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Bill of Lading 1999 O'Reilly, Talbot & Okun I A S S O C I A T June 15, 1999 File No.J84-05-17 Mr. Peter McErlain Health Agent City Hall 210 Main Street Northampton, MA 01060 EnvironmentalSafetyHealthGeotechnical t 293 Bridge Street E S ] Re: Bill of Lading Atwood Drive Northampton,MA Dear Mr. McErlain; Suite 500 Springfield, MA 01103 Tel 413 788 6222 Fax 413 788 8830 Email offieec otoenumm Included with this letter is a copy of our Bill of Lading for soil to be reused as daily cover at the Northampton Landfill. The original Bill of Lading (with signatures) will come to you with the soil. The soil is from a Limited Removal Action (LRA) which has been performed at Atwood Drive in compliance with the Massachusetts Contingency Plan (MCP). A site locus and site plan showing the location of the excavation are provided as Figures 1 and 2 respectively. In compliance with Massachusetts DEP Policy No. COMM-97-001 regarding reuse and disposal of contaminated soils at Massachusetts Landfills, the following background information is provided. Quantity of Contaminated Soil Approximately 15 yards of soil will be transported to the Landfill. Description of Source and Type of Release and Contaminants The source of the release of contaminants is not known. The lead identified at the site which exceeds the RCS-1 standard of 300 mg/kg was detected in fill. The fill is believed to have been placed at the site in the 1960s during construction of the adjacent Interstate 90. Description of Current and Former Site Usage The site is currently vacant. Prior to placement of fill on the site it may have been agricultural. Chemical Data Chemical characterization data for the soil to be reused at the landfill are summarized in Table 1. Analytical data sheets are appended with Table 1.As shown, all the analyses meet the criteria for reuse at a landfill Lead was above the theoretical level at which TCLP criteria may be exceeded (100 mg/kg), so the sample was tested for TCLP lead. A concentration of 3.23 mg/I, below the 5 mg/1 standard was detected. O'Reilly, Talbot & Okun 0-1 [ A S S O C I A T E S ] Physical Description of the Soil The excavated soil was described as a brown fine to medium sand with some brick fragments and trace silt, using the burmister soil classification system. Based on the brick fragments the soil appeared to be fill. This letter and accompanying Bill of Lading should provide all the information you need to evaluate the soil for reuse at the Northampton Landfill. Please give me a call if you have any questions or comments. Very truly yours O'Reilly,Talbot&Okun Associates, Inc. Bruce H. Nickelsen Associate cc Wayne Feiden, Ellen Freyman Attachments Page 2 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BILL OF LADING(pe.wm te 310 CUR 40.0030) BWSCL012A R+rwwwaq Number: E. RECEIVING FACILITY/TEMPORARY STORAGE LOCATION(dontmed): Temporary Storage Address: Sheet City/Town. F. DESCRIPTION OF REMEDIAT(ON WASTE: (check all that amity) 9 Contaminated Media(circle at tat apply): Grpxp(vagr SurfaceWalu ' Other ❑ Contaminated Debt(circle at that apply): Oar n/Consmr a,Waste Vegetation/Organic Materials lnogadcAbsorbent Material - Other: i -- - - ❑ Non-hazadous Unconramerned Waste(cam at that apply). Non-aqueous-Phase Liquid- Other - - ❑ Nonhazardous Co0taineized Waste(cide at that apply): -Tank BolbrnwSludgea Containers Drums Engineered impoundments Other: - Type of Contamination(cam al that apply): Gasoline Diesel Fuel 92 OS #4 Oil tats OS Waste Os Kerosene- Jet puss. Omer. Soil with lead above reportable standards Estimated Volume of Materials: Cubic Yards: 1 S Tan) Other Contaminant Sande(check onefspecIfy): ❑ Transportation Act/dent ❑ Underground Storage Tank El Omer: VA K Na w ix