Contaminated Soil 1999 EnvironmentalSafetyHealthGeotechnical
t
O'Reilly, Talbot & Okun —r
[ A S S O C I A T E S ]
November 3, 1999
File No.J84-05-17
Mr.Peter McErlain
Office of Planning and Development
City Hall
210 Main Street
Northampton,MA 01060
Re: Limited Removal Action
Atwood Drive
Northampton, MA
Dear Mr.McErlain:
293 Bridge Street
Suite 500
Springfield MA 01103
Tel 413 788 6222
Fax 413 7B8 8830
Email orete @oto-env com
This letter documents completion of a Limited Removal Action (LRA) as defined in the Massachusetts
Contingency Plan (310 CMR 40.0318) to remove lead contaminated soil from the above referenced
property in Northampton, Massachusetts. Our report is subject to the limitations attached in
Appendix A.
Background
A site locus and site plan are provided as Figures 1 and 2 respectively. An environmental site
assessment performed by O'Reilly, Talbot & Okun Associates, Inc. (OTO) for a perspective leasee
indicated that fill material was likely present on the Atwood Drive property. A series of test pits was
performed on the property, which included analytical testing of the fill material. The fill material was
tested for Extractable Petroleum Hydrocarbons (EPH), polychlorinated byphenols (PCBs) and RCRA
8 metals. Location Test Pit 1 (TP-1) contained approximately 2.5 feet of granular fill with
concentrations of lead at 347 mg/kg, above the applicable Reportable Concentration (RCS-1) for total
lead of 300 mg/kg. No EPH or PCB compounds were detected above Reportable Concentrations. A
copy of the test pit log for TP-I is provided in Appendix B Analytical data are summarized in Table I
and analytical data sheets are provided in Appendix C. We understand that the City of Northampton
was notified of concentrations of lead in site soil above reportable concentrations by facsimile letter
dated February 3, 1999
Additional Fill Characterization
The extent of lead impacted soil around TP-1 was further characterized through a boring program
performed December 18, 1998 and January 29, 1999. Ten additional soil samples were collected on
these dates and analyzed for total lead. The results are summarized in Table 1. The locations of
samples (NOHO-2,3,5,7,8,9,101,103,105, and 108) and results of total lead analyses are shown on
Figure 2. Each of these samples was collected from the fill material within 2.0 to 2.5 feet of the ground
surface, with the exception of NOHO-9, which was collected from the natural soil material
underlying the fill. Soil sample NOHO-5 had the highest total lead concentration at 783 mg/kg. The
T
O'Reilly, Talbot & Okun 4-COW-4
[ A S S O C I A T E S ]
NOHO-5 sample was tested for leachable lead by the Toxicity Characteristic Leaching Procedure
(TCLP) and found to contain a leachable lead concentration of 6.07 mg/I,which exceeded the 5.0 mg/I
standard defining a characteristically hazardous waste.
Based on the analytical data, an area of lead contaminated soil of approximately 20 cubic yards was
identified as shown on Figure 2.
Groundwater Characterization
In addition to fill characterization, a groundwater monitoring well (NOHO-1) was installed adjacent
to test pit TP-1 (approximately 15 feet south in the inferred downgradient groundwater flow direction)
to evaluate potential groundwater impacts. The well was installed on December 18, 1999 in a boring
drilled to a depth of 24 feet. The monitoring well installation and subsurface conditions encountered
are shown on the boring log attached in Appendix B.
Soil samples were collected by split spoon using standard penetration tests continuously to depths of
15 feet and screened for VOCs with the PID. No VOCs were detected. Soil conditions consisted of
granular fill to a depth of 2 feet, followed by fine to medium sand, with trace amounts of silt Thin (1
to 2 inch thick) layers of clay were observed below 10 feet. Groundwater was encountered at a depth
of approximately 18 feet.
On December 28, 1998 a groundwater sample was collected from the monitoring well. The groundwa-
ter sample was collected using an individually dedicated disposable plastic bailer. Prior to sample
collection three to five times the volume of standing water in the well was removed to provide a
sample of formation water in the well for collection. Groundwater samples were than collected into
pre-preserved bottles for analysis for Extractable and Volatile Petroleum Hydrocarbons (EPH/VPH)
Volatile Organic Compounds (VOCs) and dissolved lead. The dissolved lead sample was filtered prior
to preservation to remove sediment. The analytical data sheets for the groundwater analyses are also
attached in Appendix C. As shown, no contaminants were detected in the groundwater samples.
A groundwater sample was also screened in the field for pH and specific conductance. The pH reading
was 6.5 and the specific conductance reading was 290. These values are within the range typical for this
geographic region.
Limited Removal Action Excavation
The lead contaminated soils were excavated by CT Environmental, Inc. of Longmeadow,
Massachusetts on May 27, 1999. The excavation was observed by Bruce H. Nickelsen of O'Reilly,
Talbot & Okun Associates, Inc. The soils were excavated to a depth of 2.5 feet (the depth of fill) and
to the lateral limits shown on Figure 2. Excavated soils were placed on top of and covered with plastic
sheeting. Approximately 5 cubic yards was excavated from the vicinity of the NOHO-5 sample
location, which had been found to be characteristically hazardous based on TCLP testing. The
remaining approximately 15 cubic yards of soil were excavated and stockpiled separately. A soil sample
was collected from the 15 cubic yard pile (STOCK-1) and analyzed for TCLP lead. A concentration of
3.23 mg/I of leachable lead was detected from this sample, indicating the 15 cubic yards pile of soil was
not a characteristically hazardous waste.
Page 2
O'Reilly, Talbot & Okun ~C=1.4-4
( A S S U C I A r E S I
Sail Disposal
On September 9, 1999, the 15 cubic yard stockpile was transported to the Northampton Landfill for
use as daily cover under a Massachusetts Bill of Lading. The Bill of Lading is attached in Appendix D.
The 5 cubic yard pile was transported to Chem-Met Services, Inc. of Brownstown, Michigan for
disposal in their hazardous waste landfill. A copy of the hazardous waste manifest showing this
disposal is attached in Appendix D.Both Bill of Lading and hazardous waste manifest were signed by a
representative of the City of Northampton as generator of the waste material.
Conclusions
Based on the investigations and analytical test results described in this letter lead impacted soil has
been removed from the vicinity of the TP-1 location to levels below applicable Reportable
Concentrations. Given that soils which exceed applicable reportable concentrations have been
removed, no further actions are warranted under the MCP, other then maintenance of this
documentation report for a period of five years as required under 310 CMR 40.0318. You should sign
section M of the last page of the original Bill Of Lading,and keep it with your records.
It has been our pleasure to work with you on this project. Please feel free to call us if you have any
questions or comments.
Very truly yours,
O'Reilly,Talbot&Okun Associates,Inc.
�l._,/t(,L&t 11/1,1a/tit
Bruce H. Nickelsen
Associate
cc Wayne Fe den
Attachments: Figures
Tables
Appendix A
Appendix B-
Appendix C
Appendix D
-Limitation
Test Pit/Boring Logs
-Analytical Data
-Bill of Lading, Manifest
Page 3
Kevin J. O'Reilly
Principal
Table I
Soil Quality Data Atwood Drive
r "„ TP:l/S."1 s®H0.2 IOHs QRO5 NOHO-1 NO °4 e e OHO- =14(*D e o e O...'77 k:`
t a i 02 fy. 104�" rations
i wx
Depth;- E ' . .` a7 .v o-- a". axa '. Aa'2„O it .::"
® Coll . 0 xxft ..' ,n), .
t e t �w; t o " a° ni) °mss ND3a.: °tiND£ ° @y:NOD l rip?,s ?m
EPfi mB,.�) .ti"� 'tn. W Si.._ . , t$ . ,. ..
Aliphatics/Aromatics ND NA NA NA NA NA NA NA NA NA NA Various
Targeted PAH's Analytes(mg/Kg)
Fluoranthene ND NA NA NA NA NA NA NA NA NA NA 1,000
Phenanthrene ND NA NA NA NA NA NA NA NA NA NA 100
Pyrene ND NA NA NA NA NA NA NA NA NA NA 700
PCB-1254 0.75 NA NA NA NA NA NA NA NA NA NA 2
KCRA�SJ TALS.(tng/ 3'r-'! . . 34' .. .S.3" ei4x .8z. .=i333 . e _3 357'3337 y133 '. ,.: .r_. ?. ""*s'.'.`::,:..:
Total Barium 51.3 NA NA NA NA NA NA NA NA NA NA 1,000
Total Chromium 13.8 NA NA NA NA NA NA NA NA NA NA 1,000
Total Lead 3473 163 69 783 73 159 47.2 69.9 10.2 9.26 10.9 300
TCLP Lead NA NA NA 6.07 NA NA NA NA NA NA NA N/A
i Samples were screened for Volatile Organic Compounds(VOCs)with a Photoionization Detector(PID).
l "ND" indicates Not Detected. Only detected analytes are shown. "NA" indicates Not Analyzed.N/A indicates Not Applicable.
J Following receipt of analytical results,this sample was composited by the laboratory,and three separate aliquots of soil analyzed for total
lead.The results of this analysis indicated total lead readings of 380,302,and 474 mg/kg total lead.
\\Main\data\Bruce Nickelsen\atwooddrive table 1.lwp
O'Reilly, Talbot & Okun Associates, Inc.
Atwood Drive
Northampton, Massachusetts
Site Locus
October 1999 Figure 1
N
O'Reilly, Talbot & Okun
[ A S S O C I A T E S ]
1
LIMITATIONS
1. The observations presented in this report were made under the conditions
described herein. The conclusions presented in this report were based solely upon
the services described in the report and not on scientific tasks or procedures
beyond the scope of the project or the time and budgetary constraints imposed by
the client.
2. In preparing the report O'Reilly, Talbot, Okun & Associates Inc relied on
certain information provided by state and local officials and other parties
referenced herein and on information contained in the files of state or local
regulatory agencies. Although there may have been some degree of overlap in the
information provided by these sources, O'Reilly,Talbot, Okun&Associates, Inc.
did not attempt to independently verify the accuracy or completeness of all
information reviewed or received during the course of this assessment.
3. Observations were made of the site and of the structures on the site as indicated
within the report. Where access to portions of the site or to structures on the site
was unavailable or limited, we render no opinion as to the presence or hazardous
materials or oil, or to the presence of indirect information relating to hazardous
materials or oil in that portion of the site. In addition, we render no opinion as to
the presence of hazardous materials or oil, where direct observations of portions
of the site where obstructed by objects or coverings on or over these surfaces.
4. Unless otherwise specified in the Report, we did not perform testing or analyses
to determine the presence or concentration or concentration of asbestos or
polychlorinated biphenyls (PCBs) at the site or in the environment at the site.
5. The purpose of this Report was to assess the physical characteristics of the subject
site with respect to the presence of oil or hazardous material (OHM) in soil or
groundwater at the site, and to assess risks associated with detected OHM, within
the meaning of the Massachusetts Contingency Plan, 310 CMR 40.0000. No
specific attempt was made to check on the compliance of present or past owners
or operators of the site with federal, state, or local laws and regulations,
environmental or otherwise.
6. Risk assessment was performed in accordance with generally accepted practices of
government agencies and other consultants conducting similar characterizations.
The findings of the risk characterization are dependent on numerous assumptions
and uncertainties inherent in the risk assessment process. Therefore, the findings
of the risk assessment should not be interpreted as an absolute characterization of
actual risks, but as general indicators highlighting potential sources of risk at the
site. Although the range of uncertainty in the risk characterization has not (and
cannot) be quantified, the use of conservative assumptions throughout the process
would be expected to err on the side of protection of human health and the
environment.
7. Where analytical data or information regarding site environmental conditions was
unavailable or limited, we render no opinion as to risks due to oil or hazardous
materials in those portions of the site, or to oil or hazardous materials not tested
for.
8. Our report was prepared for the exclusive benefit of our client. Reliance upon
the report and its conclusions is not extended to third parties or future property
owners. We acknowledge copies of our report may be submitted to DEP for
MCP compliance purposes.
O'Reilly, Talbot & Okun Associates, Inc.
293 Bridge Street, Suite 500
Springfield,Massachusetts. 01103
(413)-788-6222
PROJECT
Description: Atwood Drive
Location: Northhampton, MA
Test Pit No. TP-1
Job No. 084-5-17
Date: 06/23/98
Engineer/Geologist:
Weather:
Bruce Nickelsen Contractor: Gary Guertin Ex.
Overcast, 70's Backhoe: Case 580
Capacity: 1/2 yard cubic yard
Ground Elev:
Start:
Finish:
9:10
9:30
DEPTH
SOIL DESCRIPTION
EXCAV.
EFFORT
BOULDER
COUNT
PID
REMARKS
5
Brown Fine to Medium sand with some brick fragments(Fill)
E
None
1
S-1 =ND
2.5'
Sample S-1 collected from 0-2.5 feet
Natural Brown Fine Sand,trace silt.
Sample S-2, collected from 8'
E
None
S-2 =ND
10
8.0 End of Exploration
REMARKS:
1. Samples screened with TEl 580B Photoionization detecto r, referenced to part per million(PPM)
2. Soil at 8'was moist.
benzene
in air.
PLAN
Vol. =
LEGEND
EFFORT
E=Easy
M=Moderate
D=Difficult
O'REILLY, TALBOT& O%UN ASSOCIATES, INC
ENVIRONMENTAL AND GEOTECHNICAL ENGINEERING CONSULTANTS
LOG OF BORING NOHO—I
SHEET I OF I
IOJECT Atwood Drive
°CATION
31LUNG COMPACTOR Seaboard
IFORS(&N Jeff N. i DATE STARTED
12/1898
DATE FINISHED
13/18/98
KILLING EQUIPMENT BS) ''COMPLETION DEPTH
1 240
GROUND SURFACE ELEV.
