFESSIONAL(LSP)OPINION: - Name of Organization: O'Reilly. Talbot R (Alin Assnri at es LSp Name: Bruce R. Nickelsen Tdle: Assnriatp Telephone: 413 — 788 --6222 Ext attest that I have examined and am familiar MN lye hbnnaaoe mashed h Nis submittal,including any and documents accompanying all the sgrMani of care IO2((1)Ld in my pafmabnal spirant mid}agmencaasm upon application of (1)the applicable provisions of 309 CMR 4.02(2)and(3),and (inn the provisions of 309 CMR 4.03(5L - to the best of my knowledge,Information and belief,lye assessment actions undertaken b daractedxe Vie Remedtans° Waste which is(are)the subject of this submittal for awe coney with the •provisions of 310 CMR 40 0000,and aids facility p.nnptbd to accept Remediation Waste having he possible ones and described In this submittal. 1 am aware that significant penalties may remit,Including,but notlmkted b. pkomnent,k I submit kdommtlon wbIth 1 know b be false,Inaccurate or materially Incomplete. Signature: r AL VA' /,�.LC lfu Date: 9 /S. / 99 License Number. 9000 Seal: evsee 10/154 ms ram ISpromo on tecyaeo paper. id OF M 3 'kr/ BRUCE H o NICKELSEN No 9000 Fy• 9Fn'ISTE, Jf0SflE pROi • k Massachusetts Department of Environmental Protection L3WSC-012A 0....T tlip N.G.". Bureau of Waste Site Cleanup BILL OF LADING(pursuant to dtG CMR 48.aaw) ' • - LRA CATION OF SITE OR DISPOSAL SITE WHERE REMEDIATION WASTE WAS GENERATED: s Name(optional): Atwnnd naive Location Aid. End of Cul-de-sac Northampton ZIP Doris' 01060 _ wn: erica of Generation: 5 / 27 / 99 to /_ /_ _ nal Release Tracking Numbers Associated vdth this BIG of Lading: Note: El this Bill of Lading 1s the rest&d8 Limited Removal Action(LRA)taken prior to Notification,a Release Tracking Number knot needed. RSON CONDUCTING RESPONSE ACTION ASSOCIATED WITH BILL OF LADING: A Organization: city of Northampton of Contactwa Pp nen • Title. yno (`ity Hall 710 MainStre& _ iwn: Northampton stain: HA zp Code- 01060 one: 413 -587 - 1265 Ext. IELATIONSHIP TO RELEASE OR THREAT OF RELEASE OF PERSON CONDUCTING RESPONSE ACTION SSOCIATED WITH BILL OF LADING: '.one/specify) Owner Operator Generator Transporter Other RP: IP Shoofly(circle one): 'RP Specify one): Owner Operator Generator Transporter Other PRP: (circle an attachment the name,cornea iduciary/Secured Lender gency/Publiic Utility on a Right of Way Mier Person: )wnar and/or operator is not conducting the response action associated with the Bib of Lading,provide on n.address and telephone number,including any area ode and exwSon,far each,If known. RANSPORTER/COMMON CARRIER INFORMATION: /Gammon Canter Name: tie Ste S ie✓S d" So:a En c porter btPerson: lktdc Q,SJoS.e1't TNe: t Z2 C (1.a.rf;rrx IAA: ✓-c 0 f07 0 - town: C (%t cog t t State- ft-4 a zp Code- .L hone: I LLI— 59 3 - S'(5 ( Ext. IECEIVING FACILITY/TEMPORARY STORAGE LOCATION: abriFacety Name: City of Northampton Landf 111 act Person: Peter McEr lain - TNe: Health Agent It Board of Health, 210 MIN Street 01060 _ rown: Northampton State' MA Zip code: )hone:`fi — CS 7 - /, /\ Ea of FacaGly: • Aspaaf Batd✓Cok1 Mx • Landfill/Disposal ❑ Incinerator *one) 0 Asphalt Batch/Hot Aix k7 Landfill/Daily Cover • Temporary • Thermal Processing • Landfill/Structural RA ❑ Storage Other: :ion of Hazardous Division of SdId Waste 96-214-002 EPA ldentieration A Permit re Management Permit&:. 