Response Action Associated with SW of Lading(circle ate): immediate Respite Action Release Abatement Mew. Utility-Related Abatement Measure (Limited Removal Action(LRAb Comprehensive Response Amon Other(specify): Remedied.Waste Characterization Support Documentation attached: ❑ Site History Information ❑ Sampling and Anayttat Methods and Pmledaes ❑ Laboratory Data ❑ Field Screening De la was previously submitted to DEP. app.Led,provide aa attachment staling um team and in connection with what document such Information Zip Code: G. LICENSED SITE PROFESSIONAL(LSP)OPINION: Name cfOrganizalon: Q'Rei fly Talhnt R ninth Ansnriates up Name. Bruce H. Nickelsen Two: Accnci ate Telephone: 413 - 788-6222 Exl - - -_- I hat have p�yexamined and am fanlike with the Intermaan caned hml submittal,Mcleang any a and if fesalanel.44. srq jtlgman(basm Won ePPOGt.at(q thestandardof ease i t e applicable provlstons of 309 OMR 4.02(2)and(3).and to ore best the proud of 309 CMR 4.03(5), Waste width my knowledge.Informal/on and betel,the assessment action ralderta en to dsecSrne tle Remedltmh ( ) subject of Ids submittal nor ply at the•Pmvlbrs of 310 CMR 40.0000,and such Baby Is permitted b yamopt Renedetoi haa'WnagySte described In this submittal. I an awes that Mailicant penalties may result.btim:am but not Wind to. passible lines and Imprisonment If I submit Information which I know to be false.Inaccurate or materially incomplete. Signature- Date: / /_ License Number. 9000 Revised 1 Seal: prate°.NC yuao papa. W Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSO-01 2A MONO li.e.•a D E P BILL OF LADING(pursuant to 310 CUR 40.0030) -I LRA J LOCATION Leese Name • OF SITE OR DISPOSAL SITE WHERE REMEDIATION WASTE WAS GENERATED: (optional) - .. Atwnnd naive Lacetlon Net End of Clil-de-sac rest - Northampton rip Code: 01060 _ " ty/Town: ate/Period of editlanal Release Generation: 5 / 27 / 99 m _/_ /_ Tracking Numbers Associated with this Bill of Lacing: Nom: tlMk SW of Lacing is the resatoa United Removal Adhn(LR4)taken prior toNotliutlal.a Release Tracking Numbers not needed . PERSON ame of Organization: ame of Contact treat CONDUCTING RESPONSE ACTION ASSOCIATED WITH BILL OF LADING: City of Northampton Too sin clan Title: yna City Mall 71n Mainstreet _ ky/Town: Northampton scam: MA 0.p Code: 01060 alephane: 413 -587 - 1265 Ext :. RELATIONSHIP ASSOCIATED Mock orwhpedfy) E RP Specify E PRP Specify J Fiduciary/Secured D Agency/Public Other Person: d an amer and/or person,address TO RELEASE OR THREAT OF RELEASE OF PERSON CONDUCTING RESPONSE ACTION WITH BILL OF.LADING Owner Operator Generator Transporter Other RP: (circle one): Owner Operator. Generator Transporter. Other PRP: (code one): an atachnent Lender Utility on a Right of Way operate*le not concluding the response action associated with the 0.I of Lading,provide on and Wantons number.incbdbg any area code and extension.foe each.If bown. the name,contact ). TRANSPORTER Transporter/Common Contact Person: Street /COMMON CARRIER INFORMATION: Cartier Name: - Tltlo• - gp/Town: Telephone: stem: Zip Code: _ Ext _– E. RECEIVING Operamr/FacaW Contact Person: sweat Board FACILITY/TEMPORARY STORAGE LOCATION: ' Name: City of Northampton Landfill Peter McErjatn , Tide; Health Agent of Health, 210 MIN Street 01060 _ city/Town: Telephone: Type of Fealty: (check one) Division of Waste/Class Actual/Anticipated Reason for Northampton - stm: . . MA Zip Code: – Ext. _–_ ■ Asphalt Battvcoid Mix ■ Lanai/Disposal ❑ Indnerato ❑ Asphalt Batch/Hot Mx M landMl:Mt/Cover ❑ Temporary ❑ Thermal Processing ❑ landlaSWctJral RN ❑ Storage Other. Hazardous Division of Solid Waste A Permit a: Management Perm*a:. 