DAIUM
YPE BR RSA.
SIZE@MEOE COPE
BAMEL ''.,NO.SA.W 7 DIST. UNDIST.
ASINO I'
TIME
FIRST COMPL.
1 110.
ASING HAtbt WEIGHT I DROP I WATER LEVEL(FT)
\MPLER 21/a Split Spoon i HORMO NoM
12 feet South of TP-1
9MPLER
AMMER
WEIGHT IGO pound
DROP
30inde
I LOCATION
'ENGINEEWGEOLWLET Meluu Sdwmmber
SAMPLES
DEPTH
Ff.
SAlNV.4
DESCRIPTION
�I
FIELD
IEASUREMENTS
SOIL
REMARKS
PENSTR.
RF96i.
MA IN.
RRC
D4
I MPl
NO.
DESCRIPTION
'
4W&S
2/&bH
NIINII
1 1
ID/1V16/18
INIMIVII
9/19/11
20'
6'
ID
IT
If
IS'
20'
sl
S3
S3
5-4
5-5
S-a
S-7
Helium dace.bmwm!m medium SAND.Pace silt brck Fnvpnmo.
Med ium,dense,
brown d ne,dowi fine mmedium SAND,trace medium,dub
It and trace fine snivel
Medium dense,down firm to medium SAND,trace medium,dense
brown,silt and mu fine gravel.
Medium,da,s brown.fine to medium SAND.Idle,medium due.
brown,cons SAND,twee silt(moist).
Medium,dense.brown,fine to medium SAND.liMe medium.dose
own,poem SAND, ne silt(moist).
d sane
NO
ND
ND
ND
NO
ND
N[1
PII
_
_
S
Mdium
Sand
the
_ �
_
♦�
5
♦
_
._
—
_
♦
Dame blown,r e to medium SAND.tram dmu blow SILT trot
at 18.5.
Beacon 2'wet dense,brown.silt fine SAND.
Rep 0.5 feet Medium dense,hale SILTY,Eve SAND.(moist).
(Hater table 125fl)
Bottom 5'Mdimq dame,dark brown,silty,fire SAND.(sWm¢d)
Little,very stf dark brown,clay.
E
a
__
1
_
15
L
1— _
20
zs
emmin.
Sampler maned in field wing TEL Model 580B RfRmed to PPM of Benzene in air. Readings in meta unia'ND.'indicates none detected
Well set m2v',IV oft'PVC gaming(24 IT of filter sand(24.0..12 -10 01-Ground Surface)7 of bmMite(12 0-10.0),PVC ruing pipe W-N2 fm above ground emfea.metal rising
(N 2 ft below ground surface to N2 ft above ground surface).
SPECTRUM ANALYTICAL, INC.
Laboratory Report
Client ID:TP-1/S-1
Lab ID No: AB10787
Matrix: Soil
Collected: 0623/98 by OTO
Received on 07/02/98 by DDR
QC and Data Review by
Location: Atwood Drive-Northampton,MA
Client Job No: J84-0520
Preservative: Refrigeration
Container: 1 Glass Soil Jar
Condition of Sample as Received: Satisfactory
Delivered by: Courier
Parameter
PCB-1016
PCB-1221
PCB-1232
PCB-1242
PCB-1248
PCB-1254
PCB-1260
Decachlorobiphenyl (%)
% Solids
Polychlorinated Biphenyls (PCB's)
Modified SW846 8081/8082
Result (ug/Kg)
Not detected
Not detected
Not detected
Not detected
Not detected
750
Not detected
73
91.3
MDL
Extracted Analyzed Analyst
250 07/02/98 07/06/98 TG
250 07/02/98 07/06/98 TG
250 07/02/98 07/06/98 TO
250 07/02/98 07/06/98 TG
250 07/02/98 07/06/98 TG
250 07/02/98 07/06/98 TG
250 07/02/98 07/06/98 TG
07/02/98 07/06/98 TG
0.1 07/02/98 07/02/98 SEC
SAk
SPECTitUMANALYTICAL.MC.
Massachusetts Certification MA 138
Connecticut Approval No.PH 0777
New Hampshire ID No.2538
New York ID No. 11393
Florida HRS87448
O'Reilly, Talbot&Okun Assoc.
293 Bridge Street
Springfield, MA 01103
Attn. Bruce Nickelsen
July 9, 1998
Client Project No J84-0520 Location: Atwood Drive - Northampton, MA
Lab TD Nn
Client ID Analysis Regnestrrl.
AB10787 TP-1/S-1 Extractable Oil Hydrocarbons
Modified SW846 8081/8082
Total Arsenic
Total Barium
Total Cadmium
Total Chromium
Total Lead
Total Mercury
Total Selenium
Total Silver
AE10788 TP-4/S-1 Extractable Oil Hydrocarbons
Modified SW846 8081/8082
Total Arsenic
Total Barium
Total Cadmium
Total Chromium
Total Lead
Total Mercury
Total Selenium
Total Silver
AB10789 TP-5/S-1 Extractable Oil Hydrocarbons
Modified SW846 8081/8082
Total Arsenic
Total Barium
Total Cadmium
Total Chromium
Total Lead
Total Mercury
Continued next page. . .
ENVIRONMENTAL ANALYSES
11 Alme en Drive •Agawam,Massachusetts 01001 •413-789-9018 • FAX 413-789-4076
SPECTRUM ANALYTICAL, INC.
Laboratory Report
Client ID:TP-1/S-1
Lab ID No.:AB10787
Matrix Soil
Collected: 06/23/98 by OTO
Received on 07/02/98 by DDR
QC and Data Review by
Location: Atwood Drive-Northampton,MA
Client Job No.: J84-0520
Preservative: Refrigeration
Container: 1 Glass Soil Jar
Condition of Sample as Received: Satisfactory
Delivered by: Courier
Extractable Petroleum Hydrocarbons
MA DEP Modified EPA 8270/8100
Parameter for AB10787
Aliphatics/Aromatics(mg/Kg)
C9- C18 Aliphatics
C19- 06 Aliphatics
C11- C22 Aromatics
Targeted PAH's Analytes (ug/Kg)
Acenaphthene
Acenaphthylene
Anthracene
Benzo (a) anthracene
Benzo (b) fluoranthene
Benzo (k) fluoranthene
Benzo (a)pyrene
Benzo (g,h.i)perylene
Chrysene
Dibenz(a,h) anthracene
Fluoranthene
Fluorene
Indeno (1,2,3-cd)pyrene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogate Recovery(%)
1-Chloro-octadecane(%SR)
Ortho-Terphenyl(%SR)
Results
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
43
42
MDL
Extracted Analyzed Analyst
33 07/02/98 07/08/98 MB
33 07/02/98 07/08/98 MB
33 07/02/98 07/08/98 MB
148.0 07/02/98 07/08/98 MB
148.0 07/02/98 07/08/98 MB
148.0 07/02/98 07/08/98 MB
148.0 07/02/98 07/08/98 MB
148.0 07/02/98 07/08/98 MB
148.0 07/02/98 07/08/98 MB
148.0 07/02/98 07/08/98 MB
148.0 07/02/98 07/08/98 MB
148.0 07/02/98 07/08/98 MB
148.0 07/02/98 07/08/98 MB
148.0 07/02/98 07/08/98 MB
148.0 07/02/98 07/08/98 MB
148.0 07/02/98 07/08/98 MB
148.0 07/02/98 07/08/98 MB
148.0 07/02/98 07/08/98 MB
148.0 07/02/98 07/08/98 MB
148.0 07/02/98 07/08/98 MB
07/02/98 07/08/98 MB
07/02/98 07/08/98 MB
% Solids 91.3 0.1 07/02198 07/02/98 SEC
CHAIN OF CUSTODY RECORD
age I of 1
9�
SPECTRUM ANALYTICAL
OJECT NO.: -,',' -- t(- _ 3-- 2..
'E NAME: .'.•.-_,2.2_J,o'Ip! b.' %.-i
CATION: !1 /'0,r-1) ;,\G 'u:td 1-l.V\ STATE(L-14-
FERENCE QUOTE NUMBER (RQN):
RCHASE ORDER Na:
OJECT Mgr: /ti it /li—e. >:-./ L,L
MPLER(s):
tMPLE TYPE & MATRIX CODES:
1-PCBS 2-PEST(608/B080)
4°C 2=HCI 3=F12SO4 4=HNO, 5=OTHER
>
j
w
N
ce
ce
a
:COMPOSITE G=GRAB
>i
r
i
E
Q
rf'
:AQUEOUS 3=SLUDGE
:SOIL 4=SEDIMENT
S=OTHER
X
E2
F-
E
t B USE
DNLY
SAMPLE I.D.
DATE
TIME
ryi;z'?
773- ( s- r
6/z3
(s1jt
1-4 s( s- f
' :t
2
Q
;a,.W.•
T-0-5 S- (
L<
2
--r4 cc". s- (
1
'7
(1
,;,,»v.
Lrci/
4
BY:
RECEIV,FD V.,
DATE
TIME
;RELINQUISHED
% C' f f�91, , �:A ,J 7
Y 4�/ -
7-af91(
?Lc°
IPECIAL INST9UCTIONS:
r •{
�i-Yt;l I,(,�Pr74L.;, DAd
�A
❑Return Sample
❑ Dispose TAT
• Standard
❑SP�ISI TAT
•TAT for begins when
•TAT for samples
•All TATS are subject
DATE RESULTS
SPECIAL HANDLING:
Please
check
business
consent.
day.
after Analysis
-7 to 10
r 4a
-24 hr-48
sample Is
read after
to laboratory
NEEDED'
usness
Business days
hr-T2 hr-5 b.days
received at test to the.
3 pm will begin on the
approval and customer
cirry /7,11p 1U�� $
I
„A / / d I � M "1» � '
.�i.
��' / ( f U
�I�S/Jt l_ / %�/�f:
7 Fax results when available to ( )
11 Almgrea Drive•Agawam,M
chum
01001 •413-789-9018•Fax 413-789-4076
SPECTRUM ANALYTICAL, INC.
Laboratory Report
Client ID:TP-1/S-1
Lab ID No: AB1O787
Matrix Soil
Collected: 06/23/98 by OTO
Received on 07/02/98 by DDR
QC and Data Review by
Location: Atwood Drive-Northampton,MA
Client Job No: J84-0520
Preservative: Refrigeration
Container: 1 Glass oil Jar
Condition of Sample as Received: Satisfactory
Delivered by: Courier
Parameter
Total Arsenic
Total Barium
Total Cadmium
Total Chromium
Total Lead
Total Mercury
Total Selenium
Total Silver
Result (mg/Kg)
nd
51.3
nd
13.8
347
nd
nd
nd
MDL
0.904
0.904
0.904
0.904
0.452
0.225
0.452
1.81
Metals
Method
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 245.1
EPA 200.7
EPA 200.7
Digested Analyzed Analyst
07/08/98 07/08/98 CR
07/08/98 07/08/98 CR
07/08/98 07/08/98 CR
07/08/98 07/08/98 CR
07/08/98 07/08/98 CR
07/08/98 07/07/98 JM
07/08/98 07/07/98 CR
07/08/98 07/07/98 CR
PECTIN ANALYTICAL,INC.
Massachusetts Certification MA 138
Connecticut Approval No. PH 0777
New Hampshire ID No. 2538
New York ID No. 11393
Florida HRS87448
O'Reilly, Talbot& Okun Assoc
293 Bridge Street
Springfield, MA 01103
Attu- Bruce Nickelson
December 30, 1998
Client Project No.: 30840517 Location: Atman - Northampton
I all in No
Client Til Analysis Requested
.4829056 NOHO-2 Total Lead
AB29057 NOHO-5 Total Lead
AB29058 NOHO-3 Total Lead
AB29059 NOHO-7 Total Lead
AB29060 NOHO-9 Total Lead
AB29061 NOHO-l0 Total Lead
Extractable Oil Hydrocarbons
Modified SW846 8082
AB29062 NOHO-11 Total Lead
Extractable Oil Hydrocarbons
Modified SW846 8082
AB29063 NOHO-12 Total Lead
Extractable Oil Hydrocarbons
Modified SW846 8082
.4829064 NOHO-13A Total Lead
Extractable Oil Hydrocarbons
Modified SW846 8082
AB29065 NOHO-12B Total Lead
Extractable Oil Hydrocarbons
Modified SW846 8082
AB29066 NOHO-14 Total Lead
Extractable Oil Hydrocarbons
Modified SW846 8082
AB29067 NOHO-15 Total Lead
Extractable Oil Hydrocarbons
Modified SW846 8082
AB29068 NOHO-16 Total Lead
Extractable Oil Hydrocarbons
Continued next page. . .
ENVIRONMENTAL ANALYSES
11 Almgen Drive •Agawam,Massachusetts 01001 • 413-789-9018 • FAX 413-789-4076
O'Reilly,Talbot& Okun Assoc.
December 30, 1998
Client Project: J0840517
Location. Atman-Northampton
I ah TT) Nn
Client IT) Aagjvsis Requested
AS29068 NOHO-16 Modified SW846 8082
4829069 NOHO-17 Total Lead
Extractable Oil Hydrocarbons
Modified SW846 8082
21829070 NOHO-18 Total Lead
Extractable Oil Hydrocarbons
Modified SW846 8082
ayeh
ENVIRONMENTAL ANALYSES Preside '7�T.�: :tb y Director
11 Alma en Drive •Agawam,Massachusetts 01001 • 413-789-9018 • FAX 413-789-4076
SPECTRUM ANALYTICAL, INC.