7, &: te/Class Period of Temporary Storage(specify dates if applicable): NA /_ /_ to _ /_ iaVAnedpated Temporary Storage(d applicable): NA son for sed 10(1/94 ins norm is pnnrea on recyc)ea paper. Page lo Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BILL OF LADING(pursuant to 310 t]4R 40.0030) BWSC-012A noawam«rareuaabon LRA TTIFlCATION OF PERSON CONDUCTING RESPONSE ACTION ASSOCIATED WRH THIS BILL OF LADING: under canaries of lax that I have personalty examined and am familiar with the hlwmation contained h Ids submittal,including any and meets accompanying this certification.and that,based on my Ingdry of Chose individuals Immediately responsible for obtaining the don,the matedal hbmatbn contained herein Is,to the best of my Ioaaandge and belief,bue,accurate and complete. I an aware that re signmcant penalties. including, but not limited to, possible fates and Imprisonment, for wilfully submitting false, Inaccurate, or eta,formation. re: Vri o'r %1 /" _ * Date: /L /447 Pt Person(print). w 14/NE M. FES- * As Agent for the City of Northampton .ed 10/194 1 ms form is punted on recycled paper. Page 3013 Massachusetts Department of Environmental Protection BWSC-0128 Bureau of Waste Site Cleanup aa.s Tracking Montan BILL OF LADING(pursuant to 310 CMR 4&0030) LRA LOG SHEET of W INFORMATION: 1: Signature of Transporter Representative: Receivin FaciRy/Temporery Storage Representative: A Shipment Time of Shipment Dale of Receipt Time of Receipt: /_7 /_a_4 : (circle ore)am/pm /__S- /___21 / : 1a- ___1_ _ _Z. rrac//ror L Registration: Trailer egistration (f any): (circle one)am/pm 0-0 O Load Size(cu.yds/bans): /S.(I ,I 1- r 1G 2: Signature of Transporter Representative: Receiving Facility/Temporary Storage Representative: if Shipment: Time of Shipment - Date of Receipt: Time of Receipt: / / (circle one)aMpm /_ /- _ tractor Registration: Trailer Registratico(if any): _ (circle one)am/pm Load Size(cu.yds/tons): i 3: Signature of Transporter Representative: Receiving Facility/Temporary Storage Representative: a Shipment: Time of Shipment: Date of Receipt: Time of Receipt /_ /_ (circle one)am/pm /_ / _ _ Tractor Registration: Trailer Registration(if any): (circle one)am/pm Load Size(cu.yds./tors): )4: Signature of Transporter Representative: Receiving Fadtiry/Temporary Storage Representative: at Shipment: Time of Shipment: Date of Receipt: Time of Receipt: /_ /_ (circle one)am/pm /_ /— — Tractor Registration: Trailer Registration(if any): (circle one)anVpn Load Size(cu.yds/tons): )5: Signature of Transporter Representative: Receiving Facility/temporary Storage Representative: of Shipment: Time of Shipment /_ /_ • _ (drde one)an/pm Tractor Registration: Trailer Registration Of any): Date of Receipt: Time 01 Receipt /_ /_ _ (circle one)am/pm Load Size(cu.ydsJQih): D 6: Signature of Transporter Representative: - of Shipment: Time of Shipment /_ /_ _ (circle one)arn/pm /Tractor Registration: Trailer Registration Of any): Receiving FacmryRempomry Storage Representative: Data of Receipt: Time of Receipt /— /_ • _ (circle one)ampm Load Size(cu.yds/tons): D 7: Signanre of Transporter Representative: Receiving Facility/Temporary Storage Representative: i of Shipment: Time of Shipment /_ /_ (circle one)am/pm . iTractor Registration: Trailer