96-214- 002 EPA Identification*: / _ — /— Period of Temporary Storage(specify dates If amicable): NA /_ /_ to NA Storage Temporary Td applicable): Revised 10/1/94 Ions roan Ammo on todyaecpaper. age 10 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BILL OF LADING 0xwsura to 310 CUR 40.0030) BWSC-012A Re n.d**Numbin LRA 7 CERTIFICATION OF PERSON CONDUCTING RESPONSE ACTION ASSOCIATED WITH THIS BILL OF LADING: fray under penalties of law that I have pinion*examined and am familiar with the bfamatian contained b this submittal,inducing any and documents accompanying this cetficadon.end that eased on my inquiry at those Individuals brmediataN responsible for obtaining the serration,the material Ntommlion contained herein ta,to the best of my knowledge end belief,toe.acaaata aM.canpleta. I an ware that we axe significant penalties. Including, but not Sated to, possble fines and imprisonment for wilfully submitting false. Inaccurate, or amplete information. Inaere: nit of Person(print). * As Agent for the City of Northampton * Date: eva foam ns prated on recycled paper. I age "4 Massachusetts Department of Environmental Protection BWSC-0128 Bureau of Waste Site Cleanup Mere Trstled NmM BILL OF LADING(pursuant to 310CUR40.0.30) n_I LRA II LOG SHEET OF LOAD INFORMATION: )AD 1: Signature of Transporter Representaive: ate of Shipment Time of Shipment /_ /_ (aorta one)am/pm ecWTracmr Registration: Trailer Registration Of any): Receiving FadityrTemporary Storage Represxfadve: Date of Receipt Time of Receipt: Load Size(cu.yds./tons): (drab one)am/pm DAD 2: Signature of Transporter Representative: ate of Shipment. Time of Shipment /_ (circle one)am/pm uoWTractor Registration: Trailer Registration Qf any): Receiving Fadity/Tempcmry Storage Representative: Date of Receipt. Time of Receipt /— /_ (circle one)anipm Load.Size(cu.ydsfons): DAD 3: Signature of Trarsp:der Representative: late of Shipment lime of Shipment (circle one)am/pm ix W Tractor Registration: Trailer Registration(if any): Receiving Fadlty/Temporary Storage Representative: Date of Receipt /_ /— Load Size(cu.ydsJrons): Time of Receipt • (cirde one)am/pm OAD 4: Signature of Transporter Representative: )ate of Shipment: Time of Shipment (circle one)an/pm ruck/Tractor Registration: Trailer Registraion Of any): Receiving Fadity/Temporary Storage Representative: Date of Receipt Time of Receipt /_ /_ Load Size(cu.yds/tors): (circle one)am/pm DAD 5: Signature of Transporter Representative: Date of Shipment Time of Shipment /_ /_ — (circle one)am/pm • fruci/Trador Registration: Trailer Registration Qf any): Receiving Faciity/remporary Storage Represrntative: Date of Receipt: _/— /— Load Size(cu.ydsAor6J: Time of Receipt (circle one)am/ptl LOAD 6: Signature of Transporter Representative: Date of Shipment lime of Shipment /_ /_ • (ciao one)ant/pm- Truck/Tracbr Registration: Trailer Registration Qf any): Receiving Facility/Temporary Storage Representable: Date of Receipt Tine of Receipt /_ (circle one)run/pm Load Size(cu.ydsfbns): LOAD 7: Signature of Transporter Representative: Date of Shipment: lime of Shipment Tn¢t/Traabr Registration: (circle one)am/pm , Trailer Registration Of any): Receiving Facility/Temporary Storage Representative: Date of Receipt: _ /— /— Load Size(cu.ydsibns): Time of Receipt (circle one)em/pm J. LOG SHEET VOLUME INFORMATION: aeased 10/194 Total Volume This Page(cu yds.nons)' Total Carried Forward(al yesfons): Total Carried Forward and This Page(ou.ydsAtons): HIS loam ispnarea on recydea paper. Page 1 at Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BILL OF LADING(purulent to am CMR 480030) SUMMARY SHEET BWSC-01 2C Immo m.Aaatasram LRA L ACKNOWLEDGEMENT OF RECEIPT OF REMEDIATION WASTE AT RECEIVING FACILITY OR TEMPORARY STORAGE LOCATION: ReceM,g Maly/Temporary Location Representative(print): me: Signature: - Date M. ACKNOWLEDGEMENT OF SHIPMENT AND RECEIPT OF REMEDIATION