Laboratory Report
Client ID: NOHO.2
Lab ID No: AB29056
Matrix Soil
Collected: 12/18/98 OTO
Received on 12/21/98 MBR
QC and Data Review by
Location: Atman -Northampton
Client Job No: J0840517
Preservative: Refrigeration
Container: 1 Clear Glass Jar
Condition of Sample as Received: Satisfactory
Delivered by: Client
Parameter
Total Lead
Total Lead
EPA Method 6010200.7
Result (mg/Kg) MDL
Digested Analyzed Analyst
163 0.449 1229/98 12/30/98 DMM
SPECTRUM ANALYTICAL, INC.
Laboratory Report
Client ID: NOHO-3
Lab ID No: AB29058
Matrix: Soil
Collected: 12/18/98 by OTO
Received on 12/21/98 by MBR
QC and Data Review by
Location: Atman-Northampton
Client Job No: J0840517
Preservative: Refrigeration
Container. 1 Clear Glass Jar
Condition of Sample as Received: Satisfactory
Delivered by: Client
Parameter
Total Lead
Total Lead
EPA Method 6010/200.7
Result (mg/Kg)
MDL
Digested Analyzed Analyst
69.0 0.464 12/29/98 12/30/98 DMM
SPECTRUM ANALYTICAL, INC.
Laboratory Report
Client ID: NOBO-5
Lab ID No: AB29057
Matrix: Soil
Collected: 12/18/98 by OTO
Received on 12/21/98 by MBR
OC and Data Review by
Location: Atman -Northampton
Client Job No: J0840517
Preservative: Refrigeration
Container: 1 Clear Glass Jar
Condition of Sample as Received: Satisfactory
Delivered by: Client
Parameter
Total Lead
Total Lead
EPA Method 6010/200.7
Result (mg/Kg) MDL
Digested Analyzed Analyst
783 0.455 12/29/98 12/30/98 DMM
SPECTRUM ANALYTICAL, INC.
Laboratory Report
Client ID: NO11O-7
Lab ID No: AB29059
Matrix Soil
Collected: 12/18/98 by OTO
Received on 12/21/98 by MBR
QC and Data Review by
Location: Atman-Northampton
Client Job No: J0840517
Preservative: Refrigeration
Container: 1 Clear Glass Jar
Condition of Sample as Received: Satisfactory
Delivered by Client
Parameter
Total Lead
Total Lead
EPA Method 6010/200.7
Result (mg/Kg) MDL
Digested Analyzed Analyst
73.4 0558 12/29/98 12/30/98 DMM
SPECTRUM ANALYTICAL, INC.
Laboratory Report
Client ID: NO13O-9
Lab ID No: AB29060
Matrix: Soil
Collected: 12/18/98 by OTO
Received on 12/21/98 by MBA
QC and Data Review by
Location: Atman-Northampton
Client Job No: J0840517
Preservative: Refrigeration
Container: 1 Clear Glass Jar
Condition of Sample as Received: Satisfactory
Delivered by Client
Parameter
Total Lead
Total Lead
EPA Method 6010200.7
Result (mg/Kg)
MDL
Digested Analyzed Analyst
47.2 0.458 12/29/98 12/30/98 DMM
Sh _Special Handling;..__.__
CHAIN OF CUSTODY RECORD andardTAT- "° '°bttT %�I
shtA T- 7t
,eify.ush TAT-Date Needed/r a 6/1.1>
• All TATS subject to laboratory approval;mm.
I /'� 24 hour notification needed for rushes.
Page o • Samples disposed of after 60 days unless
SPECTRUM ANALYTICAL ,,r� otherwised instructed.
Report To: K<177) Invoice To: ACtrl j Project No.: 7—CALL — OS-1 7
•J Site Name:Ark-al C'fl
Location: NJ�n/ h % tken fr b11 Slate:
Project Mgr.: ISYVC P N P.O.No.: RQN: Sampler(s):dv\P ,lc Sa)
1=4°
5
2—HCl 3=41rSOt 4=HNOr 5—NaOH 6=MeOH 7= Containers: Analyses: Notes:
fDW
Qrinking Water GW=Ground Water WW=Waste Water
C SO=S SL=Sludge 0=011 Xl= X2= ^ t
b tc
V Q l 'A
G=Grab C=Composite to O u
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Additional Instructions: ��yy �Relinq�uished By: Received By: Date: Time:
.7� r = idpo/%e ,ijj7/IR�4fstlRIntWSJLh /I `A( ;/,>--ced
Nit request I . , PIW. a;-- -/ r ', I_45`-I /d •1/- y /0--.43—t
11 Almeren Drive•Aeawam.Massachusetts 01001 •413-789-9018•Fax 413-789-4076
Special Handling: 1
gie CHAIN OF CUSTODY RECORD Standard TAT-7 to 10 business days
❑ Rush TAT-Date Needed:
• All TATS subject to laboratory approval;min.
B 24 a hour notification id needed 60 for ru unless
Page o£ • Samples disposed of after 60 days unless
SPECTRUM ANALYTICAL ,(r —rte, �ottherwised instructed.
Report To: (1� Invoice To: 11/41k(An/ Project No.: J S4—O�-17
Site Name: Minn 1'1
Location: (�if0%1-il et riPin 1 State:
Project Mgr.:
Br17(2- ^I P.O.No.: RQN: Sampler(s): MO Ji cc n )
1=4° 2=HCI 3=H2SO4 4=11NO3 5=NaOH 6=MeOH 7= Containers: Analyses: Notes:
N
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• m O -9 m a�
U I.a � �
Lab Id. Sample Id: Date: Time: w` a u u '
"Ada A10h0-jr II II
Alle16617 IVdIO4 1 i
ABA90 AJ,Iha-1 '7 ! II k I.-- 1.--: 1
Apr7.c(t,7r otin —i
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Additional Instructions: By: Received By: Date: Time:
X4.7" is/sO/9f- I I Lt A _ • -Al t. ■ PL
Jac (11C 1A a- 11/01)..., ) If 1 Y 1_, /3 “l1 • I ,'Iii,
II Almgren Drive•Agawam,Massachusetts 01001.413-789-9018•Fax 413-789-4076
IR
SPECTRUM ANALYTICAL,INC.
Massachusetts Certification M-MA 138
Connecticut Approval#PH 0777
Rhode Island#988c Maine#nla
New Hampshire ID#2538
New York ID#11393
Florida HRS87448
O'Reilly, Talbot& Olrun Assoc.
293 Bridge Street
Springfield, MA 01103
Attn: Bruce Nic&elsen
Client Project No.: 1840517 Location: Atwood Drive
January II, 1999
Lab TT) No Client ID Analysis Requested
AH29697 NOHO-1 EPA Method 8260
Extractable Oil Hydrocarbons
Soluble Lead
Volatile Petroleum Hydrocarbons
A129698 NOHO-10 Volatile Petroleum Hydrocarbons
EPA Method 8260
Extractable Oil Hydrocarbons
Soluble Lead
ENVIRONMENTAL ANALYSES
Presider aborato - Director
11 Almgren Drive •Agawam,Massachusetts 01001 • 413-789-9018 • FAX 413-789-4076
SPECTRUM ANALYTICAL, INC.
Laboratory Report
Client ID: NOH0-1
Lab ID No: AB29697
Matric Ground Water
Sampled on1228/98 by OTO
Received on 12/28/98 by MBA
QC and Data Review by AM
Location: Atwood Drive
Client Job No.: J840517
Preservative: Refrigeration,HC1
Container : 2 VOA Vials
Condition of Sample as Received: Satisfactory
Delivered by Client
Parameter for AB29697
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
Volatile Organics
EPA Method 8260
Result (ug/L) MDL
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Not detected 1.0
Analyzed Analyst
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
Continued next page...
Parameter for AB29697
Volatile Organics
EPA Method 8260
Result (ug/L) NIDL
trans-1,3-Dichloropropene Not detected 1.0
Ethylbenzene Not detected 2.0
Hexachlorobutadiene Not detected 1.0
Isopropylbenzene Not detected 1.0
4-Isopropyltoluene Not detected 1.0
Methylene chloride Not detected 1.0
Naphthalene Not detected 4.0
n-Propylbenzene Not detected 1.0
Styrene Not detected 1.0
1,1,1,2-Tetrachloroethane Not detected 1.0
1,1,2,2-Tetrachloroethane Not detected 1.0
Tetrachloroethee Not detected 8.0
Toluene Not detected 3.0
1,2,3-Trichlorobenzene Not detected 1.0
1,2,4-Trichlorobenzene Not detected 1.0
1,1,1-Trichloroethane Not detected 1.0
1,1,2-Trichloroethane Not detected 1.0
Trichloroethene Not detected 1.0
Trichlorofluoromethane Not detected 1.0
1,2,3-Trichloropropane Not detected 1.0
1,2,4-Trimethylbenzene Not detected 4.0
1,3,5-Trimethylbenzene Not detected 2.0
m,p-Xylenes Not detected 2.0
o-Xylene Not detected 1.0
Vinyl chloride Not detected 1.0
Methyl-t-butyl ether Not detected 2.0
BFB Surrogate Recovery(%) 99
p-DFB Surrogate Recovery(%) 103
CLB-d5 Surrogate Recovery (%) 97
Analyzed Analyst
01/09/99 SN
01/09/99 SN
01'09/99 SN
01/09/99 SN
01/19/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01109/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
OL/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
SPECTRUM ANALYTICAL, INC.
Laboratory Report
Location: Atwood Drive
Client Job No.: J840517
Client ID:NO11O-1
Lab ID No.:AB29697
Matrix: Ground Water
Collected: 12/28/98by QTQ
Received: 12/28/98by MBR
Preservative: Refrigeration,HO
Container: 2 VOA Vials
Condition of Sample as Received:See Attached Sheet
Volatile Petroleum Hydrocarbons
MADEP VPH 97-12
Parameter for AB29697
Aliphatics/Aromatics (mg/L)
C5-C8 Aliphatic Hydrocarbons
C9-C12 Aliphatic Hydrocarbons
C9-C10 Aromatic Hydrocarbons
Unadjusted C5-C8 Aliphatics
Unadjusted C9-C12 Aliphatics
Target VPH Analytes (ug/L)
Benzene
Ethylbenzene
Methyl-tert-butylether
Naphthalene
Toluene
m,p-Xylenes
o-Xylene
Results MDL
Not detected 0.150
Not detected 0.050
Not detected 0.050
Not detected 0.150
Not detected 0.050
Not detected 5.0
Not detected 5.0
Not detected 5.0
Not detected 5.0
Not detected 5.0
Not detected 5.0
Not detected 5.0
Analyzed Analyst
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
Dilution Factors
Carbon Chain Dilution Factor 1 01/09/99 SN
Target Analytes Dilution Factor 1 01/09/99 SN
Surrogate Recoveries (%)
2,5-Dibromotoluene PID (%SR)
2,5-Dibromotoluene FID (%SR)
2,5-Dibromotoluene GCMS (%SR)
4-Bromofluorobenzene GCMS (%SR)
NA
NA
118
106
01/09/99 SN
01/09/99 SN
01/09/99 SN
01/09/99 SN
Were all QA/QC procedures required by the VPH method followed? Yes No
Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ( / No
Were any significant modifications made to the VPH method,as specified in Section 11.3? Yes' ✓No
ayes is answered to above question,then this sample was run via GCMS using all VPH method specified QC criteria
I attest that b
the materi
inquiry of those individuals immediately responsible for obtaining the information,
repo 1 ,to the best of my knowledge and belief,accurate and complete.
/
tory Director
01/11/99
SPECTRUM ANALYTICAL, INC.
Laboratory Report
Location: Atwood Drive
Client Job No.: J840517
Client ID: NOHO-1
Lab ID No.:AB29697
Matrix: Ground Water
Collected: 1228/986y OTO
Received: 1228/98by MBR
Preservative: Refrigeration/INO3
Container: 1 Amber/1 Plastic
Condition of Sample as Received:See Attached Sheet
Extractable Petroleum Hydrocarbons
MADEP EPH 98-1,SW846 3510C Separatory Funnel Liquid-Liquid Extraction
ParameterforAB29697
Aliphatics/Aromatics (mg/L)
C9-C18 Aliphatic Hydrocarbons
C19-C36 Aliphatic Hydrocarbons
C11-C22 Aromatic Hydrocarbons
Unadjusted C11-C22 Aromatics
Diesel PAH Analytes (ug/L)
Naphthalene
2-Methylnaphthalene
Phenanthrene
Acenaphthene
Other Target PAH Analytes (ug/L)
Acenaphthylene
Anthracene
Benzo (a) anthracene
Benzo (a)pyrene
Benzo (b) fluoranthene
Benzo (g,h,i)perylene
Benzo (k) fluoranthene
Chrysene
Dibenzo (a,h) anthracene
Fluoranthene
Fluorene
Indeno (1,2,3-cd) pyrene
Pyrene
Dilution Factors
Carbon Chain Dilution Factor
Target Analyte Dilution Factor
Results
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
1
1
MDL
0.2
0.2
0.2
0.2
Extracted Analyzed Analyst
12/30/98
12/30/98
12/30/98
12/30/98
01/03/99
01/03/99
01/03/99
01/03/99
KS
KS
KS
KS
10.0 12/30/98 01/03/99 KS
10.0 12/30/98 01/03/99 KS
10.0 12/30/98 01/03/99 KS
10.0 12/30/98 01/03/99 KS
10.0 12/30/98 01/03/99 KS
10.0 12/30/98 01/03/99 KS
10.0 12/30/98 01/03/99 KS
10.0 12/30/98 01/03/99 KS
10.0 12/30/98 01/03/99 KS
10.0 12/30/98 01/03/99 KS
10.0 12/30/98 01/03/99 KS
10.0 12/30/98 01/03/99 KS
10.0 12/30/98 01/03/99 KS
10.0 12/30/98 01/03/99 KS
10.0 12/30/98 01/03/99 KS
10.0 12/30/98 01/03/99 KS
10.0 12/30/98 01/03/99 KS
12/30/98 01/03/99 KS
12/30/98 01/03/99 KS
Parameter for/0329697 Results
Surrogate Recoveries (%)
1-Chloro-octadecane Aliphatic (%SR) 82
Ortho-Terphenyl Aromatic (%SR) 62
2-Bromonaphthalene Fractionation(%SR)43
2-Fluorobiphenyl Fractionation(%SR) 51
IVIDL Extracted Analyzed Analyst
12/30/98
12/30/98
12/30/98
12/30/98
01/03/99
01/03/99
01/03/99
01/03/99
KS
KS
KS
KS
Were all QA/QC procedures required by the EPH method followed? Yes No
Were all performance/acceptance standards for required QA/QC procedures achieved? Yes C, No
Were any significant modifications made to the EPH method,as specified in Section 11.3? Yes•, __No
•If yes answered to above question,the aromatic hydrocarbons from C11-C22 along with target PAH aoalytes were performed
via GC/MS following all EPH method specified QC criteria.