Registration()f any): Date of Receipt: Time of Receipt /_ /— • _ (drde one)am/pm Load Size(cu.yds/tons): .0G SHEET VOLUME INFORMATION: Total Volume This Page(cu yds.rtans): Total Carried Forward(cu yds/tons): Total Carded Forward and This Page(cu.ydsltons): ;ad 10/1434 11713 1033115 prnea tin/9CyU6o paper. Page 1 of 1 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BILL OF LADING(Pursuant to 310 CMR 40.0030) SUMMARY SHEET ❑-I BWSC-012 RS.a..Tt.npNurn LRA L ACKNOWLEDGEMENT OF RECEIPT OF REMEDIATION WASTE AT RECEIVING FACILITY OR TEMPORARY STORAGE LOCATION: Receiving Location Reprersentatl'w(pr a : o fl % /r MP(` � 04-NdFiL`-1me: Signature: Date: —L/y /i M. ACKNOWLEDGEMENT OF SHIPMENT AND RECEIPT OF REMEDIATION WASTE BY PERSON CONDUCTING RESPONSE ACTION ASSOCIATED WITH THIS BILL OF LADING: 1 certify under penalties of law that 1 have pasonany examined and am laminar with tie bktmation oomained N is submittal,including any alp all documents accompanying this cemacanon, and Mat, based on my Inquiry of those Individuals Immediately responsible or obtaining Me information,the melarht intimation contained harem Is.to the best of my knowledge and belief,mire.accurate and complete. 1 am aware that acre area significant pomades,des. h• but not 6nRed to, possible fines and impdsormant. or wilfully submitting false, inaccurate, or Signature: 71-{R"rL .0 Dare: /_ /-17 Name of Person(prat): FR4r'/K 3 frARA y((i 4-1/ Revised 10/1/94 fns TOM s pnntea m recyaaa paper. Page 2 Massachusetts Department of Environmental Protection of Waste Site Cleanup OF LADING(Pursuant to 310 CMR 40.0030) SHEET • of BWSC-01 2C R.w..n.asN Numb.: Bureau BILL SUMMARY LRA iUMMARY OF SHIPMENTS: E OF SHIPMENT: DATE OF RECEIPT: NUMBER OF LOADS SHIPPED: DAILY VOLUME SHIPPED(CU.YDS/TONS): • SUMMARY L OF LADING TOTALSHIPPED SHEET TOTAL SHIPPED: (only it different): _ ___---_...._.,_...—. OrNa 1 n(, sed 10/194 r Iran No: 12218 NORTHAMPTON Date 09/09/9`7 ON REV . LANDFILL Time in 13: 32 mos 210 NORTHAMPTON ,OT . NORTHAMPTON , MA 01060 Time out 13 : 44 Gross- 68680 ma CUS OME 0025 care : 37040 CUSTOMER CO25 CLEAN FILL. Net : 2,1.040 OWNER CO28 CLEAN FILL. HAULER 0025 CLEAN FILL aTiAIEkIAL 07 CLEAN FILL Net onF;: ]_ 82 Price/Ton - 0 ea 7perator FRANK KARAKULA r t lo Char 6;r: 0 .00 Comment /-i�/'-� ��'//I/�,' b1'riff t u rte' C_ l imm ma ims ow v Tran No : 12218 NORTHAMPTON REG. LANDFILL Date 09/09799 210 MAIN ST . Time in 13 :32 NORTHAMPTON , MA 01060 Time out 13 : 44 Gross: 66680 CUSfOME 0025 Tare: 37040 OWNER 0025 CLEAN FILL Net: 31640 OWNt:R 8025 CLEAN FILL Net: HAULLR 0025 CLEAN FILL GLEAN FILL Net Tons: 15 .88 MATERIAL 07 Price/Ton . 0 .00 Operator FRANK KARAKULA lot Char na 0 .00 Comment , r �� J//� Signature _,_ :N` .A� 1 " _` - ' " .__ • o • • WASTE MANAGEMENT [ 310N MICHIGAN DEPARTMEN i OF — ENVIRONMENTAL QUALITY Pan 121 of wet 451,1091 ais amended. • Failure to file may subject you to DO NOY'WRITE IN THIS 5..,CE criminal and/or civil penalties under Sections 32611151 or 324.12116 MCL. ATT.D DIS. D REJ. 0 PR.D Form App oved. OMB No.2050.0039 or type. in UNIFORM HAZARDOUS WASTE MANIFEST L GitinaIlgYS U3IEPA ID No. Manifest Wl1iQUUV105 2 D t No. 8i 2. Page 1 of 1 Information in the shaded areas law.not required by Federal cfY6r RuG 1d big A to, � p, z F✓ A State Manliest Document Number MI 