WASTE BY PERSON CONDUCTING RESPONSE ACTION ASSOCIATED WITH THIS BILL OF LADING: 1 certify under penalties of law that I.have personally examined and am famwlar with the information contained In this submittal,Including any and an doormen accompanying this certification, era tat, based on my inquiry of those individuals Immediately responside for obtaining the information,the material information contained herein Is,to the best of my IeoMedge and beset,true,acaaaa and complete. I am aware that there are significant penalties, Including, but not Mated to. possible fines and Imprisonment, for wilfully submitting false, Inaccurate, or Incomplete Information Ifutly ng Signature: Name of Person(print): Revised 10/1/94 Mlle: mu tom a puma on recypuu papa. Page 2 of 2 4.11111\ Massachusetts Rr4 * Bureau Department of Environmental Protection of Waste Site Cleanup OF LADING(pursuant to 310 GAR ao.odan) SHEET of BWSG0120 Rases inecking Nim le: _ BILL D E P SUMMARY ❑—) LRA K. SUMMARY OF SHIPMENTS: DATE OF SHIPMENT: DATE OF RECEIPT: NUMBER OF LOADS SHIPPED: DAILY VOLUME SHIPPED(CU.YDSJrONS): SUMMARY SHEET TOTAL SHIPPED: BILL OF LADING TOTALSHIPPED(only II different): Revised 10/1,94 O'Reilly, Talbot & Okun Associates, Inc. Atwood Drive Northampton, Massachusetts Site Locus January 1999 Figure 1 N Table & Analytical Data • Table 1 - Soil Analytical Results ND 40 Total Arsenic Total Cadmium ND 80 Total Chromium 13.8 1000 Total Lead 347 2000 TCLP Lead(mg/I) 3.23 5.0 Total Mercury ND 10 Total Petroleum Hydrocarbons ND 5000 Total PCBs 0.75 <2 Total SVOCs ND 100 Total VOCs ND 10 Conductivity 56 8,000 umhos/cm ND indicates Not Detected • SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID:TP-1/S-1 Lab ID No: AB10787 Matrix: Soil Collected: 06/23/98 by OTO Received on 07/02/98 by DDR QC and Data Review by Location: Atwood Drive- Northampton,MA Client Job No: J84-0520 Preservative: Refrigeration Container: 1 Glass Soil Jar Condition of Sample as Received: Satisfactory Delivered by: Courier Parameter PCB-1016 PCB-1221 PCB-1232 PCB-1242 PCB-1248 PCB-1254 PCB-1260 Decachlorobiphenyl (%) % Solids Polychlorinated Biphenyls (PCB's) Modified SW846 8081/8082 Result (ug/Kg) MDL Not detected Not detected Not detected Not detected Not detected 750 Not detected 73 91.3 Extracted Analyzed Analyst 250 07/02/98 07/06/98 TG 250 07/02/98 07/06/98 TC 250 07/02/98 07/06/98 TC 250 07/02/98 07/06/98 TC 250 07/02/98 07/06/98 TO 250 07/02/98 07/06/98 TO 250 07/02/98 07/06/98 TO 07/02/98 07/06/98 TO 0.1 07/02/98 07/02/98 SEC SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID:TP-1/S-1 Lab ID No.:AB10787 Matrix: Soil Collected: 06/23/98 by OTO Received on 07/02/98 by DDR QC and Data Review by Location: Atwood Drive- Northampton,MA. Client Job No.: J84-0520 Preservative: Refrigeration Container: 1 Glass Soil Jar Condition of Sample as Received: Satisfactory Delivered by: Courier Extractable Petroleum Hydrocarbons MA DEP Modified EPA 8270/8100 Parameter for AB10787 Aliphatics/Aromatics(mg/Kg) C9- C18 Aliphatics C19- C36 Aliphatics C11- C22 Aromatics Targeted PAH's Analytes (ug/Kg) Acenaphthene Acenaphthylene Anthracene Benzo (a) anthracene Benzo (b)fluoranthene Benzo (k) fluoranthene Benzo (a)pyrene Benzo (g,h.i)perylene Chrysene Dibenz (a,h) anthracene Fluoranthene Fluorene Indeno (1,2,3-cd) pyrene 2-Methylnaphthalene Naphthalene Phenanthrene Pyrene Surrogate Recovery(%) 1-Chloro-octadecane(%SR) Ortho-Terphenyl(%SR) % Solids Results Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected 43 42 91.3 MDL Extracted Analyzed Analyst 33 07/02/98 07/08/98 MB 33 07/02/98 07/08/98 MB 33 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 07/02/98 07/08/98 MB 07/02/98 07/08/98 MB 0.1 07/02/98 07/02/98 SEC SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: TP-1/S-1 Lab ID No: AB10787 Matrix: Soil Collected: 06/23/98 by OTO Received on 07/02/98 by DDR QC and Data Review by Location: Atwood Drive-Northampton,MA Client Job No: J84-0520 Preservative: Refrigeration Container: 1 Glass Soil Jar Condition of Sample as Received: Satisfactory Delivered by Courier 'arameter E otal Arsenic Total Barium rotal Cadmium rotal Chromium rotal Lead total Mercury total Selenium Total Silver Metals Result (mg/(g) MDL nd 51.3 nd 13.8 347 nd nd nd Method 0.904 EPA 2003 0.904 EPA 200.7 0.904 EPA 200.7 0.904 EPA 200 7 0.452 EPA 200.7 0 225 EPA 245.1 0.452 EPA 200.7 1.81 EPA 200.7 Digested Analyzed Analyst 07/08/98 07/08/98 CR 07/08/98 07/08/98 CR 07/08/98 07/08/98 CR 07/08/98 07/08/98 CR 07/08/98 07/08/98 CR 07/08/98 07/07/98 JM 07/08/98 07/07/98 CR 07/08/98 07/07/98 CR 91► SPECTRUM ANALYTICAL,INC. Massachusetts Certification M-MA 138 Connecticut Approval#PH 0777 Rhode bland#98&Maine#ala New Hampshire ID#2538 New York ID#11393 Florida HRS87448 O'Reilly, Talbot&Okun 293 Bridge Street, Suite 500 Springfield, MA 01103 June 2, 1999 Client Project No.: 84-05-17 Location: Atwood Drive - Northampton, MA Lab ID No AB44666 Client ID STOCK—I Analysis Requested TCLP Lead ENVIRONMENTAL ANALYSES 11 Almgren Drive •Agawam,Massachusetts 01001 • 413-789-9018 • FAX 413-789-4076 hector • SPECTRUM ANALYTICAL, INC. Laboratory Report (Subcontracted Analysis) Client ID: STOCK-1 Lab ID No: AB44666 Matrix: Soil Collected: 05/27/99 by OTO Received on 0527/99 oy KC QC and Data Review by MD Location: Atwood Drive-Northampton,MA Client Job No: 84-05-17 Preservative: Refrigeration Container: 1 Amber Glass Condition of Sample as Received: Satisfactory Delivered by: Client Parameter rCLP Lead TCLP Lead EPA Method 1311/SW846 6010 Result (mg/L) MDL 3.23 Extracted Analyzed Analyst 0.010 06/01/99 06/02/99 CR Special Handling: I _ L� _ 1-•.-r 1* to 6nciness days CHAIN OF CUSTODY Kul VKl1 rush TAT-Date Needed: • All TATs subject to laboratory ap rova;min. 24 hour notification needed for rushes. Page f of • Samples disposed of after 60 days unless SYECTlI otherwised instructed. UMANALttICAL Report To: 0 T U Invoice To: 0 TO Project No.: 4Z L/' OS' ( 7 rr II Site Name: �-k?WO�. p '\ Di‘u r,2.4 Location: th/P 4Wititi\ \`�� State: Project Mgr.: / /U:L /-t af..„ P.O.No.: RQN: Sampler(s): A X/;c(LtL*CA" (I4-4°C 2=HC1 3=H2S0, 4=HNOr 5=NaOH 6=MeOH 7= Containers: Analyses: Notes: DW=Drinking Water GW=Ground Water WW=Waste Water SO=Soil SL=Sludge 0-0il XI= X2= A ro \ > 0 6 a .y G=Grab C=Composite - , E U w J S O O O O (.` Lab Id: Sample Id: Date: Time: w w h 2 4t 2 AB#4164,41 S k 0 (k- ( 512,1191 C So ( / . AB _ AR • AB AB . AB AB AB Wi 1 I E Additional Instructions:_, Relinquished%: i Received — Date: Time: V.L)I �✓�,t v:� n i' ,<•, 5/27/99 is o7 • SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: NOHOCOMP Lab ID No: AB32390 Matrix: Soil Collected: 01/29/99 byyyOTO Received Data Review by MBR Location: Atwood Client Job No.: J084 Preservative: Refrigeration Container : 2 Amber Glass Jars Condition of Sample as Received: Satisfactory Delivered by: Client Parameter for AB32390 cenaphthene scenaphthylene \nthracene 3enzidine - 3enzoic acid 3enzo (a) anthracene 3enzo (b) fluoranthene 3enzo (k) fluoranthene Benzo(g,h,i)perylene Benzo(a)pyrene Benzyl alcohol Bis(2-chloroethoxy) methane Bis (2-chloroethyl) ether Bis (2-chloroisopropyl) ether Bis (2-ethylhexyl)phthalate 4-Bromophenyl phenyl ether Butyl benzyl phthalate 4-Chloroaniline 2-Chloronaphthalene 4-Chloro-3-methylphenol 2-Chlorophenol 4-Chlorophenyl phenyl ether Chrysene Dibenz (a,h) anthracene Dibenzofuran Di-n-butylphthalate 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene 3,3'-Dichlorobenzidine Semivolatile Organics EPA Method 8270 Result (ug/Kg) MDL Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected 144.0 144.0 144.0 144.0 720.0 144.0 144.0 144.0 144.0 144.0 288.0 144.0 144.0 144.0 144.0 144.0 144.0 288.0 144.0 288.0 144.0 144.0 144.0 144.0 144.0 144.0 144.0 144.0 144.0 288.0 Extracted Analyzed Analyst 02/02/99 02/03/99 .KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS 02/02/99 02/03/99 KS Continued next page.. 