I attest that based up>n ml inquiry of those individuals immediately responsible for obtaining the information,
the best of my knowledge and belief,accurate and complete.
01/11/99
SPECTRUM ANALYTICAL, INC.
Laboratory Report
Client ID: NOH0-1
Lab ID No: AB29697
Matrix: Ground Water
Collected: 1228/98 by OTO
Received on 12/28/98 by MBR
OC and Data Review by
Location: Atwood Drive
Client Job No: J840517
Preservative: RefrigerationlHNO3
Container: 1 Amber/1 Plastic
Condition of Sample as Received: Satisfactory
Delivered by Client
Parameter
Soluble Lead
EPA Method 200.7
Result (mg/L) MDL
Extracted Analyzed Analyst
Soluble Lead nd 0.005 01/04/99 01/06/99 DMM
Standard TAT-7 to 10 business days
CHAIN OF CUSTODY RECORD ❑ Rush TAT-Date Needed:
• All TATS subject to laboratory approval;min.
glit 24 hour notification needed for rushes.
Page / of I • Samples disposed of after 60 days unless
otherwised instructed.
SPECTRUM ANALYTICAL —17
-t-7 �(t Project No.: �—C`'
I C Invoice To: 11/In rY nn II �_�r,
Report To: Site Name; !1'-f U)vt�
State:
Location: c {_
RQN: Sampler(s) ccv Cc-WAN',1Phf? r-
Project Mgr.: ` U(.-Q- k Sr- £ P.O.No.: Q
Anal Analyses. Notes:
=4°0(2=HC� 3=HaSOa �13N0��S=NT'a.�.,.OH 6=MeOH 7=
Containers: y
DW=Drinking Water °Ground Wa1 WW=Waste Water t7 i �
SO=Sail SL=Sludge O=Oil X1= > M — Z
CI ¢ p
G=Grab C=Composite j a o pt, .�
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Lab Id: Sample Id: Date: Time: , a cs * u se u
GW Iy' 2 I ✓ V
AB 1G 11` IA vN0—I I a6/(16 GW a�, 2 1 I V
ABg`1(rrlis Nn1(10-IO N
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AB' - • -ced By: Date: Time:
Relinquished By:
bd6
Additional Instructions: �/�/[[//�� •
I� b ,4 0
•
II Almgren Drive•Agawam,Massachusetts 01001.413-789-9018•Fax 413-789-4076
SPECI'1�1M ANiLYTICAL,INC,
Massachusetts Certification M-MA 138
Cooacedcut Approval#PH
Rhode Island M 92&Mainz#n/e
New Hasnpsbisz ID#2538
NewYoskID#11393
Florida HR587448
O'Reilly, Talbot a Okun Assoc.
293 Bridge Street
Springfield MA 01103
Atut Bruce MakeLen
Client Project No.: 30840517 Location: Abnan-Northampton
February 3, 1999
1 7,TD Nn Client-1D_
A829057 NOH0-5
TO'd
Anal3BeltEluac=1
TCZP Lead
ENVIRONMENTAL ANALYSES
11 Maim Driva Agawam,Massachusetts 01001. 4l37$9-9018• FAX 413-7894076
FT:LT 66, V 957j -
SPECTRUM ANALYTICAL,INC.
Laboratory Report(Subcontracted Analysis)
Location: Atman-Northampton
Client Job No: J0840517
Preservative: Refrigeration
Container. 1 Clear Glass Jar
Semple as Received: Satisfactory
o
Client ID:NOHO-S
Lab ID No: AB29057
Co
llected:iut&9s OTO
Received Data Reew AM
Parameter
TCLP Lead
TCLP Lead
EPA Method 1311/5W846 6019
Result(mg/L) MILL
6.07
ZOd £T:L1 66, b Clad
Extracted Analyzed Analyst
0.010 02/01/99 02/03199 CR
Spectrum Analytical,Inc.
Laboratory Report Supplement
Re eience
Methods for the Dete+mination of Organic Compounds in Drinking Water. EPA-600/418/039. EMSL 1988.
Methods for Chemical Analysis of Water and Wastes. EPA 600/4-79.020. EMSL 1983-
Methods for Organic Chemical Analysis of Municipal and Industrial Wastewater. EPA 600/4-82-057. EMSL 1982
Test Methods for Evaluating Solid Waste. Physical/Chemical Methods. EPA SW-846. 1986.
Standard Met hods for the Examinatinon of Water and Wastes. APHA-AWWA-WPCF. 1611vEdition. 1985.
Standard Methods for Comparison of Waterborne Petroleum Oils by Gas Chromatography. ASTM D 3328. 1982.
Oil Spill Identification System- U.S.Coast Guard CG-D-52-77. 1977.
Handbook for Analytical Quality Control in Water and Wastewater Laboratories. EPA 60014-79-019- EMSL 1979.
Choosing Cost-Effective QA/QC(Quality Assurance Quality Control)Programs for Chemical Anslyses. EPA 600/4-85/056.
EMSL 1985.
Report No ations
Not Detected, The compound was not detected at a concentration equal to or above
Not Pet,ND or nd the established method detection limit.
NC = Nor Calculated
MCL EPA Maximum Contamination Level
VOA = Volatile Organic Analysis (An EPA 624 Surrogate)
BFB = 4-Bromojfvarobenzene
p-DEB . • 1,4-Diffuorobenrene (An EPA 624 Surrogate)
Chforobenzene-d5 (An EPA 624 Surrogate)
CLB BC? = (An EPA 601 Surrogate)
BCP = a a,a T,-1 nrotoluene
TFf =
¢,cep-T>�varotofuene (An EPA 602 Surrogate)
Decachlorobiphenyl = (an EPA 60818080 Surrogate)
DEfinisiam
Surrogate Recovery—The recovery(expressed as a percent)of a non-method analyte(see surrogates listed
above)added to the sample for the purpose of monitoring system performance.
Matrix Spike Recovery=The recovery(expressed on analyte of to thod a alytes added to the sample for the
purpose of determining any effect of sample composition
Laboratory Replicate=Two sample aliquots taken in the analytical laboratory and analyzed separately with
identical procedures. Analyses of laboratory duplicates give era as�Stf the procedures.S$ociated with or
laboratory procedures,but not with sample collection,pr
Field Duplicate Two separate samples collected at the same time and
place under F d ntifc l circumstances t nce sand
treated exactly the same throughout field and laboratory p well as duplicates
laboratory give a measure
of the precision associated with sample collection,preservaton and storage,as
Relative Percent Difference(%RPD)=The precision measurement obtained on duplicate/replicate analyses.
4/4RPD is calculated as: %RPD v
=rah el -vaLue2 ' 100%
ave.value
£0'd £T:LT 66. P gad
' LHandliyg
CHAIN OF CUSTODY RECORD °ndard TAT-7 ol06uaiaeaad
ush T Dale Needed .., .;
IR
All TATS subject to laboratory approval;min.
24 hour notification needed for rushes.
Sl'FCIAUMAMALY7JCA1. Page / o� • Samples disposed of Thar 60days unless
'-4j n othenvised instructed.
Report To: 617?)C) Invoice To: W\CLI 9 Project No.: SOtSd-1 -• US I7
•J Site Name:A-f in Ofl
Location: NotA-ha m cribn State:
-
ProecMg : O P.O.No.: RQN: Sampler(s); WL'
1LGSC )
61=4Y 2=HCI 1=11350, 4=HNO, 5-NaOH 6=MeOH 7= Containers: Arses: Notes: I
•
•
D eking Water CW.43round Water WW-Waste Water ` 2
/SO-Soi SL-Sludge O=Oil %I= %2= p 4
•
0.-Drab C=Composite a OQ �� 4 --(
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Additional Instructions.J�C 1 4 S 5(.r Relinquished By: Received By: • Dale: Time:
Sig v�qt i�ct g�, mil/1;741v �Gh � Ai 41- II Aril
11 A Infirm,Drive•A ammo, Maaarhmm is Al AM I•411-1119-90111•Par 411-7R9.41176
SPECTRU ANAlYTICAI,INC.
Massachusetts Certification M-MA 138
Connecticut Approval#PH 0717
Rhode Island it 98&Maine#Na
New Hominid=ID#2538
New Yerk ID#11393
Florida HRS87448
O'Reilly, Talbot&Okun Assoc.
293 Bridge Sirta:t
Springfield,MA 01103
Attn: Bruce Nickebsen
Client Project No.:70840517 Location:Atwood
January 5, 1999
L'6 In No G7ient In
A329860 MONO-a
Analysis RTue_stad
Total Load
ENVIRONMENTAL ANALYSES
II Magnet Drive •Agawam,Massachusetts 01001 • 413-789-9018 • FAX 413-789-40/6
T0' d £00' ON TS:VI 66,SO OE( : 131
SPECTRUM ANALYTICAL,INC.
Laboratory Report
Client ID:NOHO-S Location: Atwood
Lab ID No: AB29860 Client Job No: J0840517
Mate Soil
Collected: 12118N8 by OTO
Received on 12/31198 by MDR
QC and Data Review by
Preservative: Refrigeration
Container: 1 Clear Glass Jar
Condition of Sample as Received: Satisfactory
Delivered by Client
Total Lead
EPA Method 6010200.7
Parameter Result(mg/Hg) MDL
Total Lead 159 0.470
ZO' d £00' °N ZS:VI 66, 50 laf
Digested Analysed Analyst
01104198 01105A9 DMM
131
Spectrum Analytical,Inc.
Laboratory Report Supplement
R&M=
M=
Methods for the Determination of Organic Compounds in Drinking Water. EPA-600/4.88/039. EMSL 1988.
Methods for Chemical Analysis of Water and Wastes. EPA 600/4.79020. EMSL 1983.
Methods for Organic Chemical Analysis of Municipal and Industrial Wastewater. EPA 600/442-057. EMSL 1982.
Test Methods for Evaluating Solid Waste. Physical/Chemical Methods. EPA SW-846. 1986.
Standard Methods for the Examiratinon of Water and Wastes. APHA-AW WA-WPCF. 16th Edition- 19S5.
Standard Methods for Comparison of Waterborne Petroleum Oils by Gas Chromatography. ASTM 0 3328. 1982.
Oil Spill Identification System. U.S Coast Guard CG-D-52.77. 1977.
Handbook for Analytical Quality Control in Water and Wastewater Laboratories- EPA 600/4.79419. EMSL 1979
Choosing Cost-Effective QA/QC(Quality Assurance/Quality Control)Programs for Chemical Anslyses. EPA 600/4-85/056.
EMSL 1985.
Retort Noations
Not Detected, = The compound was not detected at a concentration equal to or above
Not Det,ND or nd the established method detection limit
NC = Not Calculated
MCL = EPA Maximum Contamination Level
VOA = Volatile Organic Analysis
BFB = 4-Bromoflaorobenrane (An EPA 624 Surrogate)
p-DFB = 1,4-Difluorobeneene (An EPA 624 Surrogate)
CLB-d5 = ChlorobensenedS (An EPA 624 Surrogate)
BCP = 2-Bromo-l-chloropropane (An EPA 60)Surrogate)
TFT = a tea-Trtfluorotoluene (An EPA 602 Surrogate)
DecachlorobiphenYl = (an EPA 608/8080 Surrogate)
Definlllons
Surrogate Recovery=The recovery(expressed as a percent)of a non-method analyte(see surrogates listed
above)added to the sample for the purpose of monitoring system performance.
Matrix Spike Recovery=The recovery(expressed as a percent)of method analyzes added to the sample for the
purpose of determining any effect of sample composition on analyte recovery.
Laboratory Replicate=Two sample aliquots taken in the analytical laboratory and analyzed separately with
identical procedures. Analyses of laboratory duplicates give a measure of the precession associated with
laboratory procedures,but not with sample collection,preservation,or storage procedures.
Field Duplicate=Two separate samples collected at the same time and
And place of Field identifical
duplicates cu circumstances es and
under
treated exactly the same throughout field and collection,ptoep and storage,as well as with laboratory procedures.
of the precision associated with sample collection,pre
Relative Percent Difference(34 RPD)=The precision measurement obtained on duplicate/replicate analyses.
%RPD is calculated as:
%RPD a(value'-value2l• 100%
ave.value
£0' d 200' 0N ZS: VT 66. 50 upf
: 131
Special Handling:
ilik CHAIN OF CUSTODY RECORD DStandard TAT-7m I0 business ya
Rush TAT-Date Needed:� s 9Fl
• All T.ATs subject to laboratory jppro al;min.