7404681 210 HAIN ST. NORTHAMPTON, MA 01060 Generator's Phone I 413 1 587-1265 B. State Generators ID : A't OD DR. NORTHAMPTON, MA Transporter 1 Com any Name 6. US EPA ID N bet OIL RECOVERY CORP. ` HAD 985 294 693 C. State Transporter ID D.Transporters Ptione419L737-2949 Transporter 2 Company Name 8. US EPA ID Number 1 E. State Transporters ID F.,Transperter'c Phone . Desi noted Facili Name and Site C�f—HE'I SSItVICHS INC. Address 10. US EPA ID Number G $fate Facility's ID rAw 2 4,b+r., - 18550 ALLEN ROAD BROWNSTOWN, MI 48192 I HID 096 963 194 H. Facility's Phone 2/ 73F-282-9250 , . Proper Shipping 1. US DOT Description (including 1D NUMBER). Name, Hazard Class,and 12.Containers No. Type 13. Total Quantity 14 Unit WWoI 1 Waste No. �,, HM RQ,NAZARDODS WASTE SOLID, N.O.S..(D008,LEAD),9, RA3077 PG III oo5cf o60,000� . .: „., noo8 G .. . .. _.. . .. ...; '.,IK Handing Case: J. Add"d'�1 al scriptions for Matenal l� S`/.z-0 b C 15. Special Handling Instructions and Add bona/Information f ERG 1#171 24 8H. PHONE:617-523-7740 SEND COPY OF NAND% W/INV. 16. GENERATORS CERTIFICATION:I hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and are classified, packed,marked,and labeled,and are in all respects m proper condition fort ansport by highway according to applicable international and national government regulations- If 1 am a large quantity generator, 1 certify that I have a program in pi ce to reduce the volume and toxicity of waste generated to the degree I have determined to be economically practicable and that I have selected the racticable method of treatment, storage, r disposal p currently available to m which minimizes iz s the present cand future threat to human health and the environment; OR; i I am a small quantity generator, I have made a good faith effort to min. my ware generation and select the best waste management method that is available to me and that I can afford. Date Printed/Typed Name Lifyrze -o:o:. 45 47t"l . c -/ 17. Tran}porter 1 Acknowle emen)of Receipt of M'^ -'° Prihted/FYP;' Signature Month Day Year h A-=I AA ) Date Sign 18. Transporter 2 Acknowledgement a Receipt of Material Printed/Typed Name D Signature Month Day Year IIIIII 9. Discrepancy Indication Space 20. Facility Owner or Operator:Certification of receipt of hazardous materials covered by this manifest except as noted Item 19. Printed/Typed Name Signature Date Month Day Year CHEM-MET SERVICES -•■• 18550 ALLEN ROAD BROWNSTOWN, MI 48192 c , #. 046142 Phone: 734-282-9250 EPA#MID096963194 CERTIFICATE OF DISPOSAL This certifies that the waste(s) specified on MANIFEST NUMBER : 14174046 81 AND TRANSPORTER: MRD985^94693 OIL RECOVERY CORPORATION ?OR GENERATOR: MAR000010512 NORTHHRMPTION, CITY OF 201 MAIN ST. RTWOOD DR. NORTHHRMPTON, MR 01060 las been properly disposed of under the authority of all required and applicable permits and licenses, :o my best knowledge and belief based on my inquiry of individuals immediately responsible for the waste disposal. The waste identified above has been handled in compliance with one or more of the applicable performance standards specified in 40 CFR, part 268, subpart D and all applicable prohibitions set forth in 40 CFR 268.32 or RCRA section 3004 (d). Signature: Date: 09-30-1999 WHOLLY OWNED SUBSIDIARY OF PERMA-FIX ENVIRONMENTAL SERVICES, INC.