'arameter for AB32390 Result (ug/Kg) MDL Extracted Analyzed Analyst I-Dichlorophenol Not detected 144.0 02/02/99 02/03/99 KS S-Dichlorophenol Not detected 144.0 02/02/99 02ro3/99 KS Not detected 144.0 02/02/99 02/03/99 KS .ethyl phthalate 1-Dimethlylpheno] Not detected 144.0 02/02/99 02/03/99 KS 5-Dinitro-2-methylphenol Not detected 720.0 02/02/99 02/03/99 KS Not detected 720.0 02/02/99 02/03/99 KS 4-Dinitrotoluen e 4-Dinitroph Not detected 144.0 02/02/99 02/03/99 KS en 6-Dinitrotoluene Not detected 144.0 02/02/99 02/03/99 KS 2-Diphenylhydrazine Not detected 144.0 02/02/99 02/03/99 KS i-n-Propylnitrosoamine Not detected 144.0 02/02/99 02/03/99 KS luoranthene Not detected 144.0 02/02/99 02/03/99 KS luorene Not detected 144.0 02/02/99 02/03/99 KS [exachlorobenzene Not detected 144.0 02/02/99 02/03/99 KS [exachlorobutadiene Not detected 144.0 02/02/99 02/03/99 KS 144.0 02/02/99 02/03/99 KS lexachlorocyclopentadiene Not detected 144.0 02/02/99 02/03/99 KS [exachloroethafl thane Not detected 02/02/99 02/03/99 KS(1,2,3-cd) pyrene Not detected 144.0 Not detected 144.0 02/02/99 02/03/99 KS Meth ylnaphthalene Not detected - ne 144.0 02/02/99 02/03/99 .<S eth 144.0 02/02/99 02/03/99 -KS ,-Methylphenol (0-cresol) Not detected 144.0 02/02/99 02/03/99 KS ,-Methylphenol (p-cresol) Not detected 144.0 02/02/99 02/03/99 KS Qaphthalene Not detected !-Nitroaniline Not detected 720.0 02/02/99 02/03/99 KS Not detected 720.0 02/02/99 02/03/99 KS 1-Nitroaniline I-Nitroaniline Not detected 720.0 02/02/99 02/03/99 KS ■itrobenzene Not detected 144.0 02/02/99 02/03/99 KS Not detected 144.0 02/02/99 02/03/99 KS -Nitrophenol 4-Nitrophenol Not detected 720.0 02/02/99 02/03/99 KS Not detected 144.0 02/02/99 02/03/99 KS N-Nitrosodimethylamine 144.0 02/02/99 02/03/99 KS N-Nitrosodiphenylamine Not detected Not detected 720.0 02/02/99 02/03/99 KS Phe nan a P n th rophenol rene Not detected 144.0 02/02/99 02/03/99 KS Not detected 144.0 02/02/99 02/03/99 KS Pyrene Phenol Not detected 288.0 02/02/99 02/03/99 KS 1,2,4-T richlorobenzene Not detected 144.0 02/02/99 02/03/99 KS -T 2,4,5-Tichlorophenol Not detected 144.0 02/02/99 02/03/99 KS Not detected 144.0 02/02/99 02/03/99 KS 2 loropheno] 144.0 02/02/99 02/03/99 KS Py yri/dine dine Not detected Dimethyl phthalate Not detected 144.0 02/02/99 02/03/99 KS Di-n-octyl phthalate No[detected 144.0 02/02/99 02/03/99 KS 0.1 02/03/99 02/03/99 GMM % Solids 89.7 SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID:NOHOCOMP Lab ID No.:AB32390 Matrix: Soil Collected:01/29/99 byyyOTO Received Data Review by MBR Location: Atwood Client Job No.: J084 Preservative: Container: Condition of Sample as Received: Satisfactory Delivered Parameter for AB32390 Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroform 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dlbromochloromethane 1,2-Dtbromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,1-Dichloroethane 1,2 Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane Volatile Organics EPA Method 8260 Result (ug/Kg) Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected MDL 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 Extracted Analyzed Analyst 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD Continued next page.. Parameter for AB32390 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene chloride Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Triehloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene m,p-Xylenes o-Xylene Methyl-t-butyl ether Result (ug/Kg) Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected BFB Surrogate Recovery (%) 101 p-DFB Surrogate Recovery(%) 105 CLB-d5 Surrogate Recovery (%) 98 % Solids 89.7 MDL 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 6.1 12.2 6.1 6.1 Extracted Analyzed Analyst 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 CD 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 02/02/99 CD CD CD 0.1 02/03/99 02/03/99 CMM SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: NOHOCOMP Lab ID No.:AB32390 Matrix: Soil Collected: 01/29/99 by OTO QC and Data 01/29/99 eew by MBR Location: Atwood Client Job No.: J084 Preservative: Refrigeration Container 2 Amber Glass Jars nditi of Sample as Received: Satisfactory Delivered Total Hydrocarbons by GC Modified EPA Method 8100 Parameter Total Hydrocarbons (GC) Fingerprint based quantifrcaton: Gasoline Fuel Oil #2 Fuel Oil #4 Fuel Oil#6 Motor Oil Ligroin Aviation Fuel Other Oil Unidentified % Solids Result (mg/Kg) Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected 89.7 MDL Extracted Analyzed Analyst 02/02/99 02/02/99 LR 40 02/02/99 02/02/99 LR 40 02/02/99 02/02/99 LR 40 02/02/99 02/02/99 LR 80 02/02/99 02/02/99 LR 80 02/02/99 02/02/99 LR 40 02/02/99 02/02/99 LR 40 02/02/99 02/02/99 LR 80 02/02/99 02/02/99 LR 02/02/99 02/02/99 LR 0.1 02/03/99 02/03/99 GMM Petroleum identification is determined by comparing the GC fingerprint obtained from the sample with a library of GC fingerprints obtained from petroleum products. Possible match categories are as follows; Gasoline-includes regular,unleaded,premium,etc. Fuel Oil#2-includes home heating oil,#2 fuel oil and diesel. Fuel Oil#4-Includes#4 Fuel Oil. Fuel Oil#6-includes#6 oil and bunker"C"oil. Motor Oil-includes virgin and waste automobile. Ligroin-includes mineral spirits,petroleum naphtha,vm&p naphtha. Aviation Fuels-includes Kerosene,Jet A and JP-4. Other Oil-includes lubricating and cutting oil and silicon oil. Factors such as microbial degradation,weathering and solubility generally prevent specific identification within a petroleum category. A finding of"unidentified"means that the sample fingerprint was characteristic of a petroleum product,but could not be matched to a fingerprint in the library. After fingerprint identification,the amount present in the sample is quantified using a calibration curve prepared from a petroleum product of the same category as the identified petroleum. Unidentified petroleum is quantified using a petroleum calibration that approximates the distribution of compounds in the sample. A' in the results column indicates the petroleum calibration used to quantify unidentified samples. SPECTRUM ANALYTICAL,INC. Laboratory Report(Subcontracted Analyses) Client ID:NOHOCOMP Lab ID No: AB32390 Matrix: Soil Collected: 0129/99 byyyOTO Received on and Data Review by MBR rameter nductance Result 56 Location: Atwood Client Job No: J084 Preservative: Refrigeration Container: 2 Amber Glass Jars Condition of Sample as Received: Satisfactory Client Wet Chemistry Analyses MDL Units Method Start Date Analyst 1.0 umhos/cm S205/E120.1 02/01/99 PX Spectrum Analytical,Inc. Laboratory Report Supplement References :thods for the Determination of Organic Compounds in Drinking Water. EPA-600/4-88/039. EMSL 1988. ethods for Chemical Analysis of Water and Wastes. EPA 600/4-79-020. EMSL 1983. ethods for Organic Chemical Analysis of Municipal and Industrial Wastewater. EPA 600/4-82-057 est Methods for Evaluating Solid Waste. Physical/Chemical Methods. EPA SW-846. 1986. tandard Methods for the Examinatinon of Water and Wastes. APHA-AWWA-WPCF. 16th Edition. 1985. (tandard Methods for Comparison of Waterborne Petroleum Oils by Gas Chromatography. ASTM D 3328. 