24 hour m tilcation needed for msbes.
Page of / • Samples disposed of after 60 days unless
SPECTACMANALYDCRL otherwieed instructed.
Report To: GTO Invoice To: MO• 1 Project No.'SC40 4 —or'�L 17
Site Name: 4t Lt )COC ,
Localion: Stale: _ y
Project Mgr.: RVJ C P 14 P.O.No.: RQN: Sampler(s): ill • 4 I in && P
40CC 2=HCI 3=H,S0< 4=HNO, 5—NaOH 6=MeOH 7= Containers: Analyses: Notes:
DW— raking Water GW4irouad Water WW—Waste Water
'3lkSo SL-Sludge Oil XI— X2=
V j
a 4 I p a
O='emb C=Conposite a 0 B a
4 Ci d
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Lab Id: Sample W: Date: Time: E d', I. x x : x
t0a?4 44 Al0ho—X ieQft/lt So 1 i. >I
* '
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Additional Instructions: Relinquished B : „ ived By:
Of Date: Time: c
/Ii' A J al-.1 4 / /31h-9J is 4_, ,
L
11 Mom°Drive•Agawam,Mamchusetts01001 •411-789-9018•Fax 413-789.4076
SPECTRUM AN U'
Massachusetts Certification PA-MA 138
Connecticut Rhode Island#98&Maine#n/a
New Hampshire ID#1538
New York ID#I1393
Florida HRS87448
O'Reilly, Talbot& Okun Assoc.
293 Bridge Street
Springfield, MA 01103
Attn. Bruce Nickelsen
Client Project No.: J084
1,41:0D-No- c t`I77
AB32346
NOHO-101 Total Lead
AB32348
NOHO-103 Total Lead
.9B 32350
NOHO-105 Total Lead
AB32353
NOH0-108 Total Lead
NOH0-11 Conductance
AB32356
ERA Method 8260
TPH by GC
EPA Method 8270
NOHOCOMP Conductance
AB32390 EPA Method 8260
TPH by GC
EPA Method 8270
February 3, 1999
Location: Atwood
ArawAhsassa.mated
ENVIRONMENTAL ANALYSES
11 Almgren Drive• Agawam,Massachusetts 01001 • 413-789-9018• FAX 413-789-4076
SPECTRUM ANALYTICAL, INC.
Laboratory Report
Client ID:NOHO-101
Lab ID No: AB32346
Matrix: Soil
Collected: 01/29/99 by OTO
Received on 0129/99 by MBR
QC and Data Review by
Location: Atwood
Client Job No: J084
Preservative: Refrigeration
Container: 1 Clear Glass Jar
Condition of Sample as Received: Satisfactory
Delivered by Client
'arameter
tal Lead
Total Lead
EPA Method 6010/200.7
Result (mg/Kg) MDL
Digested Analyzed Analyst
69.9 0.454 02/02/99 02/03/99 CR
SPECTRUM ANALYTICAL, INC.
Laboratory Report
Client ID: NOHO-103
Lab ID No: A1332348
Matrix: Soil
Collected: 01/29/99 by OTO
Received on 0129/99 by MBA
QC and Data Review by
Location: Atwood
Client Job No: J084
Preservative: Refrigeration
Container: 1 Clear Glass Jar
Condition of Sample as Received: Satisfactory
Delivered by: Client
'arameter
tal Lead
Total Lead
EPA Method 6010/200.7
Result (mg/Kg)
MDL
Digested Analyzed Analyst
10.2 0.454 02/02/99 02/03/99 CR
SPECTRUM ANALYTICAL, INC.
Laboratory Report
Client ID: NOHO-105
Lab ID No: AB32350
Matrix Soil
Collected: 01/29/99 by OTO
Received on 0129/99 by MBR
QC and Data Review by
Location: Atwood
Client Job No: J084
Preservative: Refrigeration
Container: 1 Clear Glass Jar
Condition of Sample as Received: Satisfactory
Delivered by: Client
arameter
tal Lead
Total Lead
EPA Method 6010/200.7
Result (mg/Kg) MDL
Digested Analyzed Analyst
9.26 0.450 02/02/99 02/03/99 CR
SPECTRUM ANALYTICAL, INC.
Laboratory Report
Client ID: NOHO-108
Lab ID No: A1232353
Matrix: Soil
Collected: 01/29/99 by OTO
Received on 01/29/99 by MBR
QC and Data Review by
Location: Atwood
Client Job No: J084
Preservative: Refrigeration
Container: 1 Clear Glass Jar
Condition of Sample as Received: Satisfactory
Delivered by Client
Total Lead
EPA Method 6010/200.7
'arameter Result (mg/Kg) MDL
Digested Analyzed Analyst
tal Lead 10.9 0.447 02/02/99 02/03/99 CR
SPECTRUM ANALYTICAL,INC.
Laboratory Report
Client ID: NOHO-11
Lab ID No: AB32356
Matrix: Soil
Collected: 01/29/99 by OTO
Received on 01/29/99 by MBR
QC and Data Review by
Location: Atwood
Client Job No.: J084
Preservative: Refrigeration
Container : 3 Clear Glass Jars
Condition of Sample as Received: Satisfactory
Delivered by: Client
arameter for AB32356
maphthene
maphthylene
thracene
lzidine
izoic acid
no (a) anthracene
tzo (b) fluoranthene
no(k)fluoranthene
no(g,h,i) perylene
no (a)pyrene
nyl alcohol
(2-chloroethoxy) methane
(2-chloroethyl) ether
(2-chloroisopropyl) ether
(2-ethylhexyl)phthalate
Iromophenyl phenyl ether
tyl benzyl phthalate
iloroaniline
iloronaphthalene
lloro-3-methylphenol
;hlorophenol
;hlorophenyl phenyl ether
rysene
)enz(a,h) anthracene
,enzofuran
n-butylphthalate
-Dichlorobenzene
-Dichlorobenzene
-Dichlorobenzene
'-Dichlorobenzidine
Semivolatile Organics
EPA Method 8270
Result (ug/Kg) MDL
Extracted Analyzed Analyst
Not detected 151.0 02/02/99 02/03/99 KS
Not detected 151.0 02/02/99 02/03/99 KS
Not detected 151.0 02/02/99 02/03/99 KS
Not detected 151.0 02/02/99 02/03/99 KS
Not detected 755.0 02/02/99 02/03/99 KS
Not detected 151.0 02/02/99 02/03/99 KS
Not detected 151.0 02/02/99 02/03/99 KS
Not detected 151.0 02/02/99 02/03/99 KS
Not detected 151.0 02/02/99 02/03/99 KS
Not detected 151.0 02/02/99 02/03/99 KS
Not detected 302.0 02/02/99 02/03/99 KS
Not detected 151.0 02/02/99 02/03/99 KS
Not detected 151.0 02/02/99 02/03/99 KS
Not detected 151.0 02/02/99 02/03/99 KS
Not detected 1510.0 02/02/99 02/03/99 KS
Not detected 151.0 02/02/99 02/03/99 KS
Not detected 151.0 02/02/99 02/03/99 KS
Not detected 302.0 02/02/99 02/03/99 KS
Not detected 151.0 02/02/99 02/03/99 KS
Not detected 302.0 02/02/99 02/03/99 KS
Not detected 151.0 02/02/99 02/03/99 K5
Not detected 151.0 02/02/99 02/03/99 KS
Not detected 151.0 02/02/99 02/03/99 KS
Not detected 151.0 02/02/99 02/03/99 KS
Not detected 151.0 02/02/99 02/03/99 KS
Not detected 151.0 02/02/99 02/03/99 KS
Not detected 151.0 02/02/99 02/03/99 KS
Not detected 151.0 02/02/99 02/03/99 KS
Not detected 151.0 02/02/99 02/03/99 KS
Not detected 302.0 02/02/99 02/03/99 ICS
Continued next page..
ammeter for AB32356
Result (ug/Kg) MDL
Extracted Analyzed Analyst
Dichlorophenol Not detected 151.0 02/02/99 02/03/99 KS
Dichlorophenol Not detected 151.0 02/02/99 02/03/99 KS
:thy] phthalate Not detected 151.0 02/02/99 02/03/99 KS
-Dimethlylphenol Not detected 151.0 02/02/99 02/03/99 KS
.Dinitro-2-methylphenol Not detected 755.0 02/02/99 02/03/99 KS
-Dinitrophenol Not detected 755.0 02/02/99 02/03/99 KS
-Dinitrotoluene Not detected 151.0 02/02/99 02/03/99 KS
-Dinitrotoluene Not detected 151.0 02/02/99 02/03/99 KS
•Diphenylhydrazine Not detected 151.0 02/02/99 02/03/99 KS
n-Propylnitrosoamine Not detected 151.0 02/02/99 02/03/99 KS
oranthene Not detected 151.0 02/02/99 02/03/99 KS
orene Not detected 151.0 02/02/99 02/03/99 KS
xachlorobenzene Not detected 151.0 02/02/99 02/03/99 KS
xachlorobutadiene Not detected 151.0 02/02/99 02/03/99 KS
xachlorocyclopentadiene Not detected 151.0 02/02/99 02/03/99 KS
xachloroethane Not detected 151.0 02/02/99 02/03/99 KS
leno (1,2,3-cd)pyrene Not detected 151.0 02/02/99 02/03/99 KS
phorone Not detected 151.0 02/02/99 02/03/99 KS
4ethylnaphthalene Not detected 151.0 02/02/99 02/03/99 KS
ilethylphenol (0-cresol) Not detected 151.0 02/02/99 02/03/99 KS
dethylphenol (p-cresol) Not detected 151.0 02/02/99 02/03/99 KS
phthalene Not detected 151.0 02/02/99 02/03/99 KS
litroaniline Not detected 755.0 02/02/99 02/03/99 KS
litroaniline Not detected 755.0 02/02/99 02/03/99 KS
4itroaniline Not detected 755.0 02/02/99 02/03/99 KS
trobenzene Not detected 151.0 02/02/99 02/03/99 KS
4itrophenol Not detected 151.0 02/02/99 02/03/99 KS
4itrophenol Not detected 755.0 02/02/99 02/03/99 KS
Nitrosodimethylamine Not detected 151.0 02/02/99 02/03/99 KS
Nitrosodiphenylamine Not detected 151.0 02/02/99 02/03/99 KS
ntachlorophenol Not detected 755.0 02/02/99 02/03/99 KS
enanthrene Not detected 151.0 02/02/99 02/03/99 KS
enol Not detected 151.0 02/02/99 02/03/99 KS
rene Not detected 302.0 02/02/99 02/03/99 KS
!,4-Trichlorobenzene Not detected 151.0 02/02/99 02/03/99 KS
1,5-Trichlorophenol Not detected 151.0 02/02/99 02/03/99 KS
1,6-Trichlorophenol Not detected 151.0 02/02/99 02/03/99 KS
ridine Not detected 151.0 02/02/99 02/03/99 KS
methyl phthalate Not detected 151.0 02/02/99 02/03/99 K5
i-n-octyl phthalate Not detected 151.0 02/02/99 02/03/99 KS
Solids 86.4 0A 02/03/99 02/03/99 CD
SPECTRUM ANALYTICAL, INC.
Laboratory Report
Client ID: NO110-11
Lab ID No.:AB32356
Matrix: Soil
Collected:01/29/99 by OTO
Received on 0129/99 by MBR
QC and Data Review by
Location: Atwood
Client Job No.: J084
Preservative: Refrigeration
Container: 1 Clear Glass Jar
Condition of Sample as Received: Satisfactory
Delivered by: Client
Parameter for AB32356
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroform
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dbromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
Volatile Organics
EPA Method 8260
Result (ug/Kg)
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
MDL
31.8
31.8
31.8
31.8
31.8
31.8
31.8
31.8
31.8
31.8
31.8
31.8
31.8
31.8
31.8
31.8
31.8
31.8
31.8
31.8
31.8
31.8
31.8
31.8
31.8
31.8
31.8
31.8
Extracted Analyzed Analyst
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
CD
CD
CD
CD
CD
CD
CD
CD
CD
CD
CD
CD
CD
CD
CD
CD
CD
CD
CD
CD
CD
CD
CD
CD
CD
CD
Continued next page..
Parameter for AB32356
1,1-Dichloropropene
:is-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Elexachlorobutadiene
lsopropylbenzene
4-Isopropyltoluene
Methylene chloride
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
m,p-Xylenes
o-Xylene
Methyl-t-butyl ether
BFB Surrogate Recovery(%)
p-DFB Surrogate Recovery(%)
CLB-d5 Surrogate Recovery (%)
% Solids
Result(ug/Kg) MDL
Not detected 31.8
Not detected 31.8
Not detected 31.8
Not detected 31.8
Not detected 63.6
Not detected 31.8
Not detected 31.8
Not detected 31.8
Not detected 63.6
Not detected 31.8
Not detected 31.8
Not detected 31.8
Not detected 31.8
Not detected 31.8
Not detected 31.8
Not detected 63.6
Not detected 63.6
Not detected 31.8
Not detected 31.8
Not detected 31.8
Not detected 31.8
Not detected 31.8
Not detected 31.8
Not detected 31.8
Not detected 63.6
Not detected 31.8
Not detected 31.8
104
104
100
86.4
0.1
Extracted Analyzed Analyst
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
CD
CD
CD
02/03/99 02/03/99 CD
SPECTRUM ANALYTICAL, INC.
Laboratory Report
Client ID: NOHO-11
Lab ID No.:AB32356
Matrix: Soil
Collected: 0129/99 by OTO
Received on 01/29/99 by MBR
QC and Data Review by
Location: Atwood
Client Job No.: J084
Preservative: Refrigeration
Container: 3 Clear Glass Jars
Condition of Sample as Received: Satisfactory
Delivered by: Client
ammeter
'otal Hydrocarbons(GC) Not detected
Total Hydrocarbons by GC
Modified EPA Method 8100
Result (mg/Kg)
fingerprint based quantificaton:
iasoline
'uel Oil #2
'uel Oil #4
'uel Oil #6
4otor Oil
Igroin
,viation Fuel
)ther Oil
Jnidentified
ro Solids
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
86.4
MDL
Extracted Analyzed Analyst
02/02/99 02/02/99 LR
40 02/02/99 02/02/99 LR
40 02/02/99 02/02/99 LR
40 02/02/99 02/02/99 LR
80 02/02/99 02/02/99 LR
80 02/02/99 02/02/99 LR
40 02/02/99 02/02/99 LR
40 02/02/99 02/02/99 LR
80 02/02/99 02/02/99 LR
02/02/99 02/02/99 LR
0.1 02/03/99 02/03/99 CD
Petroleum identification is determined by comparing the GC fingerprint obtained from the sample with a
library of GC fingerprints obtained from petroleum products. Possible match categories are as follows;
Gasoline-includes regular,unleaded,premium,etc.
Fuel Oil#2-includes home heating oil,#2 fuel oil and diesel.
Fuel Oil#4-Includes#4 Fuel Oil.
Fuel Oil#6-includes#6 oil and bunker"C"oil.
Motor Oil-includes virgin and waste automobile.
Ligroin-includes mineral spirits,petroleum naphtha,vm&p naphtha.
Aviation Fuels-includes Kerosene,Jet A and JP-4.
Other Oil-includes lubricating and cutting oil and silicon oil.
Factors such as microbial degradation,weathering and solubility generally prevent specific identification
within a petroleum category. A finding of"unidentified"means that the sample fingerprint was characteristic of a
petroleum product,but could not be matched to a fingerprint in the library.
After fingerprint identification,the amount present in the sample is quantified using a calibration curve
prepared from a petroleum product of the same category as the identified petroleum. Unidentified petroleum
is quantified using a petroleum calibration that approximates the distribution of compounds in the sample.
A*in the results column indicates the petroleum calibration used to quantify unidentified samples.
SPECTRUM ANALYTICAL, INC.
Laboratory Report(Subcontracted Analyses)
Client ID: NO11O-11
Lab ID No: AB32356
Matrie Soil
Collected: 01/29/99 by OTO
Received on 01/29/99 by MBR
QC and Data Review by
Location: Atwood
Client Job No: J084
Preservative: Refrigeration
Container: 3 Clear Glass Jars
Condition of Sample as Received: Satisfactory
Delivered by Client
ameter
iductance
Result
20
Wet Chemistry Analyses
MDL
1.0
Units Method Start Date Analyst
umhos/cm S205/E120.1 02/01/99 PX
SPECTRUM ANALYTICAL, INC.
Laboratory Report
Client ID: NOHOCOMP
Lab ID No: AB32390
Matrix: Soil
Collected: 01/29/99 by OTO
Received on 01/29/99 by MBR
QC and Data Review by
Location: Atwood
Client Job No.: J084
Preservative: Refrigeration
Container : 2 Amber Glass Jars
Condition of Sampple as Received: Satisfactory
Delivered by Client
Irameter for AB32390
naphthene
naphthylene
hracene
zidine
zoic acid
¢o (a) anthracene
izo (b)fluoranthene
zo (k) fluoranthene
izo (g,h,i) perylene
izo (a)pyrene
izyl alcohol
(2-chloroethoxy) methane
(2-chloroethyl) ether
(2-chloroisopropyl) ether
(2-ethylhexyl)phthalate
romophenyl phenyl ether
yl benzyl phthalate
:hloroaniline
lloronaphthalene
:hloro-3-methylphenol
:hlorophenol
2tlorophenyl phenyl ether
rysene
tenz (a,h) anthracene
,enzofuran
n-butylphthalate
-Dichlorobenzene
-Dichlorobenzene
-Dichlorobenzene
'-Dichlorobenzidine
Semivolatile Organics
EPA Method 8270
Result (ug/Kg) MDL
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not de tected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
144.0
144.0
144.0
144.0
720.0
144.0
144.0
144.0
144.0
144.0
288.0
144.0
144.0
144.0
144.0
144.0
144.0
288.0
144.0
288.0
144.0
144.0
144.0
144.0
144.0
144.0
144.0
144.0
144.0
288.0
Extracted Analyzed Analyst
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
02/02/99 02/03/99 KS
Continued Mitt page..
rameter for AB32390
Result (ug/Kg) MOL
Extracted Analyzed Analyst
Dichlorophenol Not detected 144.0 02/02/99 02/03/99 KS
Dichlorophenol Not detected 144.0 02/02/99 02/03/99 KS
hyl phthalate Not detected 144.0 02/02/99 02/03/99 K5
Dimethlylphenol Not detected 144.0 02/02/99 02/03/99 KS
Dinitro-2-methylphenol Not detected 720.0 02/02/99 02/03/99 KS
Dinitrophenol Not detected 720.0 02/02/99 02/03/99 KS
Dinitrotoluene Not detected 144.0 02/02/99 02/03/99 KS
Dinitrotoluene Not detected 144.0 02/02/99 02/03/99 KS
Diphenylhydrazine Not detected 144.0 02/02/99 02/03/99 KS
t-Propylnitrosoamine Not detected 144.0 02/02/99 02/03/99 KS
)ranthene Not detected 144.0 02/02/99 02/03/99 KS
)rene Not detected 144.0 02/02/99 02/03/99 K5
achlorobenzene Not detected 144.0 02/02/99 02/03/99 KS
achlorobutadiene Not detected 144.0 02/02/99 02/03/99 KS
achlorocyclopentadiene Not detected 144.0 02/02/99 02/03/99 KS
achloroethane Not detected 144.0 02/02/99 02/03/99 KS
mo (1,2,3-cd)pyrene Not detected 144.0 02/02/99 02/03/99 K5
)horone Not detected 144.0 02/02/99 02/03/99 KS
ethylnaphthalene Not detected 144.0 02/02/99 02/03/99 KS
ethylphenol (0-cresol) Not detected 144.0 02/02/99 02/03/99 K5
ethylphenol (p-cresol) Not detected 144.0 02/02/99 02/03/99 KS
hthalene Not detected 144.0 02/02/99 02/03/99 KS
itroaniline Not detected 720.0 02/02/99 02/03/99 K5
itroaniline Not detected 720.0 02/02/99 02/03/99 KS
itroaniline Not detected 720.0 02/02/99 02/0399 KS
tbenzene Not detected 144.0 02/02/99 02/03/99 KS
itrophenol Not detected 144.0 02/02/99 02/03/99 KS
itrophenol Not detected 720.0 02/02/99 02/03/99 KS
ditrosodimethylamine Not detected 144.0 02/02/99 02/03/99 KS
litrosodiphenylamine Not detected 144.0 02/02/99 02/0399 KS
ltachlorophenol Not detected 720.0 02/02/99 02/03/99 KS
:nanthrene Not detected 144.0 02/02/99 02/03/99 KS
:nol Not detected 144.0 02/02/99 02/03/99 KS
ene Not detected 288.0 02/02/99 02/03/99 KS
4-Trichlorobenzene Not detected 144.0 02/02/99 02/0399 Ks
5-Trichlorophenol Not detected 144.0 02/02/99 02/03/99 KS
6-Trichlorophenol Not detected 144.0 02/02/99 02/03/99 KS
idine Not detected 144.0 02/02/99 02/03/99 KS
nethyl phthalate Not detected 144.0 02/02/99 02/03/99 KS
n-octyl phthalate Not detected 144.0 02/02/99 02/03/99 K5
Solids 89.7 0.1 02/03/99 02/03/99 GMM
SPECTRUM ANALYTICAL, INC.
Laboratory Report
Client ID: NOHOCOMP
Lab ID No.:AB32390
Matrix Soil
Collected:01/29/99 by OTO
Received on 01/29/99 by MBR
QC and Data Review by
Location: Atwood
Client Job No.: J084
Preservative:
Container:
Condition of Sample as Received: Satisfactory
Delivered by: Client
?ammeter for A1332390
3enzene
3romobenzene
3romochloromethane
3romodichloromethane
3romoform
1-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroform
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
Volatile Organics
EPA Method 8260
Result (ug/lCg)
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
MOL
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
Extracted Analyzed Analyst
02/02/99 02/02/99 0)
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
Continued next page..
'arameter for AB32390
,1-Dichloropropene
is-1,3-Dichloropropene
rans-1,3-Dichloropropene
?thylbenzene
3exachlorobutadiene
sopropylbenzene
1-Isopropyltoluene
Kethylene chloride
naphthalene
1-Propylbenzene
ityrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
m,p-Xylenes
o-Xylene
Methyl-t-butyl ether
Result (ug/Kg) MDL
Not detected 6.1
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
BFB Surrogate Recovery (%) 101
p-DFB Surrogate Recovery(%) 105
CLB-d5 Surrogate Recovery (%) 98
% Solids
89.7
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
6.1
12.2
6.1
6.1
0.1
Extracted Analyzed Analyst
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99 02/02/99 CD
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
02/02/99
CD
CD
CD
02/03/99 02/03/99 GMM
SPECTRUM ANALYTICAL, INC.
Laboratory Report
Client ID: NOHOCOMP
Lab ID No.:AB32390
Matrix: Soil
Collected: 01/29/99 by OTO
Received on 01/29/99 by MBR
QC and Data Review by
Location: Atwood
Client Job No.: J084
Preservative: Refrigeration
Container: 2 Amber Glass Jars
Condition of Sample as Received: Satisfactory
Delivered by Client
Total Hydrocarbons by GC
Modified EPA Method 8100
arameter
otal Hydrocarbons (GC)
ingerprint based quantificaton:
lasoline
uel Oil #2
uel Oil #4
uel Oil #6
lotor Oil
.groin
wiation Fuel
)ther Oil
Jnidentified
to Solids
Result (mg/Kg)
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
89.7
MDL
Extracted
02/02/99
Analyzed Analyst
02/02/99 LR
40 02/02/99 02/02/99 LR
40 02/02/99 02/02/99 LR
40 02/02/99 02/02/99 LR
80 02/02/99 02/02/99 LR
80 02/02/99 02/02/99 LR
40 02/02/99 02/02/99 LR
40 02/02/99 02/02/99 LR
80 02/02/99 02/02/99 LR
02/02/99 02/02/99 LR
0.1 02/03/99 02/03/99 GMM
Petroleum identification is determined by comparing the GC fingerprint obtained from the sample with a
library of GC fingerprints obtained from petroleum products. Possible match categories are as follows;
Gasoline-includes regular,unleaded,premium,etc.
Fuel Oil#2-includes home heating oil,#2 fuel oil and diesel.
Fuel Oil#4-Includes#4 Fuel Oil.
Fuel Oil#6-includes#6 oil and bunker"C"oil.
Motor Oil-includes virgin and waste automobile.
Ligroin-includes mineral spirits,petroleum naphtha,vm&p naphtha.
Aviation Fuels-includes Kerosene,Jet A and JP-4.
Other Oil-includes lubricating and cutting oil and silicon oil.
Factors such as microbial degradation,weathering and solubility generally prevent specific identification
within a petroleum category. A finding of"unidentified"means that the sample fingerprint was characteristic of a
petroleum product,but could not be matched to a fingerprint in the library.
After fingerprint identification,the amount present in the sample is quantified using a calibration curve
prepared from a petroleum product of the same category as the identified petroleum. Unidentified petroleum
is quantified using a petroleum calibration that approximates the distribution of compounds in the sample.
A`in the results column indicates the petroleum calibration used to quantify unidentified samples.
SPECTRUM ANALYTICAL, INC.
Laboratory Report (Subcontracted Analyses)
Client ID:NOHOCOMP
Lab ID No: AB32390
Matrix: Soil
Collected: 01/29/99 by OTO
Received on 01/29/99 by MDR
QC and Data Review by
Location: Atwood
Client Job No: J084
Preservative: Refrigeration
Container: 2 Amber Glass Jars
Condition of Sample as Received: Satisfactory
Delivered by Client
'meter
ductance
Result
56
Wet Chemistry Analyses
MDL Units Method Start Date Analyst
1.0 umhos/cm S205/E120.1 02/01/99 PX
Spectrum Analytical, Inc.
Laboratory Report Supplement
References
thods for the Determination of Organic Compounds in Drinking Water. EPA-600/4-88/039. EMSL 1988.
thods for Chemical Analysis of Water and Wastes. EPA 600/4-79-020. EMSL 1983.
:thods for Organic Chemical Analysis of Municipal and Industrial Wastewater. EPA 600/4-82-057. EMSL 1982.
st Methods for Evaluating Solid Waste. Physical/Chemical Methods. EPA SW-846. 1986.
mdard Methods for the Examinatinon of Water and Wastes. APHA-AWWA-WPCF. 16th Edition. 1985.
mdard Methods for Comparison of Waterborne Petroleum Oils by Gas Chromatography. ASTM D 3328. 1982.
1 Spill Identification System. U.S.Coast Guard CG-D-52-77. 1977.
mdbook for Analytical Quality Control in Water and Wastewater Laboratories. EPA 600/4-79-019. EMSL 1979.
loosing Cost-Effective QA/QC(Quality Assurance/Quality Control)Programs for Chemical Anslyses. EPA 600/4-85/056.
YISL 1985.
Reoort Notations
Not Detected, = The compound was not detected at a concentration equal to or above
Not Det,ND or nd the established method detection limit.