1982. Dil Spill Identification System. U.S.Coast Guard CG-D-52-77. 1977. Handbook for Analytical Quality Control in Water and Wastewater Laboratories. EPA 600/4-79-019. EMSL 1979. Choosing Cost-Effective QA/QC(Quality Assurance/Quality Control)Programs for Chemical Anslyses. EPA 600/4-85/056. EMSL 1985. EMSL 1982. - Not Detected, Not Det,ND or nd NC MCL VOA BFB p-DFB CLB-d5 BCP TFT Decachlorobiphenyl Renort�ns The compound was not detected at a concentration equal to or above the established method detection limit = Not Calculated EPA Maximum Contamination Level Volatile Organic Analysis = 4-Brompfluorobenzene = 1,4-DUuorobenzene = Chlorobenzene-di - = 2-Bromo-1-chloropropane = a,a,a-Triuorotohrene = (an EPA 608/8080 Surrogate) (An EPA 624 Surrogate) (An EPA 624 Surrogate) (An EPA 624 Surrogate) (An EPA 601 Surrogate) (An EPA 602 Surrogate) efin p itions Surrogate Recovery=The recovery(expressed as a percent)of a non-method analyte(see surrogates listed above) added to the sample for the purpose of monitoring system performance. Matrix Spike Recovery=The recovery(expressed as a percent)of method analytes added to the sample for the purpose of determining any effect of sample composition on analyte recovery. Laboratory identical procedures. Analyses of laboratory duplicates give rsa measure of the preceision associated aw th wrth laboratory procedures,but not with sample collection,preservation,or storage procedures. Field Duplicate=Two separate samples collected at the same time and place under identifical measure circumstances and treated exactly the same throughout field and laboratory p sure of as well as with laboratory procedures. Analysis of Field duplicates give a ea of thhe precision associated with sample collection,preservaton and storage, Relative Percent Difference (V°RPD)=The precision measurement obtained on duplicate/replicate analyses. %RPD is calculated as: %RPD=(valued lue2)* 100% ave.value Special Handling: ❑ Standard TAT-7 to 10 business gilL CHAIN OF CUSTODY RECORD Rush TAT-Date Needed VB II TATS subject to laboratory approva 24 hour notification needed for rushes. • Samples disposed of after 60 days unless Page of otherwised instructed. SPECTRUM ANALYTICAL � -�/'�1� n7Z) Project No.: �'l� Report To: Invoice To: U Site Name: a G Location: State: Sampler(s): r P.O.No.' RQN: Project Mgr.: - Notes: Containers: i �-4° 2=11C1 3=H2S0a 4=1-1NO3 S=NaOH 6=MeOH 7-______ v. DW=•i ing Water GW=Ground Water WW=Waste Water •=So' 1 SL=Sludge Oil X1= X2-_______ ittitimiti 111 I AB 333 .7 BEITIONWE 711111 nllnnuannnIURUMM®n•_ Q mod ' AB W.3411 1 C o— II MEM -■"11flf fl flMMMP ` j o r ma -1 ■1a■ 0mmu �i P 1■ tronvorna anionnumarmumoronterm AB. __11111.111111111111111111 151111111111111111151111 UM 'iv ) Received By: Date: ?I Additional Instructions: ��� ��== • Special Handling: ❑ Standard TAT-7 to 10 busine cI s g‘ CHAIN OF CUSTODY RECORD ❑Rush TAT-Date Needed: (-5/ • All TATs subject to laboratory approval;mm. 24 hour notification needed for rushes. • Samples disposed of after 60 days unless Page_a_of othenvised instructed. SPECTRUM ANALYTICAL &A Project No.: —13 Invoice To: Report To: Site Name: A 7/ AZ Location: State: Al RQN: Sampler(s): A I Project Mgr.: �S l'V(Q v P.O.No.: Analyses: Notes: =q° 2=HC1 3=H,S0. 4=HN0, S=NaOH 6=MeOH 7= Containers: DW=Drinking Water GW=Ground Water WW=Waste Water •=Sor SL—Sludge O=Oil X1= 111 o L G=Grab C=Composite m Lab Id: Sample Id: Date: Time: . a AB N3c/C) SS MIIIIIIIMMISIngfiaMINS 5; SS 111111.1����D���a���D r : AB �1111111D1111111MMI IMI lki AB IIIIIIIIIIIIIIIIIIIIIINIIIIIIMIIIIIIINIIIIIIMIMIMM AB IMMIIIMISIM111111111.1S, AB ; --_■■■■■.■■..■■.■■■■S AB --_■■■■.■.■.■.■■■■■■ AB --_■■■.■■■.■■■■■■■■■ --_■■ 1115 ■■■■■■■ ■ ■ AB Received By: Date: Time: Relinquished By: Additional Instructions: ' 1