NC = Not Calculated
MCL = EPA Maximums Contamination Level
VOA = Volatile Organic Analysis
BFB = 4-Bromofluorobenzene (An EPA 624 Surrogate)
p-DFB = . 1,4-Diiluorobenzene (An EPA 624 Surrogate)
CLB-d5 = Chlorobenzene-d5 (An EPA 624 Surrogate)
BCP = 2-Bromo-l-chloropropane (An EPA 601 Surrogate)
TFT = a,a,a-Trj luorotohrene (An EPA 602 Surrogate)
Decachlorobiphenyl = (an EPA 608/8080 Surrogate)
Definitions
Surrogate Recovery=The recovery(expressed as a percent)of a non-method analyte(see surrogates listed
above)added to the sample for the purpose of monitoring system performance.
Matrix Spike Recovery=The recovery(expressed as a percent)of method analytes added to the sample for the
purpose of determining any effect of sample composition on analyte recovery.
Laboratory Replicate=Two sample aliquots taken in the analytical laboratory and analyzed separately with
identical procedures. Analyses of laboratory duplicates give a measure of the preceision associated with
laboratory procedures,but not with sample collection,preservation,or storage procedures.
Field Duplicate=Two separate samples collected at the same time and place under identifical circumstances and
treated exactly the same throughout field and laboratory procedures. Analysis of Field duplicates give a measure
of the precision associated with sample collection,preservaton and storage,as well as with laboratory procedures.
Relative Percent Difference(%RPD)=The precision measurement obtained on duplicate/replicate analyses.
%RPD is calculated as:
%RPD=(valuel -value21* 100%
ave.value
CHAIN OF CUSTODY IZhCUKll a aranaa - - u o
L4})`Rush TAT T-Date Needed: WE 6•
II TATs subject to laboratory approva
24 hour notification needed for rushes.
Page / of • Samples disposed of after 60 days unless
SPECTRUMAHALYTICAL ,t �� �/� 7 other-wised instructed.
OTT) Invoice To: l�(t2� 1 t'l Project No.: �`�V
Report To: ^
Site Name: t'l-1 F(s9C2UC
Location: ,rA ( State:
Project Mgr.: f�ice P.O.No.: RQN:
Sampler(s): J('1 e (t C.\el-) SI
(1=4°Q 2=HC1 3=1-1,S0• 4=HNO, 5=NaOH 6=Me0H 7=
Containers: Analyses Notes:
DW-Drinking Water GW=Ground Water WW=Waste Water H O id, 18
SO=Soil' SL=Sludge 0=Oi1 Xl= X2= ? A A H
• cv 0 a • > d) G ) \C(1'
➢
G=Gmb G-Composite d`
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u fi a) x O O O O W d d vi
Lab Id Sample Id: Date: Time: 2 µ, a x xt a x `...j
V 3
hi a 1 SO 1 1 V'T` ✓ ✓ - ^YJ (\},x.t9 0.1\(uLFS,)
Ash?lt Ut�I(7��b
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AR 7a',n I 17 si.-V-�'a.�i `�`'1) M4L(.A
✓ iz nlr11 I r9 '
AR ' ./B(< ` v. 7('' CO 1\in1 e1
7 Ncllo ID4/ 9 7 t er "�7 Cen„ix,�'iC- ftchto,-lot._
AB )3R{\ k o'10 /�, r
AB,3:act L cA et W 1 y x 0e -ta i, ni4o MC,
AB- zz 1 V � 1a aka ti�6- ru&e 0.,
A8✓A3) MlO�7 'Aet 1 V y- V ✓.s (vf G,,m,
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•
AB d ? ctr1c71) 1 L-- x bn 644,Pit I1,0U )r,t,e,
Date: 'h fu' 2•Al M
Relinquished By: Received By: fr' Y1 rm�:
Additional Instructions: /�
3' 7-- a>(' A Q cl L 4i iC QTIO-`�(A e LL4 , ,-294`. /1.:43-htiu
❑Fax results when available to( )
11 Almgren Drive•Agawam,Massachusetts 01001 •413-789-9018•Fax 413-789-4076
CHAIN OF CUSTODY RE UKU ❑u RushTAT-Date Needed LS 7�
• All TATs subject to laboratory approval;mm.
IR 24 hour notification needed for rushes.
Page a of D-- • Samples disposed of after 60 days unless
SPECTRUM ANALYTICAL ,^' / ,t k 1 Fotherwised instructed.
1 -
Report To: 0 .) Invoice To: NI a i Vy Project No.: tf
/// Site Name: -"E'149 0 cc(
/ A Location: A r State:
Project Mgr.: �[rZ
GS Ai P.O.No.: RQN: Sampler(s): e c I rS r s
64°B! 2=HCI 3=H2SOa 4=HN01 S=NaOH 6=Me0H 7=
Containers: Analyses: Notes:
DW=Prinking Water GW=Ground Water W W=Waste Water y H
.-S SL=Sludge O=Oil X1= X2= b i°
ro O
Z
P. o a
C
G=Grab C=Composite E
> Q U a ,
B x o 0 0 0 o q4 cc
Lab Id: Sample Id: Date: Time: ',$ a a x x u V i 1- C,
1i L-4,--1 ( 1 �-P tu rr 4ato • I ,NJIr i,
AB,j,�, b �D� o Cow P / I�1t i y q G , ( 7 7 V
1 1Ja1.,,-3, ♦uWL„-F
B
Ctnelfv.i� Fur C.vlwi 141
AB l
AB e Aiii i...]7o i 7' rico
AB
t. W ICA 134 fr7 f-r,.)111 D
AB
AB .
AB
AB'
Additional Instructions: Relinquished By: Received By: Date: Time:
❑Fax results when available to( )
I I Almgren Drive•Agawam,Massachusetts 01001 •413-789-9018•Fax 413-789-4076
SPECTRUM.ANALYTICAL,LNC.
Massachusetts Certification M-MA 138
Connccticut Approval#PH 0777
Rhode Island#98&Maine#n/a
New Hampshire ID#2538
New York ID#11393
Florida HRS87448
O'Reilly, Talbot&Okun
293 Bridge Street, Suite 500
Springfield, MA 01103
June 2, 1999
Client Project Not 84-05-17 Location: Atwood Drive - Northampton, MA
Lab ID No
AB44666
Client to
STOCK-1
Analysis Re[11rwctrcl
TCLP Lead
or-ed.b
u /
bal •ye
Presiden orator irector
ENVIRONMENTAL ANALYSES
I 1 Almgren Drive • Agawam,Massachusetts 01001 • 413-789-9018 • FAX 413-789-4076
SPECTRUM ANALYTICAL, INC.
Laboratory Report(Subcontracted Analysis)
Client ID: STOCK-1
Lab ID No: AB44666
Matrix: Soil
Collected: 05/27/99 by OTO
Received on 05/27/99 by KC
QC and Data Review by MD
Location: Atwood Drive-Northampton,MA
Client Job No: 84-05-17
Preservative: Refrigeration
Container: 1 Amber Glass
Condition of Sample as Received: Satisfactory
Delivered by: Client
rameter
P Lead
TCLP Lead
EPA Method 1311/SW846 6010
Result (mg/L) MDL
3.23
Extracted Analyzed Analyst
0.010 06/01/99 06/02/99 CR
CHAIN OF CUSTODY REUUKll u
Rush TAT-Date Needed: (.7///214/4
• All TATs subject to laboratory apyrovai;min.
III 24 hour notification needed for rushes.
Page(of / • Samples disposed of after 60 days unless
SPECTRUM ANALYTICAL otherwised instructed.
0 Project No.: Ci c( i^)5 ( 7
Report To: ( �T Invoice To: (� 1 �i r
Site Name: �kTOVnO"/, (JT. f 54
Location: Alf d`4k(Mve. rS-oan State:44LL
Project Mgr.: A. It
.< • • P.O.No.; RQN: Sampler(s): /f Adhr-(, "
(144°C 2=HC1 3=H2SOs 4=HN0, 5=NaOH 6=MeOH 7= Containers: Analyses: Notes:
DW=Drinking Water GW=Ground Water WW=Waste Water IT
0 IT
SO=Sail Sf=Sludge 0 0i1 X1= X2= - A
> C7
d = 'P
G=Grab C=Composite i O E R n
1 i > d 0 w
s' x O O O O iv
Lab Id: Sample Id: Date: Time: $_ a w 4t 4t u
bii
.ABIAT104 S •Cue k- i .51;4://q1 C S! 1 / _
AB
.
AB
AB-
AB
AB
AB
AB
AB
Additional Instructions:_ Relinquished B Received By: Date: Time:
7� I/l. ,t 4\ "'WAA,-cdttedera—_ IA 7/91 /G•7=07
❑Fax results when available to( )
11 Almgren Drive•Agawam,Massachusetts 01001 •413-789-9018•Fax 413-789-4076
Massachusetts Department of Environmental Protection
Bureau of Waste Site Cleanup
BILL OF LADING(pursuant to 310 CYR 4toos0
8WSC-o,
Imams Taman/
�I LRA
E. RECEIVING FACILITyfTEMPORARy STORAGE LOCATION(continued):
Temporary Storage Address:
Street
City/Town.
F. DESCRIPTION OF REMEDIATION WASTE:
(check all that apply)
® Contaminated Media(circle all that apply):
❑ Contaminated Debris(circle all that apply):
Inorganic Absrbant Materials
Sate: Zip Code:
GmuMwaaor Swims Water - Otter:
Demoilion/Coastrurath Waste Vegetation/Organic Materials
❑ Non-hazardous 00000th nedzed Waste(drrde al that apply): Non-aqueous Phase Uquid Otter:
❑ Non-hazardous Containerized Waste(ekde al that apply): Tankeottms,Sludges Container: Drums
Engineered Impoundments Other: -
Type of CanbminaEan(circle al that apply): Gasoline Diesel Fuel *2 ell *4 Oil e6 OR Waste 01
kerosene Jet Fuel otter; Soil with lead above reportable standards
Estimated Volume of Materials: Cubic Yank: 1 S - Tons: Other:
Contaminant Source(check anaspecify): ❑ Transportation Accident ❑ Underground Storage Tank ®Omer. VA A wit w.A
Response Actin Associated with Bill of Lading(circle rue): immediate Response Actin Release Abatement Measure
Utility-Related Abatement Measure (linked Removal Action(LAA)-3/4) Comprehensive Response khan
Other(specify):
Remediaticn Waste Characterization Support Documentation attached:
❑ Sine History Information ❑ Sampling act Analytical Methods and Pbcedmes ❑ Laboratory Data ❑ Field Data
paabueN to DEP..
If supporting dooumenthicn k not appended,provide an attachment stating the date and h comedian will what document such information
was submitted
-
G. LICENSED SITE PROFESSIONAL(LSP)OPINION: -
Name of Organization: O'Reilly. Talbot R (Alin Assnri at es
LSp Name: Bruce R. Nickelsen Tdle: Assnriatp
Telephone: 413 — 788 --6222 Ext
attest that I have examined and am familiar MN lye hbnnaaoe mashed h Nis submittal,including any and documents accompanying all the sgrMani of care IO2((1)Ld in my pafmabnal spirant mid}agmencaasm upon application of
(1)the applicable provisions of 309 CMR 4.02(2)and(3),and
(inn the provisions of 309 CMR 4.03(5L -
to the best of my knowledge,Information and belief,lye assessment actions undertaken b daractedxe Vie Remedtans°
Waste which is(are)the subject of this submittal for awe coney with the
•provisions of 310 CMR 40 0000,and aids facility p.nnptbd to accept Remediation Waste having he
possible ones and
described In this submittal. 1 am aware that significant penalties may remit,Including,but notlmkted b.
pkomnent,k I submit kdommtlon wbIth 1 know b be false,Inaccurate or materially Incomplete.
Signature: r AL VA' /,�.LC lfu
Date: 9 /S. / 99
License Number. 9000
Seal:
evsee 10/154 ms ram ISpromo on tecyaeo paper.
id OF M
3 'kr/
BRUCE H
o NICKELSEN
No 9000
Fy• 9Fn'ISTE,
Jf0SflE pROi •
k
Massachusetts Department of Environmental Protection
L3WSC-012A
0....T tlip N.G.".
Bureau of Waste Site Cleanup
BILL OF LADING(pursuant to dtG CMR 48.aaw) '
•
-
LRA
CATION OF SITE OR DISPOSAL SITE WHERE REMEDIATION WASTE WAS GENERATED:
s Name(optional):
Atwnnd naive Location Aid. End of Cul-de-sac
Northampton ZIP Doris' 01060 _
wn:
erica of Generation: 5 / 27 / 99 to /_ /_
_
nal Release Tracking Numbers Associated vdth this BIG of Lading:
Note: El this Bill of Lading 1s the rest&d8 Limited Removal Action(LRA)taken prior to Notification,a Release Tracking
Number knot needed.
RSON CONDUCTING RESPONSE ACTION ASSOCIATED WITH BILL OF LADING:
A Organization: city of Northampton
of Contactwa Pp nen • Title.
yno
(`ity Hall 710 MainStre&
_
iwn: Northampton stain: HA zp Code- 01060
one: 413 -587 - 1265 Ext.
IELATIONSHIP TO RELEASE OR THREAT OF RELEASE OF PERSON CONDUCTING RESPONSE ACTION
SSOCIATED WITH BILL OF LADING:
'.one/specify)
Owner Operator Generator Transporter Other RP:
IP Shoofly(circle one):
'RP Specify one): Owner Operator Generator Transporter Other PRP:
(circle
an attachment the name,cornea
iduciary/Secured Lender
gency/Publiic Utility on a Right of Way
Mier Person:
)wnar and/or operator is not conducting the response action associated with the Bib of Lading,provide on
n.address and telephone number,including any area ode and exwSon,far each,If known.
RANSPORTER/COMMON CARRIER INFORMATION:
/Gammon Canter Name: tie Ste S ie✓S d" So:a En c
porter
btPerson: lktdc Q,SJoS.e1't TNe:
t Z2 C (1.a.rf;rrx IAA: ✓-c
0 f07 0 -
town: C (%t cog t t State- ft-4 a zp Code-
.L
hone: I LLI— 59 3 - S'(5 ( Ext.
IECEIVING FACILITY/TEMPORARY STORAGE LOCATION:
abriFacety Name: City of Northampton Landf 111
act Person: Peter McEr lain - TNe: Health Agent
It Board of Health, 210 MIN Street
01060 _
rown: Northampton State' MA Zip code:
)hone:`fi — CS 7 - /, /\ Ea
of FacaGly: • Aspaaf Batd✓Cok1 Mx • Landfill/Disposal ❑ Incinerator
*one) 0 Asphalt Batch/Hot Aix k7 Landfill/Daily Cover • Temporary
• Thermal Processing • Landfill/Structural RA ❑ Storage
Other:
:ion of Hazardous Division of SdId Waste 96-214-002 EPA ldentieration
A Permit re Management Permit&:.
7,
&:
te/Class
Period of Temporary Storage(specify dates if applicable): NA /_ /_ to _
/_
iaVAnedpated
Temporary Storage(d applicable): NA
son for
sed 10(1/94
ins norm is pnnrea on recyc)ea paper.
Page lo
Massachusetts Department of Environmental Protection
Bureau of Waste Site Cleanup
BILL OF LADING(pursuant to 310 t]4R 40.0030)
BWSC-012A
noawam«rareuaabon
LRA
TTIFlCATION OF PERSON CONDUCTING RESPONSE ACTION ASSOCIATED WRH THIS BILL OF LADING:
under canaries of lax that I have personalty examined and am familiar with the hlwmation contained h Ids submittal,including any and
meets accompanying this certification.and that,based on my Ingdry of Chose individuals Immediately responsible for obtaining the
don,the matedal hbmatbn contained herein Is,to the best of my Ioaaandge and belief,bue,accurate and complete. I an aware that
re signmcant penalties. including, but not limited to, possible fates and Imprisonment, for wilfully submitting false, Inaccurate, or
eta,formation.
re: Vri o'r %1 /" _ * Date: /L /447
Pt Person(print). w 14/NE M. FES-
* As Agent for the City of Northampton
.ed 10/194 1 ms form is punted on recycled paper.
Page 3013
Massachusetts Department of Environmental Protection BWSC-0128
Bureau of Waste Site Cleanup aa.s Tracking Montan
BILL OF LADING(pursuant to 310 CMR 4&0030)
LRA
LOG SHEET of
W INFORMATION:
1: Signature of Transporter Representative: Receivin FaciRy/Temporery Storage Representative:
A Shipment Time of Shipment Dale of Receipt Time of Receipt:
/_7 /_a_4 : (circle ore)am/pm /__S- /___21 / : 1a-
___1_ _ _Z.
rrac//ror L Registration: Trailer egistration (f any): (circle one)am/pm
0-0 O Load Size(cu.yds/bans): /S.(I
,I
1- r
1G
2: Signature of Transporter Representative: Receiving Facility/Temporary Storage Representative:
if Shipment: Time of Shipment - Date of Receipt: Time of Receipt:
/ / (circle one)aMpm /_ /-
_
tractor Registration: Trailer Registratico(if any): _ (circle one)am/pm
Load Size(cu.yds/tons):
i 3: Signature of Transporter Representative: Receiving Facility/Temporary Storage Representative:
a Shipment: Time of Shipment: Date of Receipt: Time of Receipt
/_ /_ (circle one)am/pm /_ /
_ _
Tractor Registration: Trailer Registration(if any): (circle one)am/pm
Load Size(cu.yds./tors):
)4: Signature of Transporter Representative: Receiving Fadtiry/Temporary Storage Representative:
at Shipment: Time of Shipment: Date of Receipt: Time of Receipt:
/_ /_ (circle one)am/pm /_ /—
—
Tractor Registration: Trailer Registration(if any): (circle one)anVpn
Load Size(cu.yds/tons):
)5: Signature of Transporter Representative: Receiving Facility/temporary Storage Representative:
of Shipment: Time of Shipment
/_ /_ • _ (drde one)an/pm
Tractor Registration: Trailer Registration Of any):
Date of Receipt: Time 01 Receipt
/_ /_
_
(circle one)am/pm
Load Size(cu.ydsJQih):
D 6: Signature of Transporter Representative: -
of Shipment: Time of Shipment
/_ /_ _ (circle one)arn/pm
/Tractor Registration: Trailer Registration Of any):
Receiving FacmryRempomry Storage Representative:
Data of Receipt: Time of Receipt
/— /_ •
_
(circle one)ampm
Load Size(cu.yds/tons):
D 7: Signanre of Transporter Representative: Receiving Facility/Temporary Storage Representative:
i of Shipment: Time of Shipment
/_ /_ (circle one)am/pm .
iTractor Registration: Trailer Registration()f any):
Date of Receipt: Time of Receipt
/_ /— •
_
(drde one)am/pm
Load Size(cu.yds/tons):
.0G SHEET VOLUME INFORMATION:
Total Volume This Page(cu yds.rtans):
Total Carried Forward(cu yds/tons):
Total Carded Forward and This Page(cu.ydsltons):
;ad 10/1434
11713 1033115 prnea tin/9CyU6o paper.
Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Waste Site Cleanup
BILL OF LADING(Pursuant to 310 CMR 40.0030)
SUMMARY SHEET
❑-I
BWSC-012
RS.a..Tt.npNurn
LRA
L ACKNOWLEDGEMENT OF RECEIPT OF REMEDIATION WASTE AT RECEIVING FACILITY OR TEMPORARY STORAGE
LOCATION:
Receiving Location Reprersentatl'w(pr a : o fl % /r MP(`
� 04-NdFiL`-1me:
Signature:
Date: —L/y /i
M. ACKNOWLEDGEMENT OF SHIPMENT AND RECEIPT OF REMEDIATION WASTE BY PERSON
CONDUCTING RESPONSE ACTION ASSOCIATED WITH THIS BILL OF LADING:
1 certify under penalties of law that 1 have pasonany examined and am laminar with tie bktmation oomained N is submittal,including any alp
all documents accompanying this cemacanon, and Mat, based on my Inquiry of those Individuals Immediately responsible or obtaining Me
information,the melarht intimation contained harem Is.to the best of my knowledge and belief,mire.accurate and complete. 1 am aware that
acre area significant pomades,des. h• but not 6nRed to, possible fines and impdsormant. or wilfully submitting false, inaccurate, or
Signature:
71-{R"rL .0 Dare: /_ /-17
Name of Person(prat): FR4r'/K 3 frARA y((i 4-1/
Revised 10/1/94
fns TOM s pnntea m recyaaa paper.
Page 2
Massachusetts
Department of Environmental Protection
of Waste Site Cleanup
OF LADING(Pursuant to 310 CMR 40.0030)
SHEET • of
BWSC-01 2C
R.w..n.asN Numb.:
Bureau
BILL
SUMMARY
LRA
iUMMARY OF SHIPMENTS:
E OF SHIPMENT:
DATE OF RECEIPT:
NUMBER OF LOADS SHIPPED:
DAILY VOLUME SHIPPED(CU.YDS/TONS):
•
SUMMARY
L OF LADING TOTALSHIPPED
SHEET TOTAL SHIPPED:
(only it different):
_ ___---_...._.,_...—. OrNa 1 n(,
sed 10/194
r
Iran No: 12218 NORTHAMPTON Date 09/09/9`7 ON REV . LANDFILL Time in 13: 32
mos 210 NORTHAMPTON ,OT .
NORTHAMPTON , MA 01060 Time out 13 : 44
Gross- 68680
ma
CUS OME 0025 care : 37040
CUSTOMER CO25 CLEAN FILL. Net : 2,1.040
OWNER CO28 CLEAN FILL.
HAULER 0025 CLEAN FILL
aTiAIEkIAL 07 CLEAN FILL Net onF;: ]_ 82
Price/Ton - 0 ea
7perator FRANK KARAKULA
r t lo Char 6;r: 0 .00
Comment /-i�/'-� ��'//I/�,'
b1'riff t u rte' C_ l
imm
ma
ims
ow
v
Tran No : 12218 NORTHAMPTON REG. LANDFILL Date 09/09799
210 MAIN ST . Time in 13 :32
NORTHAMPTON , MA 01060 Time out 13 : 44
Gross: 66680
CUSfOME 0025 Tare: 37040
OWNER 0025 CLEAN FILL Net: 31640
OWNt:R 8025 CLEAN FILL Net:
HAULLR 0025 CLEAN FILL
GLEAN FILL Net Tons: 15 .88
MATERIAL 07 Price/Ton . 0 .00
Operator FRANK KARAKULA
lot Char na 0 .00
Comment ,
r �� J//�
Signature _,_ :N` .A� 1 " _` - ' " .__
•
o
•
• WASTE MANAGEMENT [ 310N
MICHIGAN DEPARTMEN i OF
— ENVIRONMENTAL QUALITY
Pan 121 of wet 451,1091 ais amended.
• Failure to file may subject you to
DO NOY'WRITE IN THIS 5..,CE criminal and/or civil penalties under
Sections 32611151 or 324.12116 MCL.
ATT.D DIS. D REJ. 0 PR.D
Form App oved. OMB No.2050.0039
or type.
in
UNIFORM HAZARDOUS
WASTE MANIFEST
L GitinaIlgYS U3IEPA ID No. Manifest
Wl1iQUUV105 2 D t No.
8i
2. Page 1
of 1
Information in the shaded areas
law.not required by Federal
cfY6r RuG 1d big A to, � p, z F✓
A State Manliest Document Number
MI 7404681
210 HAIN ST. NORTHAMPTON, MA 01060
Generator's Phone I 413 1 587-1265
B. State Generators ID : A't OD DR.
NORTHAMPTON, MA
Transporter 1 Com any Name 6. US EPA ID N bet
OIL RECOVERY CORP. ` HAD 985 294 693
C. State Transporter ID
D.Transporters Ptione419L737-2949
Transporter 2 Company Name 8. US EPA ID Number
1
E. State Transporters ID
F.,Transperter'c Phone
. Desi noted Facili Name and Site
C�f—HE'I SSItVICHS INC.
Address 10. US EPA ID Number
G $fate Facility's ID
rAw 2 4,b+r., -
18550 ALLEN ROAD
BROWNSTOWN, MI 48192 I HID 096 963 194
H. Facility's Phone 2/
73F-282-9250 , .
Proper Shipping
1. US DOT Description (including 1D NUMBER). Name, Hazard Class,and
12.Containers
No.
Type
13.
Total
Quantity
14
Unit
WWoI
1 Waste
No.
�,,
HM
RQ,NAZARDODS WASTE SOLID, N.O.S..(D008,LEAD),9,
RA3077 PG III
oo5cf
o60,000�
. .: „.,
noo8
G
.. . .. _.. . .. ...; '.,IK
Handing Case:
J. Add"d'�1 al scriptions for Matenal
l� S`/.z-0
b
C
15. Special Handling Instructions and Add bona/Information
f ERG 1#171 24 8H. PHONE:617-523-7740 SEND COPY OF NAND% W/INV.
16. GENERATORS CERTIFICATION:I hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and are classified,
packed,marked,and labeled,and are in all respects m proper condition fort ansport by highway according to applicable international and national government regulations-
If 1 am a large quantity generator, 1 certify that I have a program in pi ce to reduce the volume and toxicity of waste generated to the degree I have determined
to be economically practicable and that I have selected the racticable method of treatment, storage, r disposal p currently available to m which minimizes iz s the
present cand future threat to human health and the environment; OR; i I am a small quantity generator, I have made a good faith effort to min. my ware
generation and select the best waste management method that is available to me and that I can afford.
Date
Printed/Typed Name
Lifyrze -o:o:. 45 47t"l . c -/
17. Tran}porter 1 Acknowle emen)of Receipt of M'^ -'°
Prihted/FYP;'
Signature
Month Day Year
h A-=I AA )
Date
Sign
18. Transporter 2 Acknowledgement a Receipt of Material
Printed/Typed Name
D
Signature
Month Day Year
IIIIII
9. Discrepancy Indication Space
20. Facility Owner or Operator:Certification of receipt of hazardous materials covered by this manifest except as noted
Item 19.
Printed/Typed Name
Signature
Date
Month Day Year
CHEM-MET SERVICES
-•■• 18550 ALLEN ROAD
BROWNSTOWN, MI 48192
c , #. 046142
Phone: 734-282-9250
EPA#MID096963194
CERTIFICATE OF DISPOSAL
This certifies that the waste(s) specified on MANIFEST NUMBER : 14174046 81
AND TRANSPORTER: MRD985^94693
OIL RECOVERY CORPORATION
?OR GENERATOR: MAR000010512
NORTHHRMPTION, CITY OF
201 MAIN ST.
RTWOOD DR.
NORTHHRMPTON, MR 01060
las been properly disposed of under the authority of all required and applicable permits and licenses,
:o my best knowledge and belief based on my inquiry of individuals immediately responsible for the
waste disposal.
The waste identified above has been handled in compliance with one or more of the
applicable performance standards specified in 40 CFR, part 268, subpart D and all applicable
prohibitions set forth in 40 CFR 268.32 or RCRA section 3004 (d).
Signature:
Date: 09-30-1999
WHOLLY OWNED SUBSIDIARY OF PERMA-FIX ENVIRONMENTAL SERVICES, INC.